JP2012529549A5 - - Google Patents
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- Publication number
- JP2012529549A5 JP2012529549A5 JP2012514476A JP2012514476A JP2012529549A5 JP 2012529549 A5 JP2012529549 A5 JP 2012529549A5 JP 2012514476 A JP2012514476 A JP 2012514476A JP 2012514476 A JP2012514476 A JP 2012514476A JP 2012529549 A5 JP2012529549 A5 JP 2012529549A5
- Authority
- JP
- Japan
- Prior art keywords
- per
- fluoroionomer
- group
- solvent
- liquid composition
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 238000000034 method Methods 0.000 claims description 14
- 239000002904 solvent Substances 0.000 claims description 9
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 6
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 claims description 6
- 239000002131 composite material Substances 0.000 claims description 3
- 238000005470 impregnation Methods 0.000 claims description 2
- 239000012528 membrane Substances 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims 23
- 239000007788 liquid Substances 0.000 claims 11
- 229910052731 fluorine Inorganic materials 0.000 claims 9
- 229910052794 bromium Inorganic materials 0.000 claims 8
- 229910052801 chlorine Inorganic materials 0.000 claims 8
- 229910052736 halogen Inorganic materials 0.000 claims 8
- 150000002367 halogens Chemical group 0.000 claims 8
- 229910052740 iodine Inorganic materials 0.000 claims 8
- 150000001768 cations Chemical class 0.000 claims 6
- 239000000178 monomer Substances 0.000 claims 5
- 239000003495 polar organic solvent Substances 0.000 claims 5
- NBVXSUQYWXRMNV-UHFFFAOYSA-N fluoromethane Chemical compound FC NBVXSUQYWXRMNV-UHFFFAOYSA-N 0.000 claims 4
- 239000004215 Carbon black (E152) Substances 0.000 claims 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims 3
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims 3
- 238000003682 fluorination reaction Methods 0.000 claims 3
- 229930195733 hydrocarbon Natural products 0.000 claims 3
- 150000002430 hydrocarbons Chemical group 0.000 claims 3
- 229920001774 Perfluoroether Polymers 0.000 claims 2
- 125000003118 aryl group Chemical group 0.000 claims 2
- 238000005341 cation exchange Methods 0.000 claims 2
- 125000005843 halogen group Chemical group 0.000 claims 2
- 229910052739 hydrogen Inorganic materials 0.000 claims 2
- ZXEKIIBDNHEJCQ-UHFFFAOYSA-N isobutanol Chemical compound CC(C)CO ZXEKIIBDNHEJCQ-UHFFFAOYSA-N 0.000 claims 2
- 239000002243 precursor Substances 0.000 claims 2
- 125000000008 (C1-C10) alkyl group Chemical group 0.000 claims 1
- RRZIJNVZMJUGTK-UHFFFAOYSA-N 1,1,2-trifluoro-2-(1,2,2-trifluoroethenoxy)ethene Chemical class FC(F)=C(F)OC(F)=C(F)F RRZIJNVZMJUGTK-UHFFFAOYSA-N 0.000 claims 1
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 1
- QYKIQEUNHZKYBP-UHFFFAOYSA-N Vinyl ether Chemical compound C=COC=C QYKIQEUNHZKYBP-UHFFFAOYSA-N 0.000 claims 1
- 238000000137 annealing Methods 0.000 claims 1
- 239000012736 aqueous medium Substances 0.000 claims 1
- 125000006615 aromatic heterocyclic group Chemical group 0.000 claims 1
- 229920001577 copolymer Polymers 0.000 claims 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims 1
- 125000001033 ether group Chemical group 0.000 claims 1
- 230000008020 evaporation Effects 0.000 claims 1
- 238000001704 evaporation Methods 0.000 claims 1
- 239000011737 fluorine Substances 0.000 claims 1
- 125000001153 fluoro group Chemical group F* 0.000 claims 1
- 125000003709 fluoroalkyl group Chemical group 0.000 claims 1
- 229920002313 fluoropolymer Polymers 0.000 claims 1
- 239000004811 fluoropolymer Substances 0.000 claims 1
- 239000001257 hydrogen Substances 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 239000003960 organic solvent Substances 0.000 claims 1
