JP2010509491A5 - - Google Patents
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- Publication number
- JP2010509491A5 JP2010509491A5 JP2009537318A JP2009537318A JP2010509491A5 JP 2010509491 A5 JP2010509491 A5 JP 2010509491A5 JP 2009537318 A JP2009537318 A JP 2009537318A JP 2009537318 A JP2009537318 A JP 2009537318A JP 2010509491 A5 JP2010509491 A5 JP 2010509491A5
- Authority
- JP
- Japan
- Prior art keywords
- film
- chitosan
- pvoh
- bisulfite
- weight
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 13
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 13
- 235000019422 polyvinyl alcohol Nutrition 0.000 claims description 13
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims description 6
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims description 6
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims description 6
- 239000004327 boric acid Substances 0.000 claims description 6
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 6
- 239000004971 Cross linker Substances 0.000 claims description 5
- 239000003431 cross linking reagent Substances 0.000 claims description 5
- 239000004014 plasticizer Substances 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- DWAQJAXMDSEUJJ-UHFFFAOYSA-M Sodium bisulfite Chemical compound [Na+].OS([O-])=O DWAQJAXMDSEUJJ-UHFFFAOYSA-M 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 235000010267 sodium hydrogen sulphite Nutrition 0.000 claims description 3
- BTBUEUYNUDRHOZ-UHFFFAOYSA-N Borate Chemical compound [O-]B([O-])[O-] BTBUEUYNUDRHOZ-UHFFFAOYSA-N 0.000 claims description 2
- 239000004606 Fillers/Extenders Substances 0.000 claims description 2
- KDYFGRWQOYBRFD-UHFFFAOYSA-N Succinic acid Natural products OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 claims description 2
- 239000003963 antioxidant agent Substances 0.000 claims description 2
- 229910021538 borax Inorganic materials 0.000 claims description 2
- KDYFGRWQOYBRFD-NUQCWPJISA-N butanedioic acid Chemical compound O[14C](=O)CC[14C](O)=O KDYFGRWQOYBRFD-NUQCWPJISA-N 0.000 claims description 2
- 239000000314 lubricant Substances 0.000 claims description 2
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 claims description 2
- 239000011976 maleic acid Substances 0.000 claims description 2
- 235000006408 oxalic acid Nutrition 0.000 claims description 2
- 150000003839 salts Chemical class 0.000 claims description 2
- 239000004328 sodium tetraborate Substances 0.000 claims description 2
- 235000010339 sodium tetraborate Nutrition 0.000 claims description 2
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 claims description 2
- 229920001661 Chitosan Polymers 0.000 claims 11
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 claims 7
- 229910052783 alkali metal Inorganic materials 0.000 claims 7
- 150000001340 alkali metals Chemical class 0.000 claims 7
- 150000003863 ammonium salts Chemical class 0.000 claims 7
- WBZKQQHYRPRKNJ-UHFFFAOYSA-L disulfite Chemical compound [O-]S(=O)S([O-])(=O)=O WBZKQQHYRPRKNJ-UHFFFAOYSA-L 0.000 claims 7
- 238000000034 method Methods 0.000 claims 5
- 239000000243 solution Substances 0.000 claims 4
- 230000021736 acetylation Effects 0.000 claims 3
- 238000006640 acetylation reaction Methods 0.000 claims 3
- 230000007062 hydrolysis Effects 0.000 claims 3
- 238000006460 hydrolysis reaction Methods 0.000 claims 3
- 229920000642 polymer Polymers 0.000 claims 3
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims 2
