JP2013531600A - チタン化合物を製造する方法 - Google Patents

チタン化合物を製造する方法 Download PDF

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Publication number
JP2013531600A
JP2013531600A JP2013511389A JP2013511389A JP2013531600A JP 2013531600 A JP2013531600 A JP 2013531600A JP 2013511389 A JP2013511389 A JP 2013511389A JP 2013511389 A JP2013511389 A JP 2013511389A JP 2013531600 A JP2013531600 A JP 2013531600A
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mixture
titanium dioxide
temperature
tiocl
range
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Japanese (ja)
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JP2013531600A5 (enExample
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ジェフリー・スコット・トンプソン
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EIDP Inc
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EI Du Pont de Nemours and Co
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/04—Oxides; Hydroxides
    • C01G23/047—Titanium dioxide
    • C01G23/053—Producing by wet processes, e.g. hydrolysing titanium salts
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/003—Titanates
    • C01G23/005—Alkali titanates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00—Lithium compounds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/04—Oxides; Hydroxides
    • C01G23/047—Titanium dioxide
    • C01G23/053—Producing by wet processes, e.g. hydrolysing titanium salts
    • C01G23/0536—Producing by wet processes, e.g. hydrolysing titanium salts by hydrolysing chloride-containing salts
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/485—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of mixed oxides or hydroxides for inserting or intercalating light metals, e.g. LiTi2O4 or LiTi2OxFy
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/11—Powder tap density
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/80—Compositional purity
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Battery Electrode And Active Subsutance (AREA)
JP2013511389A 2010-05-21 2011-05-20 チタン化合物を製造する方法 Pending JP2013531600A (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US34724910P 2010-05-21 2010-05-21
US61/347,249 2010-05-21
PCT/US2011/037344 WO2011146838A2 (en) 2010-05-21 2011-05-20 Process for making titanium compounds

Publications (2)

Publication Number Publication Date
JP2013531600A true JP2013531600A (ja) 2013-08-08
JP2013531600A5 JP2013531600A5 (enExample) 2014-06-19

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Family Applications (1)

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JP2013511389A Pending JP2013531600A (ja) 2010-05-21 2011-05-20 チタン化合物を製造する方法

Country Status (7)

Country Link
US (1) US20130039844A1 (enExample)
EP (1) EP2571811A4 (enExample)
JP (1) JP2013531600A (enExample)
KR (1) KR20130080019A (enExample)
CN (1) CN102906025A (enExample)
CA (1) CA2794633A1 (enExample)
WO (1) WO2011146838A2 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20210039660A (ko) * 2019-10-02 2021-04-12 더블유알씨 주식회사 이산화티탄 분말의 제조 방법

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101431693B1 (ko) 2011-12-29 2014-08-22 주식회사 포스코 이산화티타늄 나노분말, 타이타네이트, 리튬 타이타네이트 나노 분말 및 이들의 제조 방법
US20140363366A1 (en) * 2013-06-05 2014-12-11 E I Du Pont De Nemours And Company Process for making titanium compounds
CN105883917B (zh) * 2016-05-26 2017-10-24 宜宾天原集团股份有限公司 一种利用氯化法钛白粉废气制备TiO2及HCl溶液的方法
CN112174197B (zh) * 2020-09-29 2022-05-24 攀钢集团研究院有限公司 以四氯化钛为原料制备锂电负极材料钛酸锂的方法
KR102428917B1 (ko) * 2022-02-11 2022-08-02 김래희 개선된 티타늄옥시클로라이드의 제조 방법