- 125000005010 perfluoroalkyl group Chemical group 0.000 claims 1
- -1 vinyl ether carboxylate Chemical class 0.000 claims 1
- 239000006185 dispersion Substances 0.000 description 5
- 0 *C(F)=C(O*)F Chemical compound *C(F)=C(O*)F 0.000 description 1
- 241000023320 Luma <angiosperm> Species 0.000 description 1
- 239000012470 diluted sample Substances 0.000 description 1
- 229920000554 ionomer Polymers 0.000 description 1
- OSWPMRLSEDHDFF-UHFFFAOYSA-N methyl salicylate Chemical compound COC(=O)C1=CC=CC=C1O OSWPMRLSEDHDFF-UHFFFAOYSA-N 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 239000004810 polytetrafluoroethylene Substances 0.000 description 1
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP09162625.9 | 2009-06-12 | ||
| EP09162625 | 2009-06-12 | ||
| PCT/EP2010/058182 WO2010142772A1 (en) | 2009-06-12 | 2010-06-10 | Fluoroionomers dispersions having low surface tension, low liquid viscosity and high solid content |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2012529549A JP2012529549A (ja) | 2012-11-22 |
| JP2012529549A5 true JP2012529549A5 (enExample) | 2014-06-26 |
| JP5575885B2 JP5575885B2 (ja) | 2014-08-20 |
Family
ID=41202555
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2012514476A Active JP5575885B2 (ja) | 2009-06-12 | 2010-06-10 | 低い表面張力、低い液体粘度および高い固体含量を有するフルオロイオノマー分散体 |
Country Status (6)
| Country | Link |
|---|---|
| US (2) | US9450262B2 (enExample) |
| EP (1) | EP2440586B1 (enExample) |
| JP (1) | JP5575885B2 (enExample) |
| KR (1) | KR101740746B1 (enExample) |
| CN (2) | CN102459361B (enExample) |
| WO (1) | WO2010142772A1 (enExample) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5409803B2 (ja) * | 2008-12-11 | 2014-02-05 | ソルヴェイ・スペシャルティ・ポリマーズ・イタリー・エッセ・ピ・ア | フルオロイオノマー組成物の精製 |
| US8709199B2 (en) * | 2011-09-13 | 2014-04-29 | GM Global Technology Operations LLC | Method of preparing a water vapor transfer membrane |
| WO2013064640A1 (en) | 2011-11-04 | 2013-05-10 | Solvicore Gmbh & Co. Kg | Method for the preparation of catalyst-coated membranes |
| US10020526B2 (en) | 2012-09-12 | 2018-07-10 | GM Global Technology Operations LLC | Reverse osmosis membranes made with PFSA ionomer and ePTFE |
| FR3001732B1 (fr) | 2013-02-04 | 2016-02-26 | Rhodia Operations | Utilisation d'agents dispersants pour la preparation d'encres pour piles a combustible |
| JP2016519398A (ja) * | 2013-04-29 | 2016-06-30 | エルジー・ケム・リミテッド | 高分子電解質膜、高分子電解質膜を含む膜電極接合体および膜電極接合体を含む燃料電池 |
| JP6151111B2 (ja) * | 2013-07-02 | 2017-06-21 | 旭化成株式会社 | 電解質溶液の製造方法、電解質溶液、電解質膜、電極触媒層、膜電極接合体、及び固体高分子電解質型燃料電池 |
| EP2842620A1 (en) | 2013-08-26 | 2015-03-04 | Agfa-Gevaert | A method for preparing a composite membrane |
| WO2020183306A1 (en) * | 2019-03-12 | 2020-09-17 | 3M Innovative Properties Company | Dispersible perfluorosulfonic acid ionomer compositions |
| US20220320558A1 (en) * | 2019-06-06 | 2022-10-06 | W. L. Gore & Associates, Inc. | Method of wetting low surface energy substrate and a system therefor |
| KR102507911B1 (ko) * | 2021-03-31 | 2023-03-07 | 도레이첨단소재 주식회사 | 양이온 교환막 및 이의 제조방법 |
Family Cites Families (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3282875A (en) * | 1964-07-22 | 1966-11-01 | Du Pont | Fluorocarbon vinyl ether polymers |
| GB1286859A (en) | 1968-11-26 | 1972-08-23 | Du Pont | Solutions of fluorinated polymers |
| US4433082A (en) * | 1981-05-01 | 1984-02-21 | E. I. Du Pont De Nemours And Company | Process for making liquid composition of perfluorinated ion exchange polymer, and product thereof |
| JPH01217042A (ja) * | 1986-09-26 | 1989-08-30 | Dow Chem Co:The | パーフルオロスルホネートイオノマー薄膜の製造方法 |
| CA2268629A1 (en) | 1996-10-15 | 1998-04-23 | E.I. Du Pont De Nemours And Company | Compositions containing particles of highly fluorinated ion exchange polymer |
