JP2009524630A5 - - Google Patents
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- Publication number
- JP2009524630A5 JP2009524630A5 JP2008551845A JP2008551845A JP2009524630A5 JP 2009524630 A5 JP2009524630 A5 JP 2009524630A5 JP 2008551845 A JP2008551845 A JP 2008551845A JP 2008551845 A JP2008551845 A JP 2008551845A JP 2009524630 A5 JP2009524630 A5 JP 2009524630A5
- Authority
- JP
- Japan
- Prior art keywords
- propylene
- acrolein
- reaction
- glycerin
- oxidation reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 29
- HGINCPLSRVDWNT-UHFFFAOYSA-N Acrolein Chemical compound C=CC=O HGINCPLSRVDWNT-UHFFFAOYSA-N 0.000 claims description 16
- 235000011187 glycerol Nutrition 0.000 claims description 12
- 238000007254 oxidation reaction Methods 0.000 claims description 10
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 claims description 10
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 claims description 10
- 230000003197 catalytic effect Effects 0.000 claims description 6
- 239000007864 aqueous solution Substances 0.000 claims description 4
- 238000006243 chemical reaction Methods 0.000 claims description 4
- 230000018044 dehydration Effects 0.000 claims description 3
- 238000006297 dehydration reaction Methods 0.000 claims description 3
- 238000011144 upstream manufacturing Methods 0.000 claims description 3
- 238000000034 method Methods 0.000 claims 5
- 239000007789 gas Substances 0.000 claims 3
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims 2
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims 2
- 230000003647 oxidation Effects 0.000 claims 2
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 claims 1
- 239000003054 catalyst Substances 0.000 claims 1
- 229910001882 dioxygen Inorganic materials 0.000 claims 1
- 239000007788 liquid Substances 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 239000000203 mixture Substances 0.000 claims 1
- JOLPFRQHFARWCF-UHFFFAOYSA-N propane-1,2,3-triol;prop-1-ene Chemical group CC=C.OCC(O)CO JOLPFRQHFARWCF-UHFFFAOYSA-N 0.000 claims 1
- 239000000243 solution Substances 0.000 description 2
- RBNPOMFGQQGHHO-UHFFFAOYSA-N glyceric acid Chemical compound OCC(O)C(O)=O RBNPOMFGQQGHHO-UHFFFAOYSA-N 0.000 description 1
- 239000012495 reaction gas Substances 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR0601061A FR2897059B1 (fr) | 2006-02-07 | 2006-02-07 | Procede de preparation d'acide acrylique |
| FR0601061 | 2006-02-07 | ||
| PCT/FR2007/050758 WO2007090991A2 (fr) | 2006-02-07 | 2007-02-06 | Procede de preparation d'acide acrylique |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2009524630A JP2009524630A (ja) | 2009-07-02 |
| JP2009524630A5 true JP2009524630A5 (enExample) | 2011-10-20 |
| JP5097128B2 JP5097128B2 (ja) | 2012-12-12 |
Family
ID=37075914
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2008551845A Expired - Fee Related JP5097128B2 (ja) | 2006-02-07 | 2007-02-06 | アクリル酸の製法方法 |
Country Status (16)
| Country | Link |
|---|---|
| US (1) | US7880034B2 (enExample) |
| EP (1) | EP1981835B1 (enExample) |
| JP (1) | JP5097128B2 (enExample) |
| KR (1) | KR101004593B1 (enExample) |
| CN (1) | CN101400639B (enExample) |
| AT (1) | ATE430724T1 (enExample) |
| BR (1) | BRPI0707533A2 (enExample) |
| DE (1) | DE602007001072D1 (enExample) |
| ES (1) | ES2325695T3 (enExample) |
| FR (1) | FR2897059B1 (enExample) |
| MY (1) | MY139630A (enExample) |
| PL (1) | PL1981835T3 (enExample) |
| PT (1) | PT1981835E (enExample) |
| RU (1) | RU2397156C2 (enExample) |
| WO (1) | WO2007090991A2 (enExample) |
| ZA (1) | ZA200806644B (enExample) |
Families Citing this family (28)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2920767B1 (fr) * | 2007-09-06 | 2009-12-18 | Arkema France | Procede de vaporisation reactive de glycerol |
| FR2934261B1 (fr) * | 2008-07-25 | 2015-04-10 | Arkema France | Procede de synthese d'esters de l'acide acrylique |