Citations (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2512807A (en) * 1947-09-23 1950-06-27 Nicholson Douglas Gillison Purification of titanium halides
US4923682A (en) * 1989-03-30 1990-05-08 Kemira, Inc. Preparation of pure titanium dioxide with anatase crystal structure from titanium oxychloride solution
US4944936A (en) * 1987-04-10 1990-07-31 Kemira, Inc. Titanium dioxide with high purity and uniform particle size and method therefore
WO1999003784A1 (en) * 1997-07-15 1999-01-28 Sony Corporation Lithium hydrogentitanates and process for the preparation thereof
JP2000034124A (ja) * 1998-07-16 2000-02-02 Korea Atom Energ Res Inst 結晶性酸化チタン超微粒単分散粉末の製造方法
JP2001213622A (ja) * 2000-01-26 2001-08-07 Toho Titanium Co Ltd チタン酸リチウムの製造方法およびリチウムイオン電池並びにその電極
JP2002211925A (ja) * 2000-11-20 2002-07-31 Ishihara Sangyo Kaisha Ltd チタン酸リチウム及びその製造方法並びにそれを用いてなるリチウム電池
US20020102205A1 (en) * 2001-01-29 2002-08-01 Amatucci Glenn G. Nanostructure lithium titanate electrode for high cycle rate rechargeable electrochemical cell
CN1631795A (zh) * 2004-11-16 2005-06-29 浙江工业大学 一种金红石相二氧化钛纳米粉体的制备方法
US20060257746A1 (en) * 2005-05-13 2006-11-16 Hiroki Inagaki Nonaqueous electrolyte battery, lithium-titanium composite oxide, battery pack and vehicle
CN101074112A (zh) * 2007-06-27 2007-11-21 仙桃市中星电子材料有限公司 高纯超细二氧化钛的制备方法
JP2008105943A (ja) * 2001-07-20 2008-05-08 Altairnano Inc チタン酸リチウムの製造方法
WO2010137582A1 (ja) * 2009-05-26 2010-12-02 石原産業株式会社 チタン酸リチウム及びその製造方法並びにそれを用いた電極活物質及び蓄電デバイス

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4540167B2 (ja) * 1999-02-16 2010-09-08 東邦チタニウム株式会社 チタン酸リチウムの製造方法
CN1275342C (zh) * 2004-12-17 2006-09-13 清华大学 锂离子电池负极材料球形Li4Ti5O12的制备方法
CN100411994C (zh) * 2006-07-07 2008-08-20 清华大学 一种掺碳球形Li4Ti2O12的制备方法
KR101045416B1 (ko) * 2006-09-12 2011-06-30 주식회사 엘지화학 리튬티탄산화물 분말, 그 제조방법, 이를 포함하는 전극,및 이차전지
CN101378119A (zh) * 2008-10-06 2009-03-04 天津巴莫科技股份有限公司 锂离子电池用碳包覆型钛酸锂的制备方法
CN101428851A (zh) * 2008-12-04 2009-05-13 上海大学 锂离子电池负极材料钛酸锂的制备方法
CN101587948B (zh) * 2009-06-19 2011-05-18 中南大学 一种Li4Ti5O12/C复合电极材料的制备方法

Patent Citations (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2512807A (en) * 1947-09-23 1950-06-27 Nicholson Douglas Gillison Purification of titanium halides
US4944936A (en) * 1987-04-10 1990-07-31 Kemira, Inc. Titanium dioxide with high purity and uniform particle size and method therefore
US4923682A (en) * 1989-03-30 1990-05-08 Kemira, Inc. Preparation of pure titanium dioxide with anatase crystal structure from titanium oxychloride solution
WO1999003784A1 (en) * 1997-07-15 1999-01-28 Sony Corporation Lithium hydrogentitanates and process for the preparation thereof
JP2000034124A (ja) * 1998-07-16 2000-02-02 Korea Atom Energ Res Inst 結晶性酸化チタン超微粒単分散粉末の製造方法
JP2001213622A (ja) * 2000-01-26 2001-08-07 Toho Titanium Co Ltd チタン酸リチウムの製造方法およびリチウムイオン電池並びにその電極
JP2002211925A (ja) * 2000-11-20 2002-07-31 Ishihara Sangyo Kaisha Ltd チタン酸リチウム及びその製造方法並びにそれを用いてなるリチウム電池
US20020102205A1 (en) * 2001-01-29 2002-08-01 Amatucci Glenn G. Nanostructure lithium titanate electrode for high cycle rate rechargeable electrochemical cell
JP2008105943A (ja) * 2001-07-20 2008-05-08 Altairnano Inc チタン酸リチウムの製造方法
CN1631795A (zh) * 2004-11-16 2005-06-29 浙江工业大学 一种金红石相二氧化钛纳米粉体的制备方法
US20060257746A1 (en) * 2005-05-13 2006-11-16 Hiroki Inagaki Nonaqueous electrolyte battery, lithium-titanium composite oxide, battery pack and vehicle
CN101074112A (zh) * 2007-06-27 2007-11-21 仙桃市中星电子材料有限公司 高纯超细二氧化钛的制备方法
WO2010137582A1 (ja) * 2009-05-26 2010-12-02 石原産業株式会社 チタン酸リチウム及びその製造方法並びにそれを用いた電極活物質及び蓄電デバイス