- 239000007864 aqueous solution Substances 0.000 claims 2
- 239000002002 slurry Substances 0.000 claims 2
- 238000005266 casting Methods 0.000 claims 1
- 238000001704 evaporation Methods 0.000 claims 1
- 235000011187 glycerol Nutrition 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 230000003381 solubilizing effect Effects 0.000 claims 1
- 239000002904 solvent Substances 0.000 claims 1
- 238000003756 stirring Methods 0.000 claims 1
- 239000004094 surface-active agent Substances 0.000 claims 1
- 229920003169 water-soluble polymer Polymers 0.000 claims 1
- 239000003795 chemical substances by application Substances 0.000 description 6
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 1
- 239000004952 Polyamide Substances 0.000 description 1
- 239000002518 antifoaming agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 239000007844 bleaching agent Substances 0.000 description 1
- 239000002981 blocking agent Substances 0.000 description 1
- GUJOJGAPFQRJSV-UHFFFAOYSA-N dialuminum;dioxosilane;oxygen(2-);hydrate Chemical compound O.[O-2].[O-2].[O-2].[Al+3].[Al+3].O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O GUJOJGAPFQRJSV-UHFFFAOYSA-N 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000002105 nanoparticle Substances 0.000 description 1
- 229920002647 polyamide Polymers 0.000 description 1
Applications Claiming Priority (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US11/559,262 | 2006-11-13 | ||
| US11/559,262 US20080110370A1 (en) | 2006-11-13 | 2006-11-13 | Water-soluble film |
| US88583807P | 2007-01-19 | 2007-01-19 | |
| US60/885,838 | 2007-01-19 | ||
| US11/733,595 US20080176985A1 (en) | 2006-11-13 | 2007-04-10 | Water-soluble film |
| US11/733,595 | 2007-04-10 | ||
| PCT/US2007/084566 WO2008064014A2 (en) | 2006-11-13 | 2007-11-13 | Water-soluble film |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2014137515A Division JP2014177654A (ja) | 2006-11-13 | 2014-07-03 | 水溶性フィルム |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2010509491A JP2010509491A (ja) | 2010-03-25 |
| JP2010509491A5 true JP2010509491A5 (enExample) | 2010-12-24 |
| JP5620105B2 JP5620105B2 (ja) | 2014-11-05 |
Family
ID=39273096
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2009537318A Expired - Fee Related JP5620105B2 (ja) | 2006-11-13 | 2007-11-13 | 水溶性フィルム |
| JP2014137515A Abandoned JP2014177654A (ja) | 2006-11-13 | 2014-07-03 | 水溶性フィルム |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2014137515A Abandoned JP2014177654A (ja) | 2006-11-13 | 2014-07-03 | 水溶性フィルム |
Country Status (6)
| Country | Link |
|---|---|
| US (2) | US20080176985A1 (enExample) |
| EP (1) | EP2087028B1 (enExample) |
| JP (2) | JP5620105B2 (enExample) |
| CA (1) | CA2669397C (enExample) |
| PL (1) | PL2087028T3 (enExample) |
| WO (1) | WO2008064014A2 (enExample) |
Families Citing this family (58)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2011511123A (ja) * | 2008-01-31 | 2011-04-07 | ザ プロクター アンド ギャンブル カンパニー | キトサンのアセチル化 |
| RU2555042C2 (ru) | 2010-07-02 | 2015-07-10 | Дзе Проктер Энд Гэмбл Компани | Способ доставки активнодействующего вещества |
| WO2012003319A2 (en) | 2010-07-02 | 2012-01-05 | The Procter & Gamble Company | Filaments comprising an active agent nonwoven webs and methods for making same |
| US20180163325A1 (en) | 2016-12-09 | 2018-06-14 | Robert Wayne Glenn, Jr. | Dissolvable fibrous web structure article comprising active agents |
