JP2015143214A - パック - Google Patents
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- JP2015143214A JP2015143214A JP2014260921A JP2014260921A JP2015143214A JP 2015143214 A JP2015143214 A JP 2015143214A JP 2014260921 A JP2014260921 A JP 2014260921A JP 2014260921 A JP2014260921 A JP 2014260921A JP 2015143214 A JP2015143214 A JP 2015143214A
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Images
Abstract
【解決手段】不織布または織布からなる基材2と、ゲル3とを有し、少なくともゲル3に化粧料組成物が保持されて構成され、ゲル3を顔面に貼り付けて使用されるシート状のパック1であって、パック1は、顔面に貼り付けた際の縦方向における伸長率が15〜50%、顔面に貼り付けた際の横方向における伸長率が3〜14%、顔面に貼り付けた際の縦方向における50%伸長回復率が50%以上、ブリード率が9〜16%であることを特徴とするパック1。
【選択図】図1
Description
図1は本発明に係るパックの一例として顔面全体の大きさに該当するパック1を示す平面図であり、図2は図1に示すパック1のI−I線断面図である。
パック全体の厚みは、パックを切断し、その断面のマイクロスコープ(デジタル顕微鏡)写真における5個所の厚みを目視にて測定し、それら測定値を平均することにより求めた。
ゲル層(ゲルのみの部分)の厚みは、その断面のマイクロスコープ写真における5個所の厚みを目視にて測定し、それら測定値を平均することにより求めた。
中間層(基材における、ゲルが浸透した部分)の厚みは、パックから切り出した長方形の試験片について、以下の式により算出した。
(中間層の厚み)=(パックの重量)−(ゲル層の重量)−(基材の重量)
/{(ゲルの密度)×(ゲルの面積)}
なお、以下の各実施例では、中間層の厚みの測定に使用する試験片の寸法を統一した。
(1)基材を含まない、所定の厚みdのゲルシートを作成する。
(2)(1)で得られたゲルシートを所定の面積Sに切り取り、重量Wを電子天秤にて測定する。
(3)次式より、ゲルの密度を算出する。
(ゲルの密度)=W/(d×S)
また、ゲルの面積は、試験片の縦の長さと横の長さとの積とした。
(ゲル層の重量)=(ゲル層の厚み)×(ゲルの密度)×(ゲルの面積)
(基材の重量)=(基材の目付け)×(基材の面積)
基材の面積は、試験片の縦の長さと横の長さとの積とした。
中間層を除く基材(基材における、ゲルが浸透していない部分)の厚みは、以下の式により算出した。
(中間層を除く基材の厚み)
=(パック全体の厚み)−(ゲル層の厚み)−(中間層の厚み)
水(69.90重量%)、ポリアクリル酸ナトリウム(高分子骨格:3.5重量%)、メタケイ酸アルミン酸マグネシウム(架橋剤:0.8重量%)、ジプロピレングリコール(保湿剤:10重量%)、ポリエチレングリコール1000(ブリード促進剤:2.0重量%)、グリセリン(保湿剤:1.0重量%)、ジグリセリン(保湿剤:4.0重量%)、キサンタンガム(粘剤:0.3重量%)、オリーブスクワラン(保湿剤:2.0重量%)、加水分解コラーゲン(植物・動物エキス:0.1重量%)、フェノキシエタノール(防腐剤):0.4重量%)の各成分をガラスもしくはプラスチック製容器でスリーワンモーターを用いて混ぜたところに、30重量%酒石酸水溶液(架橋促進剤:水4.2重量%、酒石酸1.8重量%)を加えてpHが5のゲル組成物を調製した。
ゲル組成物の塗布量を変更し、ゲルの厚みをそれぞれ0.54mm(パック全体の厚み0.80mm)、0.90mm(パック全体の厚み1.20mm)、1.02mm(パック全体の厚み1.40mm)とした以外は、上記実施例1と同様にしてパックを得た。
上記実施例1において、基材を、目付75g/m2のニードルパンチ製法によるPET繊維製の不織布(ダイワボウポリテック株式会社製:製品名NI−75)とした以外は、上記実施例1と同様にして、ゲルの厚みが0.85mmでパック全体の厚みが1.00mmのパックを得た。
上記実施例1において、基材を、目付90g/m2のニードルパンチ製法によるPET繊維製の不織布(ダイワボウポリテック株式会社製:製品名QZ−90)とした以外は、上記実施例1と同様にして、ゲルの厚みが0.74mmでパック全体の厚みが1.05mmのパックを得た。
上記実施例1において、基材を、目付90g/m2のスパンレース製法によるPET繊維製の不織布(日本バイリーン株式会社製:製品名EW7900)とした以外は、上記実施例1と同様にして、ゲルの厚みが0.94mmでパック全体の厚みが1.15mmのパックを得た。
上記実施例1において、基材を、目付80g/m2のスパンレース製法によるPET繊維製の不織布(日本バイリーン株式会社製:製品名EW2080S)とした以外は、上記実施例1と同様にして、ゲルの厚みが0.83mmでパック全体の厚みが1.10mmのパックを得た。
上記実施例1において、基材を、目付95g/m2のスパンレース製法によるPP繊維製の不織布(日本バイリーン株式会社製:製品名EL5600T)とした以外は、上記実施例1と同様にして、ゲルの厚みが0.80mmでパック全体の厚みが1.35mmのパックを得た。
上記実施例3において、基材を、目付60g/m2のスパンボンド製法及びスパンレース製法によるセルロース(キュプラ)製の不織布(旭化成せんい株式会社製:製品名ベンリーゼ(登録商標)SE603)とした以外は、上記実施例3と同様にして、ゲルの厚みが0.8mmでパック全体の厚みが0.8mmのパックを得た。
上記実施例3において、基材を、目付80g/m2のスパンボンド製法及びスパンレース製法によるセルロース(キュプラ)製の不織布(旭化成せんい株式会社製:製品名ベンリーゼ(登録商標)SE803)とした以外は、上記実施例3と同様にして、ゲルの厚みが0.8mmでパック全体の厚みが0.8mmのパックを得た。
上記実施例3において、基材を、目付100g/m2のスパンボンド製法及びスパンレース製法によるセルロース(キュプラ)製の不織布(旭化成せんい株式会社製:製品名ベンリーゼ(登録商標)SE103)とした以外は、上記実施例3と同様にして、ゲルの厚みが0.8mmでパック全体の厚みが0.8mmのパックを得た。
上記実施例3において、基材を、目付70g/m2のスパンボンド製法によるポリオレフィン系エラストマー製の不織布(出光ユニテック株式会社製:製品名ストラフレックス(登録商標)UN5070)とした以外は、上記実施例3と同様にして、ゲルの厚みが0.8mmでパック全体の厚みが0.8mmのパックを得た。
上記実施例3において、基材を、厚み0.04mmのポリウレタン製のフィルム(小松製練株式会社製:製品名ST2641)とした以外は、上記実施例3と同様にして、ゲルの厚みが0.8mmでパック全体の厚みが0.84mmのパックを得た。
上記実施例3において、基材を、厚み0.4mmの、ポリウレタンフィルムとポリエステル織布との複合基材(小松製錬株式会社製:製品名575)とした以外は、上記実施例3と同様にして、ゲルの厚みが0.8mmでパック全体の厚みが1.2mmのパックを得た。
イソステアリルグリセリルエーテル(2.0重量%)、ポリアクリル酸ソーダ(6.0重量%)、ポリアクリル酸(2.5重量%)、グリセリン(25.0重量%)、ミリスチン酸イソプロピル(2.0重量%)、スクワラン(4.0重量%)、水酸化アルミニウムゲル(0.2重量%)、軽質無水シリカ(2.0重量%)、ポリソルベート80(2.0重量%)、精製水(バランス)の各成分を均一に混ぜ合わせることによりゲル組成物を調製した。
結果を表1および表2に示す。
結果を表3に示す。
2 基材
3 ゲル
31 ゲル層
32 中間層
Claims (5)
- 不織布または織布からなる基材と、ゲルとを有し、少なくともゲルに化粧料組成物が保持されて構成され、ゲルを顔面に貼り付けて使用されるシート状のパックであって、
パックは、顔に貼り付けた際の縦方向および横方向における以下の方法で測定される伸長率が縦方向で15〜50%、横方向で3〜14%、顔に貼り付けた際の縦方向における以下の方法で測定される50%伸長回復率が50%以上、以下の方法で測定されるブリード率が9〜16%であることを特徴とするパック。
伸長率の測定方法;幅50mm×長さ60mmのパックを長さ40mmの間隔でチャックし、伸長速度80mm/分で引き伸ばして1Nの荷重時の長さLを測定し、伸長率(%)=[(L−40)/40]×100を計算する。
50%伸長回復率の測定方法;幅25mm×長さ60mmのパックを長さ40mmの間隔でチャックし、伸長速度300mm/分でチャック間距離が60mmの長さとなるまで伸長させた後、同じ速度で戻し、得られる荷重−伸び曲線より残留応力が0となる時の伸びL´(残留応力が0になる時のチャック間距離−測定前のチャック間距離(40mm))を測定し、50%伸長回復率(%)=[[(60−40)−L´]/(60−40)]×100を計算する。
ブリード率の測定方法;50mm×50mm角に切断したパックを二つ折りにした重量Aの濾紙の片面に貼り付けて当該濾紙の間に挟み込んで試料とし、試料の重量Sを測定し、この試料を100mm×200mm×3mmの2枚のガラス板の間でさらに挟んで10分間放置する。その後、試料からパックを取り除いて濾紙の重量Cを測定し、濾紙にブリードした化粧料組成物の液量(C−A)からブリード率R=[(C−A)/(S−A)]×100を計算する。 - 前記パックは、顔に貼り付けた際の縦方向における以下の方法で測定される25%伸長回復時の力が0.15〜1.0N/25mmである請求項1記載のパック。
25%伸長回復時の力;50%伸長回復率の測定時と同一条件でパックを伸長させた後、同じ速度でチャック間距離が50mmとなるまで戻し、その時の力を、25%伸長回復時の力として測定する。 - 前記パックは、以下の方法で測定される垂直粘着力が0.020〜0.028N/12mmφである請求項1または2に記載のパック。
垂直粘着力の測定方法;30mm×30mm角に切断したパックのゲルの面に、直径12mmのSUS304製円柱を1mm/分の速度で0.294Nの荷重となるように押し当て、10秒間接触後、300mm/分の速度で引きはがし、その際の引きはがしに要した力を垂直粘着力として測定する。 - 前記パックは、不織布の目付が75〜100g/m2、ゲルの厚みが0.3〜1.5mmである請求項1ないし3の何れか一に記載のパック。
- 前記パックは、顔面全体に該当する大きさ、顔面の上半部に該当する大きさ、または顔面の下半部に該当する大きさに形成されたものである請求項1ないし4の何れか一に記載のパック。
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JPWO2018181930A1 (ja) * | 2017-03-31 | 2019-12-26 | 積水化成品工業株式会社 | ゲルシート |
CN110430859B (zh) * | 2017-03-31 | 2022-09-30 | 积水化成品工业株式会社 | 凝胶片 |
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