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JPN6014041198; ＬＥＥ，　Ｊ．-Ｈ．　ｅｔ　ａｌ: 'Ｅｓｔｉｍａｔｉｏｎ　ｏｆ　ｒｅａｃｔｉｏｎ　ｃｏｎｄｉｔｉｏｎｓ　ｆｏｒ　ｓｙｎｔｈｅｓｉｓ　ｏｆ　ｎａｎｏｓｉｚｅｄ　ｂｒｏｏｋｉｔｅ-ｔｙｐｅ　ｔｉｔａｎｉｕｍ　ｄｉｏｘｉｄｅ　ｆｒｏｍ　ａｑｕ' Ｊ．　Ｍａｔｅｒ．　Ｓｃｉ． Ｖｏｌ．４０，　Ｎｏ．１１, 200506, ｐ．２８４３-２８４７ *
JPN6014041199; 中原勝儼: 無機化合物・錯体辞典 , 19970610, ｐ．４７４, 講談社 *
JPN6015037496; ＺＡＮＧ，　Ｇ．　ｅｔ　ａｌ: 'Ｐｒｅｐａｒａｔｉｏｎ　ｏｆ　Ｌｉ４Ｔｉ５Ｏ１２　ｗｉｔｈ　Ｈｙｄｒａｔｉｏｎ　Ｔｉｔａｎｉｕｍ　Ｄｉｏｘｉｄｅ　ｆｏｒ　Ｅｌｅｃｔｒｏｃｈｅｍｉｃａｌ　Ｈｙｂｒｉｄ　Ｃａｐａｃｉｔｏｒ' Ｊｏｕｒｎａｌ　ｏｆ　Ｉｎｏｒｇａｎｉｃ　Ｍａｔｅｒｉａｌｓ Ｖｏｌ．２４，　Ｎｏ．３, 200905, ｐ．５３１-５３４ *
JPN6015037497; 舟木好右衛門，外: 'ＴｉＣｌ４の加水分解によって生成するＴｉＯ２の性状に関する研究' 工業化学雑誌 Ｖｏｌ．５９，　Ｎｏ．１１, 1956, ｐ．１２９５-１２９７ *
JPN6015037498; 舟木好右衛門，外: 'ＴｉＣｌ４の加水分解によるＴｉＯ２の製造に関する研究' 工業化学雑誌 Ｖｏｌ．５９，　Ｎｏ．１１, 1956, ｐ．１２９１-１２９５ *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20210039660A (ko) * 2019-10-02 2021-04-12 더블유알씨 주식회사 이산화티탄 분말의 제조 방법
KR102256399B1 (ko) 2019-10-02 2021-05-26 더블유알씨 주식회사 이산화티탄 분말의 제조 방법

Also Published As

Publication number Publication date
KR20130080019A (ko) 2013-07-11
WO2011146838A2 (en) 2011-11-24
CN102906025A (zh) 2013-01-30
WO2011146838A3 (en) 2012-03-29
EP2571811A2 (en) 2013-03-27
CA2794633A1 (en) 2011-11-24
US20130039844A1 (en) 2013-02-14
EP2571811A4 (en) 2016-02-17

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