| US6025092A (en) * | 1998-02-13 | 2000-02-15 | E. I. Du Pont De Nemours And Company | Fluorinated ionomers and their uses |
| US6100324A (en) * | 1998-04-16 | 2000-08-08 | E. I. Du Pont De Nemours And Company | Ionomers and ionically conductive compositions |
| IT1303779B1 (it) | 1998-11-23 | 2001-02-23 | Ausimont Spa | Preparazione di soluzioni di polimeri fluorurati solfonici. |
| WO2001060876A1 (en) | 2000-02-16 | 2001-08-23 | Daikin Industries, Ltd. | Process for producing fluoroionomer, method for purification and concentration of the ionomer, and method of film formation |
| ITMI20010921A1 (it) | 2001-05-07 | 2002-11-07 | Ausimont Spa | Polimeri (per)fluorurati amorfi |
| US6713567B2 (en) * | 2001-07-13 | 2004-03-30 | E. I. Du Pont De Nemours And Company | Method for forming fluorinated ionomers |
| WO2004078842A1 (ja) * | 2003-03-03 | 2004-09-16 | Daikin Industries Ltd. | 含フッ素ポリマー液状組成物、オルガノゾル製造方法、膜及び燃料電池 |
| CN100426575C (zh) | 2003-05-13 | 2008-10-15 | 旭硝子株式会社 | 固体高分子型燃料电池用电解质聚合物、其制造方法和膜·电极接合体 |
| EP2452955B1 (en) | 2003-09-10 | 2016-12-14 | Asahi Kasei Kabushiki Kaisha | Stabilized fluoropolymer and method for producing same |
| US6986947B2 (en) * | 2003-10-09 | 2006-01-17 | 3M Innovative Properties Company | Method of modifying a fluoropolymer and articles thereby |
| US7173067B2 (en) * | 2003-12-17 | 2007-02-06 | 3M Innovative Properties Company | Polymer electrolyte membranes crosslinked by direct fluorination |
| JP4437407B2 (ja) * | 2004-01-22 | 2010-03-24 | 旭化成株式会社 | フッ素化スルホン酸ポリマーの製造方法 |
| ITMI20040789A1 (it) | 2004-04-22 | 2004-07-22 | Solvay Solexis Spa | Membrane fluorurate |
| US20060014887A1 (en) | 2004-07-19 | 2006-01-19 | 3M Innovative Properties Company | Method of hydrolyzing a dispersion of ionic fluoropolymer |
| US7304101B2 (en) | 2004-07-19 | 2007-12-04 | 3M Innovative Properties Company | Method of purifying a dispersion of ionic fluoropolymer |
| EP2264818B1 (en) * | 2004-08-18 | 2012-05-09 | Asahi Glass Company, Limited | Electrolyte polymer for fuel cells, process for its production, electrolyte membrane and membrane/electrode assembly |
| ITMI20042554A1 (it) * | 2004-12-30 | 2005-03-30 | Solvay Solexis Spa | Procedimento per la preparazione di dispersioni di fluoropolimeri |
| US7214740B2 (en) | 2005-05-03 | 2007-05-08 | 3M Innovative Properties Company | Fluorinated ionomers with reduced amounts of carbonyl end groups |
| WO2007073500A2 (en) | 2005-12-22 | 2007-06-28 | E. I. Du Pont De Nemours And Company | Methods to prepare chemically stabilized ionomers containing inorganic fillers |
| WO2008054420A2 (en) | 2005-12-22 | 2008-05-08 | E. I. Du Pont De Nemours And Company | Chemically stabilized ionomers containing inorganic fillers |
| EP1985636B1 (en) * | 2006-02-03 | 2019-07-17 | Daikin Industries, Ltd. | Method for producing -so3h group-containing fluoropolymer |
| EP1914251A1 (en) | 2006-10-17 | 2008-04-23 | Solvay Solexis S.p.A. | Process for stabilizing fluoropolymer having ion exchange groups |
| CN101606262B (zh) | 2006-12-22 | 2013-10-02 | 索维索莱克西斯公开有限公司 | 干燥条件下操作燃料电池的方法 |
| CN101020758B (zh) * | 2007-02-25 | 2010-05-19 | 山东东岳神舟新材料有限公司 | 一种聚合物离子交换膜及其制备方法 |
-
2010
- 2010-06-10 US US13/376,641 patent/US9450262B2/en active Active
- 2010-06-10 EP EP10725124.1A patent/EP2440586B1/en active Active
- 2010-06-10 CN CN201080025899.2A patent/CN102459361B/zh active Active
- 2010-06-10 JP JP2012514476A patent/JP5575885B2/ja active Active
- 2010-06-10 CN CN201910500316.XA patent/CN110272512A/zh active Pending
- 2010-06-10 KR KR1020117030673A patent/KR101740746B1/ko active Active
- 2010-06-10 WO PCT/EP2010/058182 patent/WO2010142772A1/en not_active Ceased
-
2016
- 2016-08-16 US US15/238,385 patent/US9947952B2/en active Active
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