JP2008538213A5 - - Google Patents
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- Publication number
- JP2008538213A5 JP2008538213A5 JP2008503155A JP2008503155A JP2008538213A5 JP 2008538213 A5 JP2008538213 A5 JP 2008538213A5 JP 2008503155 A JP2008503155 A JP 2008503155A JP 2008503155 A JP2008503155 A JP 2008503155A JP 2008538213 A5 JP2008538213 A5 JP 2008538213A5
- Authority
- JP
- Japan
- Prior art keywords
- liquid
- water
- monocarboxylic acid
- liquid phase
- oxidation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000007791 liquid phase Substances 0.000 claims description 88
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 86
- 239000002904 solvent Substances 0.000 claims description 85
- 239000006227 byproduct Substances 0.000 claims description 78
- 239000007788 liquid Substances 0.000 claims description 75
- 239000007789 gas Substances 0.000 claims description 73
- 238000000926 separation method Methods 0.000 claims description 60
- 238000007254 oxidation reaction Methods 0.000 claims description 57
- 239000012071 phase Substances 0.000 claims description 55
- 238000000034 method Methods 0.000 claims description 50
- 150000004945 aromatic hydrocarbons Chemical class 0.000 claims description 43
- 230000003647 oxidation Effects 0.000 claims description 41
- 238000010992 reflux Methods 0.000 claims description 40
- 239000011541 reaction mixture Substances 0.000 claims description 34
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 claims description 29
- 239000002243 precursor Substances 0.000 claims description 28
- 238000006243 chemical reaction Methods 0.000 claims description 23
- 239000012535 impurity Substances 0.000 claims description 21
- 150000002763 monocarboxylic acids Chemical class 0.000 claims description 16
- 239000012452 mother liquor Substances 0.000 claims description 14
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 8
- 239000003054 catalyst Substances 0.000 claims description 8
- 239000001301 oxygen Substances 0.000 claims description 8
- 229910052760 oxygen Inorganic materials 0.000 claims description 8
- 239000012265 solid product Substances 0.000 claims description 7
- 125000003118 aryl group Chemical group 0.000 claims description 6
- 239000007787 solid Substances 0.000 claims description 6
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 5
- 239000001257 hydrogen Substances 0.000 claims description 5
- 229910052739 hydrogen Inorganic materials 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 5
- 239000002253 acid Substances 0.000 claims description 4
- 229910001385 heavy metal Inorganic materials 0.000 claims description 4
- 238000005984 hydrogenation reaction Methods 0.000 claims description 4
- 239000000047 product Substances 0.000 claims description 4
- -1 aromatic carboxylic acids Chemical class 0.000 claims description 3
- 239000012264 purified product Substances 0.000 claims description 3
- 238000006467 substitution reaction Methods 0.000 claims description 2
- 150000002762 monocarboxylic acid derivatives Chemical class 0.000 claims 67
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims 15
- 238000005194 fractionation Methods 0.000 claims 13
- 238000000746 purification Methods 0.000 claims 11
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims 9
- URLKBWYHVLBVBO-UHFFFAOYSA-N Para-Xylene Chemical group CC1=CC=C(C)C=C1 URLKBWYHVLBVBO-UHFFFAOYSA-N 0.000 claims 6
- 238000004891 communication Methods 0.000 claims 6
- LPNBBFKOUUSUDB-UHFFFAOYSA-N p-toluic acid Chemical compound CC1=CC=C(C(O)=O)C=C1 LPNBBFKOUUSUDB-UHFFFAOYSA-N 0.000 claims 6
- 239000012530 fluid Substances 0.000 claims 4
- 238000004519 manufacturing process Methods 0.000 claims 4
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 claims 3
- KXKVLQRXCPHEJC-UHFFFAOYSA-N acetic acid trimethyl ester Natural products COC(C)=O KXKVLQRXCPHEJC-UHFFFAOYSA-N 0.000 claims 3
- 230000000717 retained effect Effects 0.000 claims 3
- 239000012808 vapor phase Substances 0.000 claims 3
- 238000005406 washing Methods 0.000 claims 3
- 238000003763 carbonization Methods 0.000 claims 1
- 125000002843 carboxylic acid group Chemical group 0.000 claims 1
- 238000004821 distillation Methods 0.000 claims 1
- 229910052751 metal Inorganic materials 0.000 claims 1
- 239000002184 metal Substances 0.000 claims 1
- 230000001590 oxidative effect Effects 0.000 claims 1
- 238000011084 recovery Methods 0.000 claims 1
- 238000005204 segregation Methods 0.000 claims 1
- 239000002002 slurry Substances 0.000 claims 1
- 125000001424 substituent group Chemical group 0.000 claims 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US66379205P | 2005-03-21 | 2005-03-21 | |
| US60/663,792 | 2005-03-21 | ||
| PCT/US2006/010486 WO2006102459A1 (en) | 2005-03-21 | 2006-03-20 | Process and apparatus for manufacturing aromatic carboxylic acids including pure forms thereof |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2008538213A JP2008538213A (ja) | 2008-10-16 |
| JP2008538213A5 true JP2008538213A5 (enExample) | 2009-05-14 |
| JP5254001B2 JP5254001B2 (ja) | 2013-08-07 |
Family
ID=36481307
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2008503155A Expired - Fee Related JP5254001B2 (ja) | 2005-03-21 | 2006-03-20 | その純粋形態を含む芳香族カルボン酸を製造するための方法及び装置 |
Country Status (18)
| Country | Link |
|---|---|
| US (4) | US8173834B2 (enExample) |
| EP (3) | EP1861348B1 (enExample) |
| JP (1) | JP5254001B2 (enExample) |
| KR (3) | KR101432517B1 (enExample) |
| CN (3) | CN101146757B (enExample) |
| AT (3) | ATE477230T1 (enExample) |
| BR (3) | BRPI0609328B1 (enExample) |
| CA (3) | CA2599461C (enExample) |
| DE (3) | DE602006015446D1 (enExample) |
| EG (1) | EG25228A (enExample) |
| ES (3) | ES2328402T3 (enExample) |
| MX (3) | MX2007011184A (enExample) |
| PL (3) | PL1866273T3 (enExample) |
| PT (3) | PT1861349E (enExample) |
| RU (3) | RU2414448C2 (enExample) |
| UA (1) | UA96569C2 (enExample) |
| WO (3) | WO2006102459A1 (enExample) |
| ZA (1) | ZA200707537B (enExample) |
Families Citing this family (64)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7264422B2 (en) * | 2004-03-25 | 2007-09-04 | Owens-Corning Fiberglas Technology Inc. | Rotary separator for mineral fibers |
| KR101432517B1 (ko) * | 2005-03-21 | 2014-08-22 | 비피 코포레이션 노쓰 아메리카 인코포레이티드 | 순수 형태를 포함하는 방향족 카르복실산의 제조 방법 및제조 장치 |
| KR100794317B1 (ko) * | 2006-02-20 | 2008-01-11 | (주)에이엠티퍼시픽 | 방향족 화합물의 산화반응시 반응기 배출가스로부터 물을제거하는 방법 |
| US7566802B2 (en) | 2006-05-24 | 2009-07-28 | Eastman Chemical Company | Process for energy recovery and water removal in the preparation of aromatic carboxylic acids |
| US7465824B2 (en) * | 2007-02-08 | 2008-12-16 | Bp Corporation North America Inc. | Process for the production of high purity aromatic carboxylic acids using a benzoic acid and water solvent for oxidation and purification |
| BRPI0721363A2 (pt) * | 2007-02-28 | 2013-01-08 | Hitachi Plant Technologies Ltd | processos para a produÇço de um Ácido carboxÍlico aromÁtico bruto, e de um Ácido dicarboxÍlico aromÁtico bruto |
| KR100860343B1 (ko) * | 2007-03-15 | 2008-09-26 | 삼성석유화학(주) | 친환경적이고 단순화된 방향족 디카르복실산의 제조방법 |
| KR100894761B1 (ko) | 2007-10-18 | 2009-04-24 | 주식회사 효성 | 에너지를 회수 및 재활용하는 2,6-나프탈렌디카르복실산제조방법 |
| US9493387B2 (en) * | 2008-10-31 | 2016-11-15 | Grupo Petrotemex, S.A. De C.V. | Dicarboxylic acid production with minimal wastewater generation |
| US9493389B2 (en) * | 2008-10-31 | 2016-11-15 | Grupo Petrotemex, S.A. De C.V. | Dicarboxylic acid production with enhanced energy recovery |
| US9505692B2 (en) * | 2008-10-31 | 2016-11-29 | Grupo Petrotemex, S.A. De C.V. | Dicarboxylic acid production with self-fuel oxidative destruction |
| US20100113735A1 (en) * | 2008-10-31 | 2010-05-06 | Eastman Chemical Company | Integrated Co-Production of Dicarboxylic Acids |
| US9493388B2 (en) * | 2008-10-31 | 2016-11-15 | Grupo Petrotemex, S.A. De C.V. | Dicarboxylic acid production with direct fired off-gas heating |
| WO2010064006A1 (en) * | 2008-12-02 | 2010-06-10 | Invista Technologies S.A.R.L. | Systems and methods for managing reactor transients |
| US20100243228A1 (en) * | 2009-03-31 | 2010-09-30 | Price Richard J | Method and Apparatus to Effect Heat Transfer |
| DE102009029912A1 (de) * | 2009-06-19 | 2011-06-30 | E.ON Anlagen Service GmbH, 45896 | Verfahren und Vorrichtung zur Gewinnung von Energie aus einem gasförmigen oder flüssigen Brennstoff |
| US8944152B2 (en) * | 2009-07-22 | 2015-02-03 | Johnson Controls Technology Company | Compact evaporator for chillers |
| CN102574094A (zh) * | 2009-10-02 | 2012-07-11 | 英威达技术有限公司 | 减少夹带的系统和方法 |
| WO2011100682A2 (en) * | 2010-02-15 | 2011-08-18 | Invista Technologies S.A.R.L. | Purification of carboxylic acids by catalytic hydrogenation |
| US20120031096A1 (en) * | 2010-08-09 | 2012-02-09 | Uop Llc | Low Grade Heat Recovery from Process Streams for Power Generation |
| US8466312B2 (en) * | 2010-08-20 | 2013-06-18 | Grupo Petrotemex, S.A. De C.V. | Terephthalic acid purge filtration rate by controlling % water in filter feed slurry |
| US9963413B2 (en) | 2010-08-20 | 2018-05-08 | Grupo Petrotemex, S.A. De C.V. | Terephthalic acid purge filtration rate by controlling % water in filter feed slurry |
| CN103476738B (zh) * | 2010-11-22 | 2016-03-16 | 英威达技术有限公司 | 芳族羧酸的生产 |
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| US8992640B2 (en) * | 2011-02-07 | 2015-03-31 | General Electric Company | Energy recovery in syngas applications |
| FR2990989B1 (fr) * | 2012-05-22 | 2016-03-11 | IFP Energies Nouvelles | Procede de production d'electricite par recuperation de la chaleur residuelle de fluides gazeux issus d'une colonne de distillation |
| GB201219983D0 (en) * | 2012-11-06 | 2012-12-19 | Davy Process Techn Ltd | Apparatus and process |
| US20150014148A1 (en) * | 2013-07-11 | 2015-01-15 | Celanese Acetate Llc | Process for Energy Recovery in Manufacturing Cellulose Esters |
| DE102013016660A1 (de) * | 2013-10-09 | 2015-04-09 | Ralf Spitzl | Verfahren und Vorrichtung zur plasmakatalytischen Umsetzung von Stoffen |
| MX375895B (es) * | 2013-12-18 | 2025-03-07 | Bp Corp North America Inc | Proceso mejorado para fabricar acidos carboxilicos aromaticos. |
| WO2015102654A1 (en) * | 2013-12-30 | 2015-07-09 | Bp Corporation North America Inc. | Purification of aromatic carboxylic acids |
| CN105873889A (zh) * | 2013-12-30 | 2016-08-17 | Bp北美公司 | 使用脱水塔冷凝物来纯化粗产物而制备对苯二甲酸的方法 |
| US9394223B2 (en) | 2013-12-31 | 2016-07-19 | Bp Corporation North America Inc. | Oxidation process for preparing purified aromatic carboxylic acids |
| WO2015103172A1 (en) | 2013-12-31 | 2015-07-09 | Bp Corporation North America Inc. | Solid-liquid separations with a no-dry rotary pressure filter |
| CN111909023A (zh) * | 2013-12-31 | 2020-11-10 | Bp北美公司 | 在制造纯化的芳族羧酸中的高压冷凝液生成 |
| JP6158149B2 (ja) * | 2014-08-11 | 2017-07-05 | 株式会社神戸製鋼所 | 蒸留装置 |
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| KR101645514B1 (ko) * | 2015-10-26 | 2016-08-08 | 주식회사 롤팩 | 진공포장장치 |
| MX2018008193A (es) | 2015-12-31 | 2018-08-28 | Bp Corp North America Inc | Procedimientos para la recuperacion del acido acetico precedente de corrientes acuosas. |
| TW201823194A (zh) * | 2016-12-29 | 2018-07-01 | 美商Ｂｐ公司北美股份有限公司 | 經純化的對苯二甲酸(pta)排氣孔蒸汽之利用 |
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| EP3658526A4 (en) | 2017-07-25 | 2021-03-10 | BP Corporation North America Inc. | ROUTING OF A FILTER RINSING PRODUCT OF A PURIFIED AROMATIC CARBOXYLIC ACID FOR ENERGY OPTIMIZATION |
| US20210380519A1 (en) | 2017-08-01 | 2021-12-09 | Bp Corporation North America Inc. | Process for pre-heating boiler feed water in the manufacture of purified aromatic carboxylic acids |
| CN111108084A (zh) * | 2017-08-01 | 2020-05-05 | Bp北美公司 | 纯化芳族羧酸制造中锅炉给水的电加热 |
| US11091419B2 (en) | 2017-11-22 | 2021-08-17 | Exxonmobil Chemical Patents Inc. | Preparation and purification of biphenyldicarboxylic acids |
| DE102018110296A1 (de) * | 2018-04-27 | 2019-10-31 | Linde Aktiengesellschaft | Verfahren zur Behandlung einer sulfidhaltigen Ablauge |
| KR20210027388A (ko) | 2018-06-29 | 2021-03-10 | 비피 코포레이션 노쓰 아메리카 인코포레이티드 | 큰 기공 필터를 사용하는 고액 분리 프로세스 |
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| CN110015954A (zh) * | 2019-01-31 | 2019-07-16 | 武汉有机实业有限公司 | 食品添加剂苯甲酸钠的生产方法 |
| EP3769830A1 (en) * | 2019-07-22 | 2021-01-27 | Sulzer Management AG | Process for distilling a crude composition in a rectification plant including an indirect heat pump |
| ES2995216T3 (en) | 2019-10-31 | 2025-02-07 | Ineos Us Chemicals Company | Solid-liquid separation processes |
| CN111389314B (zh) * | 2020-03-31 | 2020-12-11 | 南京延长反应技术研究院有限公司 | Px生产pta的内置微界面机组强化反应系统及工艺 |
| CN115803311A (zh) * | 2020-09-27 | 2023-03-14 | 英力士美国化学公司 | 回收氧化副产物的方法 |
| US12017197B2 (en) * | 2021-06-22 | 2024-06-25 | Andreas Döring | