JP2010533113A - 多段階断熱的気相酸化による塩素の製造方法 - Google Patents

多段階断熱的気相酸化による塩素の製造方法 Download PDF

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JP2010533113A
JP2010533113A JP2010515373A JP2010515373A JP2010533113A JP 2010533113 A JP2010533113 A JP 2010533113A JP 2010515373 A JP2010515373 A JP 2010515373A JP 2010515373 A JP2010515373 A JP 2010515373A JP 2010533113 A JP2010533113 A JP 2010533113A
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catalyst
oxygen
catalyst bed
hydrogen chloride
process according
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JP2010533113A5 (enExample
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シエレン，ラルフ
シユベルト，シユテフアン
ムレツコ，レスラウ
ボルフ，アウレル
シユリユター，オリバー・フエリクス−カール
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バイエル・テクノロジー・サービシズ・ゲゼルシヤフト・ミツト・ベシユレンクテル・ハフツング
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Priority claimed from DE102007033114A external-priority patent/DE102007033114A1/de
Priority claimed from DE200710033113 external-priority patent/DE102007033113A1/de
Priority claimed from DE200710033107 external-priority patent/DE102007033107A1/de
Application filed by バイエル・テクノロジー・サービシズ・ゲゼルシヤフト・ミツト・ベシユレンクテル・ハフツング filed Critical バイエル・テクノロジー・サービシズ・ゲゼルシヤフト・ミツト・ベシユレンクテル・ハフツング
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0496—Heating or cooling the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/02—Apparatus characterised by being constructed of material selected for its chemically-resistant properties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0403—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the fluid flow within the beds being predominantly horizontal
    • B01J8/0423—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the fluid flow within the beds being predominantly horizontal through two or more otherwise shaped beds
    • B01J8/0438—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the fluid flow within the beds being predominantly horizontal through two or more otherwise shaped beds the beds being placed next to each other
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0446—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
    • B01J8/0449—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds
    • B01J8/0453—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds the beds being superimposed one above the other
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0446—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
    • B01J8/0476—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more otherwise shaped beds
    • B01J8/048—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more otherwise shaped beds the beds being superimposed one above the other
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B7/00—Halogens; Halogen acids
    • C01B7/01—Chlorine; Hydrogen chloride
    • C01B7/03—Preparation from chlorides
    • C01B7/04—Preparation of chlorine from hydrogen chloride
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212—Plates; Jackets; Cylinders
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00548—Flow
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00548—Flow
    • B01J2208/00557—Flow controlling the residence time inside the reactor vessel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00628—Controlling the composition of the reactive mixture
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/02—Processes carried out in the presence of solid particles; Reactors therefor with stationary particles
    • B01J2208/023—Details
    • B01J2208/024—Particulate material
    • B01J2208/025—Two or more types of catalyst
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/02—Apparatus characterised by their chemically-resistant properties
    • B01J2219/0204—Apparatus characterised by their chemically-resistant properties comprising coatings on the surfaces in direct contact with the reactive components
    • B01J2219/0236—Metal based
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/02—Apparatus characterised by their chemically-resistant properties
    • B01J2219/025—Apparatus characterised by their chemically-resistant properties characterised by the construction materials of the reactor vessel proper
    • B01J2219/0277—Metal based
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/02—Apparatus characterised by their chemically-resistant properties
    • B01J2219/025—Apparatus characterised by their chemically-resistant properties characterised by the construction materials of the reactor vessel proper
    • B01J2219/0277—Metal based
    • B01J2219/0286—Steel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/02—Apparatus characterised by their chemically-resistant properties
    • B01J2219/025—Apparatus characterised by their chemically-resistant properties characterised by the construction materials of the reactor vessel proper
    • B01J2219/0277—Metal based
    • B01J2219/029—Non-ferrous metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/12—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of actinides
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28—HEAT EXCHANGE IN GENERAL
    • F28D—HEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
    • F28D7/00—Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Fluid Mechanics (AREA)
  • Inorganic Chemistry (AREA)
  • Catalysts (AREA)
JP2010515373A 2007-07-13 2008-06-26 多段階断熱的気相酸化による塩素の製造方法 Withdrawn JP2010533113A (ja)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
DE102007033114A DE102007033114A1 (de) 2007-07-13 2007-07-13 Verfahren zur Herstellung von Chlor durch Gasphasenoxidation von Chlorwasserstoff
DE200710033113 DE102007033113A1 (de) 2007-07-13 2007-07-13 Temperaturstabiler Katalysator für die Chlorwasserstoffgasphasenoxidation
DE200710033107 DE102007033107A1 (de) 2007-07-13 2007-07-13 Verfahren zur Herstellung von Chlor durch vielstufige adiabatische Gasphasenoxidation
PCT/EP2008/005184 WO2009010168A1 (de) 2007-07-13 2008-06-26 Verfahren zur herstellung von chlor durch vielstufige adiabatische gasphasenoxidation

Publications (2)

Publication Number Publication Date
JP2010533113A true JP2010533113A (ja) 2010-10-21
JP2010533113A5 JP2010533113A5 (enExample) 2011-07-14

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JP2010515373A Withdrawn JP2010533113A (ja) 2007-07-13 2008-06-26 多段階断熱的気相酸化による塩素の製造方法