| EP3533908A1 (en) | 2010-07-02 | 2019-09-04 | The Procter & Gamble Company | Nonwoven web comprising one or more active agents |
| CA2803371C (en) | 2010-07-02 | 2016-04-19 | The Procter & Gamble Company | Process for making films from nonwoven webs |
| US10087401B2 (en) | 2012-03-16 | 2018-10-02 | Monosol, Llc | Water soluble compositions incorporating enzymes, and method of making same |
| US9394092B2 (en) | 2012-04-16 | 2016-07-19 | Monosol, Llc | Powdered pouch and method of making same |
| US10829621B2 (en) | 2013-01-11 | 2020-11-10 | Monosol, Llc | Edible water-soluble film |
| US10144837B2 (en) | 2014-05-06 | 2018-12-04 | Basf Coatings Gmbh | Method for delivering aluminum into waterborne tint base or paint and refinish mixer system |
| JP5781676B1 (ja) | 2014-09-12 | 2015-09-24 | 株式会社アイセロ | 水溶性フィルム、包装袋、内容物放出体、及び水溶性フィルムの製造方法 |
| CA3078064C (en) | 2014-10-13 | 2022-12-13 | Monosol, Llc. | Water-soluble polyvinyl alchool blend film, related methods, and related articles |
| AU2015333790A1 (en) | 2014-10-13 | 2017-04-20 | The Procter & Gamble Company | Articles comprising water-soluble polyvinyl alcohol blend film and related methods |
| TWI689547B (zh) | 2014-10-13 | 2020-04-01 | 美商摩諾索公司 | 具有塑化劑摻合物的水溶性聚乙烯醇膜、相關方法及相關物品 |
| EP3207084B1 (en) * | 2014-10-13 | 2021-01-27 | The Procter and Gamble Company | Articles comprising water-soluble polyvinyl alcohol film with plasticizer blend and related methods |
| TWI677525B (zh) | 2014-10-13 | 2019-11-21 | 美商摩諾索公司 | 水溶性聚乙烯醇摻合物膜、相關方法及相關物品 |
| CN104744716B (zh) * | 2015-04-03 | 2018-03-09 | 广州康华微创生物科技有限公司 | 一种壳聚糖与改性聚乙烯醇复合膜的制备方法 |
| DE102015213943A1 (de) * | 2015-07-23 | 2017-01-26 | Henkel Ag & Co. Kgaa | Wasch- oder Reinigungsmittel umfassend wenigstens zwei Phasen |
| JP6992253B2 (ja) * | 2015-09-11 | 2022-01-13 | 三菱ケミカル株式会社 | 水溶性フィルム及び薬剤包装体 |
| KR102516145B1 (ko) | 2015-09-11 | 2023-03-30 | 미쯔비시 케미컬 주식회사 | 수용성 필름, 약제 포장체 및 수용성 필름의 제조 방법 |
| US10414889B2 (en) | 2015-09-11 | 2019-09-17 | Mitsubishi Chemical Corporation | Water-soluble film and chemical agent package |
| JP7035313B2 (ja) * | 2015-09-11 | 2022-03-15 | 三菱ケミカル株式会社 | 水溶性フィルム及び薬剤包装体 |
| JPWO2017043514A1 (ja) * | 2015-09-11 | 2018-06-21 | 日本合成化学工業株式会社 | フィルムロール及び薬剤包装体 |
| JP6888256B2 (ja) * | 2015-11-12 | 2021-06-16 | 三菱ケミカル株式会社 | 水溶性フィルム及び薬剤包装体 |
| JP6888257B2 (ja) * | 2015-12-22 | 2021-06-16 | 三菱ケミカル株式会社 | 水溶性フィルム及び薬剤包装体 |
| FR3049605B1 (fr) * | 2016-04-05 | 2018-03-23 | Arkema France | Procede d'obtention de films fins et articles filmogenes |
| US11767405B2 (en) | 2016-04-13 | 2023-09-26 | Monosol, Llc | Water soluble film, packets employing the film, and methods of making and using same |
| DE102016004464A1 (de) | 2016-04-15 | 2017-10-19 | Martin-Luther-Universität Halle-Wittenberg | Verpackung von Milch in auflösbaren Portionskapseln und Verfahren zu deren Herstellung duch lonen-Hydrokolloid-lnteraktionen |
| DE102016004463B4 (de) | 2016-04-15 | 2018-03-08 | Martin-Luther-Universität Halle-Wittenberg | Verpackung von Milch in auflösbaren Portionskapseln und Verfahren zu deren Herstellung durch Kristallisation |
| US10443024B2 (en) | 2016-06-13 | 2019-10-15 | Monosol, Llc | Water-soluble unit dose articles made from a combination of different films |
| EP3469059B1 (en) | 2016-06-13 | 2024-08-07 | The Procter & Gamble Company | Water-soluble unit dose articles made from a combination of different films and containing household care compositions |