| WO2010012586A1 (de) | 2008-07-28 | 2010-02-04 | Basf Se | Verfahren zur auftrennung von in einem produktgasgemisch einer partiellen heterogen katalysierten gasphasenoxidation einer c3-vorläuferverbindung der acrylsäure als hauptbestandteil enthaltener acrylsäure und als nebenprodukt enthaltenem glyoxal |
| DE102008040799A1 (de) | 2008-07-28 | 2008-12-11 | Basf Se | Verfahren zur Auftrennung von in einem Produktgasgemisch einer partiellen heterogen katalysierten Gasphasenoxidation einer C3-Vorläuferverbindung der Acrylsäure als Hauptbestandteil enthaltener Acrylsäure und als Nebenprodukt enthaltenem Glyoxal |
| DE102008041573A1 (de) | 2008-08-26 | 2010-03-04 | Basf Se | Verfahren zur Auftrennung von in einem Produktgasgemisch einer partiellen heterogen katalysierten Gasphasenoxidation einer C3-Vorläuferverbindung der Acrylsäure als Hauptbestandteil enhaltener Acrylsäure und als Nebenprodukt enthaltenem Glyoxal |
| JP5305827B2 (ja) * | 2008-10-17 | 2013-10-02 | 株式会社日本触媒 | アクロレイン及びアクリル酸の製造方法 |
| FR2943351B1 (fr) * | 2009-03-18 | 2011-04-29 | Arkema France | Agent de mise en oeuvre acrylique |
| US8105971B2 (en) * | 2009-04-02 | 2012-01-31 | Lummus Technology Inc. | Process for making catalysts useful for the conversion of paraffins to olefins |
| WO2011000808A2 (de) | 2009-07-01 | 2011-01-06 | Basf Se | Verfahren der abtrennung von acrylsäure aus dem produktgasgemisch einer heterogen katalysierten partiellen gasphasenoxidation wenigstens einer c3-vorläuferverbindung |
| DE102010001228A1 (de) | 2010-01-26 | 2011-02-17 | Basf Se | Verfahren der Abtrennung von Acrylsäure aus dem Produktgasgemisch einer heterogen katalysierten partiellen Gasphasenoxidation wenigstens einer C3-Vorläuferverbindung |
| DE102009027401A1 (de) | 2009-07-01 | 2010-02-18 | Basf Se | Verfahren der Abtrennung von Acrylsäure aus dem Produktgasgemisch einer heterogen katalysierten partiellen Gasphasenoxidation wenigstens einer C3-Vorläuferverbindung |
| FR2948365B1 (fr) * | 2009-07-22 | 2011-09-09 | Arkema France | Procede de fabrication d'acide acrylique bio-ressource a partir de glycerol |
| SG179188A1 (en) | 2009-09-18 | 2012-04-27 | Nippon Kayaku Kk | Catalyst and process for preparing acrolein and/or acrylic acid by dehydration reaction of glycerin |
| FR2958185B1 (fr) * | 2010-03-30 | 2012-04-20 | Arkema France | Procede d'oxydation selective de monoxyde de carbone |
| WO2012010923A1 (en) | 2010-07-19 | 2012-01-26 | Arkema France | Process for manufacturing acrolein from glycerol |
| DE102010040921A1 (de) * | 2010-09-16 | 2012-03-22 | Basf Se | Verfahren zur Herstellung von Acrylsäure aus Methanol und Essigsäure |
| DE102010040923A1 (de) * | 2010-09-16 | 2012-03-22 | Basf Se | Verfahren zur Herstellung von Acrylsäure aus Ethanol und Formaldehyd |
| DE102010042216A1 (de) | 2010-10-08 | 2011-06-09 | Basf Se | Verfahren zur Hemmung der unerwünschten radikalischen Polymerisation von in einer flüssigen Phase P befindlicher Acrylsäure |
| DE102011076931A1 (de) | 2011-06-03 | 2012-12-06 | Basf Se | Wässrige Lösung, enthaltend Acrylsäure und deren konjugierte Base |
| WO2013008279A1 (en) | 2011-07-14 | 2013-01-17 | Nippon Kayaku Kabushiki Kaisha | Process for preparing catalyst used in production of acrolein and/or acrylic acid and process for preparing acrolein and/or acrylic acid by dehydration reaction of glycerin |
| WO2013017904A1 (en) | 2011-07-29 | 2013-02-07 | Arkema France | Improved process of dehydration reactions |
| FR2989684B1 (fr) * | 2012-04-18 | 2014-10-31 | Arkema France | Procede de fabrication d'acroleine et/ou d'acide acrylique a partir de glycerol |
| US9440903B2 (en) * | 2012-09-24 | 2016-09-13 | Arkema Inc. | Shell and tube oxidation reactor with improved resistance to fouling |
| EP3004041B1 (de) * | 2013-06-03 | 2020-05-06 | Evonik Operations GmbH | Verfahren zur herstellung von acrolein |
| WO2017025391A1 (en) | 2015-08-07 | 2017-02-16 | Basf Se | Process for production of acrylic acid |
| KR102044428B1 (ko) | 2015-12-23 | 2019-12-02 | 주식회사 엘지화학 | 글리세린으로부터 아크릴산의 제조방법 |
| WO2020020697A1 (de) | 2018-07-26 | 2020-01-30 | Basf Se | Verfahren zur hemmung der unerwünschten radikalischen polymerisation von in einer flüssigen phase p befindlicher acrylsäure |
| JP7651589B2 (ja) | 2020-03-26 | 2025-03-26 | ベーアーエスエフ・エスエー | 液相ｐに存在するアクリル酸の望ましくないフリーラジカル重合を抑制する方法 |
Family Cites Families (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR695931A (fr) | 1929-06-15 | 1930-12-23 | Schering Kahlbaum Ag | Procédé de fabrication d'acroléine |
| US2558520A (en) * | 1948-01-29 | 1951-06-26 | Us Ind Chemicals Inc | Production of acrolein from glycerol |
| GB1152215A (en) * | 1965-10-12 | 1969-05-14 | Rohm & Haas | Preparation of Acrolein |
| JPS55102536A (en) * | 1979-01-30 | 1980-08-05 | Mitsubishi Petrochem Co Ltd | Preparation of acrylic acid |
| US5080898A (en) * | 1982-05-12 | 1992-01-14 | The University Hospital | Enzymatically active toxin coupled to a cell-specific ligand |
| CA1299193C (en) * | 1986-07-17 | 1992-04-21 | Gordon Gene Harkreader | Anhydrous diluents for the propylene oxidation reaction to acrolein and acrolein oxidation to acrylic acid |
| CA1305178C (en) * | 1986-08-21 | 1992-07-14 | Gordon Gene Harkreader | Anhydrous diluent process for the propylene oxidation reaction to acrolein and acrolein oxidation to acrylic acid |
| JPH0813777B2 (ja) * | 1986-12-11 | 1996-02-14 | 三菱化学株式会社 | アクリル酸の製造法 |
| US5218146A (en) * | 1987-05-27 | 1993-06-08 | Nippon Shokubai Kagaku Kogyo Co., Ltd. | Process for production of acrylic acid |
| JPH0686399B2 (ja) * | 1987-05-27 | 1994-11-02 | 株式会社日本触媒 | アクリル酸の製造方法 |
| AU606160B2 (en) * | 1987-05-27 | 1991-01-31 | Nippon Shokubai Kagaku Kogyo Co. Ltd. | Process for production of acrylic acid |
| DE4238493C1 (de) * | 1992-11-14 | 1994-04-21 | Degussa | Verfahren zur Herstellung von Acrolein und dessen Verwendung |
| TW476746B (en) | 1997-07-23 | 2002-02-21 | Shell Int Research | Hydrogenolysis of glycerol |
| DE19848208A1 (de) | 1998-10-20 | 2000-04-27 | Deg Engineering Gmbh | Reaktor für die katalytische Umsetzung von Reaktionsmedien, insbesondere von gasförmigen Reaktionsmedien |
| DE10019381B4 (de) | 2000-04-19 | 2006-05-18 | Daun, Klaus-Dieter, Dipl.-Ing. | Reaktor für die katalytische Umsetzung von Reaktionsmedien, insbesondere von gasförmigen Reaktionsmedien |
| DE60133473T2 (de) * | 2001-12-14 | 2009-05-20 | Evonik Stockhausen Gmbh | Verfahren zur Herstellung von Acrylsäure |
| US7294734B2 (en) * | 2003-05-02 | 2007-11-13 | Velocys, Inc. | Process for converting a hydrocarbon to an oxygenate or a nitrile |
| JP5006507B2 (ja) * | 2004-01-30 | 2012-08-22 | 株式会社日本触媒 | アクリル酸の製造方法 |
-
2006
- 2006-02-07 FR FR0601061A patent/FR2897059B1/fr not_active Expired - Fee Related
-
2007
- 2007-02-06 JP JP2008551845A patent/JP5097128B2/ja not_active Expired - Fee Related
- 2007-02-06 PL PL07731584T patent/PL1981835T3/pl unknown
- 2007-02-06 DE DE602007001072T patent/DE602007001072D1/de active Active
- 2007-02-06 RU RU2008135966/04A patent/RU2397156C2/ru not_active IP Right Cessation
- 2007-02-06 PT PT07731584T patent/PT1981835E/pt unknown
- 2007-02-06 BR BRPI0707533-2A patent/BRPI0707533A2/pt not_active IP Right Cessation
- 2007-02-06 MY MYPI20083003A patent/MY139630A/en unknown
- 2007-02-06 CN CN2007800045903A patent/CN101400639B/zh not_active Expired - Fee Related
- 2007-02-06 ES ES07731584T patent/ES2325695T3/es active Active
- 2007-02-06 EP EP07731584A patent/EP1981835B1/fr not_active Not-in-force
- 2007-02-06 US US12/278,016 patent/US7880034B2/en not_active Expired - Fee Related
- 2007-02-06 AT AT07731584T patent/ATE430724T1/de not_active IP Right Cessation
- 2007-02-06 KR KR1020087019397A patent/KR101004593B1/ko not_active Expired - Fee Related
- 2007-02-06 WO PCT/FR2007/050758 patent/WO2007090991A2/fr not_active Ceased
-
2008
- 2008-07-30 ZA ZA200806644A patent/ZA200806644B/xx unknown
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