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Country Link
US (1) US20100260660A1 (enExample)
EP (1) EP2170495A1 (enExample)
JP (1) JP2010533113A (enExample)
CN (1) CN101687160A (enExample)
WO (1) WO2009010168A1 (enExample)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2011184280A (ja) * 2010-03-11 2011-09-22 Sumitomo Chemical Co Ltd 固定床反応器による塩素の製造方法
JP2014516315A (ja) * 2011-08-17 2014-07-10 アレヴァ ゲゼルシャフト ミット ベシュレンクテル ハフツング 酸化ウラン触媒体の製造方法
WO2021137400A1 (ko) 2019-12-31 2021-07-08 한화솔루션 주식회사 염화수소 산화반응용 성형촉매 및 이의 제조방법
JP2024515354A (ja) * 2021-04-21 2024-04-09 ベーアーエスエフ・エスエー 塩素を調製するためのプロセス

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DE102008050975A1 (de) * 2008-10-09 2010-04-15 Bayer Technology Services Gmbh Mehrstufiges Verfahren zur Herstellung von Chlor
DE102009021675A1 (de) * 2009-05-16 2010-11-18 Bayer Technology Services Gmbh Verfahren zur Herstellung von Chlor durch Gasphasenoxidation von Chlorwasserstoff in Gegenwart eines Ceroxid-Katalysators
DE102009033640A1 (de) * 2009-07-17 2011-03-03 Bayer Technology Services Gmbh Verfahren zur Herstellung von Chlor durch Gasphasenoxidation von Chlorwasserstoff in Anwesenheit von Schwefeloxiden
CN103796949A (zh) * 2011-07-05 2014-05-14 拜耳知识产权有限责任公司 在绝热反应级联中使用氧化铈催化剂制备氯气的方法
CN104437268B (zh) * 2014-11-06 2017-07-14 南京大学 多级并联强化固定床反应器及其使用方法
CN104591090B (zh) 2014-12-22 2016-09-07 上海方纶新材料科技有限公司 一种氯化氢催化氧化制备氯气的方法
CN105776141B (zh) * 2016-01-27 2018-03-09 烟台大学 一种氯化氢催化氧化制氯气新型固定床反应器
JP2020019687A (ja) * 2018-08-02 2020-02-06 住友化学株式会社 臭素の製造方法
WO2023094364A1 (en) * 2021-11-23 2023-06-01 Basf Se Process for preparing a gas stream comprising chlorine
CN117599689A (zh) * 2023-11-30 2024-02-27 上海交通大学 一种HCl高效转化为Cl2的方法及反应装置
CN119386781A (zh) * 2025-01-06 2025-02-07 西北民族大学 一种氯化氢制氯气的多级催化氧化反应器

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CA1260229A (en) * 1986-06-30 1989-09-26 Mitsui Chemicals, Inc. Production process of chlorine
CN1150127C (zh) * 1996-08-08 2004-05-19 住友化学工业株式会社 氯的生产方法
CN1182717A (zh) * 1996-10-31 1998-05-27 住友化学工业株式会社 氯气的生产方法
AU3073400A (en) * 1999-01-22 2000-08-07 Sumitomo Chemical Company, Limited Method for producing chlorine
EP1251951B2 (en) * 2000-01-25 2014-10-29 Meggitt (U.K.) Limited Chemical reactor with heat exchanger
US7033553B2 (en) * 2000-01-25 2006-04-25 Meggitt (Uk) Limited Chemical reactor
DE10235476A1 (de) * 2002-08-02 2004-02-12 Basf Ag Integriertes Verfahren zur Herstellung von Isocyanaten
DE10250131A1 (de) * 2002-10-28 2004-05-06 Basf Ag Verfahren zur Herstellung von Chlor aus Salzsäure
DE10258153A1 (de) * 2002-12-12 2004-06-24 Basf Ag Verfahren zur Herstellung von Chlor durch Gasphasenoxidation von Chlorwasserstoff
DE10361519A1 (de) * 2003-12-23 2005-07-28 Basf Ag Verfahren zur Herstellung von Chlor durch Gasphasenoxidation von Chlorwasserstoff
DE102004006610A1 (de) * 2004-02-11 2005-09-01 Basf Ag Reaktor und Verfahren zur Herstellung von Chlor aus HCI
US7772447B2 (en) * 2004-12-22 2010-08-10 Exxonmobil Chemical Patents Inc. Production of liquid hydrocarbons from methane
DE102007020140A1 (de) * 2006-05-23 2007-11-29 Bayer Materialscience Ag Verfahren zur Herstellung von Chlor durch Gasphasenoxidation

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2011184280A (ja) * 2010-03-11 2011-09-22 Sumitomo Chemical Co Ltd 固定床反応器による塩素の製造方法
JP2014516315A (ja) * 2011-08-17 2014-07-10 アレヴァ ゲゼルシャフト ミット ベシュレンクテル ハフツング 酸化ウラン触媒体の製造方法
WO2021137400A1 (ko) 2019-12-31 2021-07-08 한화솔루션 주식회사 염화수소 산화반응용 성형촉매 및 이의 제조방법
KR20210086140A (ko) 2019-12-31 2021-07-08 한화솔루션 주식회사 염화수소 산화반응용 성형촉매 및 이의 제조방법
US12472486B2 (en) 2019-12-31 2025-11-18 Hanwha Solutions Corporation Molding catalyst for hydrogen chloride oxidation reaction, and method for producing same
JP2024515354A (ja) * 2021-04-21 2024-04-09 ベーアーエスエフ・エスエー 塩素を調製するためのプロセス

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EP2170495A1 (de) 2010-04-07
CN101687160A (zh) 2010-03-31
WO2009010168A1 (de) 2009-01-22
US20100260660A1 (en) 2010-10-14

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