| CN109312277B (zh) | 2016-06-13 | 2021-10-15 | 蒙诺苏尔有限公司 | 提高水溶性单位剂量制品的密封强度的第一薄膜和第二薄膜的用途 |
| EP3469060A1 (en) | 2016-06-13 | 2019-04-17 | The Procter & Gamble Company | Water-soluble unit dose articles made from a combination of different films and containing household care compositions |
| CA3001552A1 (en) | 2016-06-13 | 2017-12-21 | Monosol, Llc | Water-soluble packets |
| CA3023508A1 (en) | 2016-06-13 | 2017-12-21 | The Procter & Gamble Company | Water-soluble unit dose articles made from a combination of different films and containing household care compositions |
| MX380727B (es) | 2017-01-27 | 2025-03-12 | Procter & Gamble | Composiciones en la forma de estructuras sólidas solubles que comprenden partículas aglomeradas efervescentes. |
| JP6923673B2 (ja) | 2017-05-16 | 2021-08-25 | ザ プロクター アンド ギャンブル カンパニーＴｈｅ Ｐｒｏｃｔｅｒ ＆ Ｇａｍｂｌｅ Ｃｏｍｐａｎｙ | 溶解性固形構造体の形態のコンディショニングヘアケア組成物 |
| CN111492047A (zh) | 2018-01-26 | 2020-08-04 | 宝洁公司 | 水溶性制品以及相关方法 |
| KR20200086739A (ko) | 2018-01-26 | 2020-07-17 | 더 프록터 앤드 갬블 캄파니 | 효소를 포함하는 수용성 단위 용량 물품 |
| CA3087583C (en) | 2018-01-26 | 2024-01-09 | The Procter & Gamble Company | Water-soluble unit dose articles comprising perfume |
| WO2019147532A1 (en) | 2018-01-26 | 2019-08-01 | The Procter & Gamble Company | Water-soluble unit dose articles comprising perfume |
| WO2019168829A1 (en) | 2018-02-27 | 2019-09-06 | The Procter & Gamble Company | A consumer product comprising a flat package containing unit dose articles |
| CA3098544A1 (en) | 2018-05-02 | 2019-11-07 | Monosol, Llc | Water-soluble polyvinyl alcohol blend film, related methods, and related articles |
| US10982176B2 (en) | 2018-07-27 | 2021-04-20 | The Procter & Gamble Company | Process of laundering fabrics using a water-soluble unit dose article |
| US11666514B2 (en) | 2018-09-21 | 2023-06-06 | The Procter & Gamble Company | Fibrous structures containing polymer matrix particles with perfume ingredients |
| US12234431B2 (en) | 2018-10-03 | 2025-02-25 | The Procter & Gamble Company | Water-soluble unit dose articles comprising water-soluble fibrous structures and particles |
| CN113748195B (zh) | 2019-01-28 | 2024-01-19 | 宝洁公司 | 可回收利用的、可再生的或可生物降解的包装 |
| US12031254B2 (en) | 2019-03-19 | 2024-07-09 | The Procter & Gamble Company | Process of reducing malodors on fabrics |
| EP3712237A1 (en) | 2019-03-19 | 2020-09-23 | The Procter & Gamble Company | Fibrous water-soluble unit dose articles comprising water-soluble fibrous structures |
| EP3989913A1 (en) | 2019-06-28 | 2022-05-04 | The Procter & Gamble Company | Dissolvable solid fibrous articles containing anionic surfactants |
| CN110790885B (zh) * | 2019-08-30 | 2022-05-03 | 武汉理工大学 | 一种聚乙烯醇/壳聚糖季铵盐抗菌自愈水凝胶及其制备方法和应用 |
| CA3172321A1 (en) | 2020-05-01 | 2021-11-04 | Farzaneh REZAEI | Stable liquid formulations for nitrogen-fixing microorganisms |
| MX2023001042A (es) | 2020-07-31 | 2023-02-16 | Procter & Gamble | Bolsa fibrosa soluble en agua que contiene granulos para el cuidado del cabello. |
| CN114867834A (zh) | 2020-08-19 | 2022-08-05 | 宝洁公司 | 含有直接添加的微胶囊的柔性多孔可溶性固体片材制品及其制备方法 |
| EP4001385A1 (en) * | 2020-11-17 | 2022-05-25 | The Procter & Gamble Company | Automatic dishwashing composition |
| US12403083B2 (en) | 2021-08-30 | 2025-09-02 | The Procter & Gamble Company | Dissolvable solid structure comprising first and second polymeric structurants |
| WO2023072457A1 (en) * | 2021-10-25 | 2023-05-04 | Unilever Ip Holdings B.V. | Films and capsules |
| US20250145544A1 (en) | 2022-02-09 | 2025-05-08 | Pivot Bio, Inc. | Dry formulated nitrogen-fixing microbe packaged in water-soluble film for rapid and safe dispersal in aqueous mixtures |
Family Cites Families (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3692725A (en) * | 1970-10-28 | 1972-09-19 | Kimberly Clark Co | Stabilized binder for water-flushable non-woven webs |
| US4801636A (en) * | 1987-03-24 | 1989-01-31 | The Clorox Company | Rinse soluble polymer film composition for wash additives |
| JP2662901B2 (ja) | 1990-12-19 | 1997-10-15 | 大日精化工業株式会社 | 風合い改良剤組成物 |
| JP3195817B2 (ja) | 1992-01-17 | 2001-08-06 | 株式会社クラレ | 耐水性組成物 |
| KR0159976B1 (ko) | 1994-06-21 | 1999-01-15 | 전동원 | 생분해성 키토산/셀룰로즈 복합체 필름의 제조방법 |
| JP3609898B2 (ja) * | 1996-06-03 | 2005-01-12 | 株式会社クラレ | 薬剤包装用水溶性フィルム |
| DE19636510A1 (de) * | 1996-09-09 | 1998-03-12 | Clariant Gmbh | Polyvinylalkohol-Kompositionen |
| CA2338710C (en) * | 1998-07-29 | 2009-10-27 | Guido Waeschenbach | A tablet comprising a basic composition and particle comprising core and envelope |
| EP1019486A1 (de) * | 1998-07-29 | 2000-07-19 | Benckiser N.V. | Zusammensetzung zur verwendung in einer waschmaschine |
| JP2002530479A (ja) * | 1998-11-13 | 2002-09-17 | ジェネンコア インターナショナル インコーポレーテッド | 流動床による低密度顆粒 |
| GB2365018A (en) | 2000-07-24 | 2002-02-13 | Procter & Gamble | Water soluble pouches |
| MXPA03010366A (es) * | 2001-05-14 | 2004-03-16 | Procter & Gamble | Producto limpiador. |
| GB0114847D0 (en) | 2001-06-18 | 2001-08-08 | Unilever Plc | Water soluble package and liquid contents thereof |
| GB0114850D0 (en) | 2001-06-18 | 2001-08-08 | Unilever Plc | Water soluble package and liquid contents thereof |
| JP3917435B2 (ja) * | 2002-02-12 | 2007-05-23 | 大日精化工業株式会社 | 水性溶液組成物 |
| KR20040012487A (ko) * | 2002-07-31 | 2004-02-11 | 롬 앤드 하스 캄파니 | 트리거드 반응 조성물 |
| GB0222964D0 (en) | 2002-10-03 | 2002-11-13 | Unilever Plc | Polymeric film for water soluble package |
| JP4056859B2 (ja) * | 2002-11-11 | 2008-03-05 | 日本合成化学工業株式会社 | 水溶性フィルム |
| DE60319347T2 (de) * | 2003-05-23 | 2009-02-19 | The Procter & Gamble Company, Cincinnati | Waschmittelzusammensetzung zum Gebrauch in einer Textilwasch- oder Geschirrspülmaschine |
| JP4630396B2 (ja) * | 2003-12-16 | 2011-02-09 | 日本合成化学工業株式会社 | 水溶性フィルム |
| CN1906612A (zh) * | 2004-01-19 | 2007-01-31 | 奈杰尔·汉密尔顿 | 用于记录通信网络中跨一个或多个搜索引擎的搜索轨迹的方法和系统 |
| JP4222280B2 (ja) | 2004-09-16 | 2009-02-12 | ヤマハ株式会社 | 演奏情報出力装置及び楽器及び演奏情報を出力するための方法及び該方法をコンピュータで実行するためのプログラム。 |
| US8728449B2 (en) * | 2005-01-22 | 2014-05-20 | Monosol Llc | Water-soluble film article having salt layer, and method of making the same |
| ATE481444T1 (de) * | 2005-05-13 | 2010-10-15 | Procter & Gamble | Funktionalisierte folien |
| EP2079825A2 (en) * | 2006-11-13 | 2009-07-22 | The Procter and Gamble Company | Water-soluble detergent pouch |
-
2007
- 2007-04-10 US US11/733,595 patent/US20080176985A1/en not_active Abandoned
- 2007-11-13 WO PCT/US2007/084566 patent/WO2008064014A2/en not_active Ceased
- 2007-11-13 PL PL07854627T patent/PL2087028T3/pl unknown
- 2007-11-13 CA CA2669397A patent/CA2669397C/en not_active Expired - Fee Related
- 2007-11-13 JP JP2009537318A patent/JP5620105B2/ja not_active Expired - Fee Related
- 2007-11-13 EP EP07854627.2A patent/EP2087028B1/en active Active
- 2007-11-13 US US12/513,024 patent/US8268914B2/en active Active
-
2014
- 2014-07-03 JP JP2014137515A patent/JP2014177654A/ja not_active Abandoned
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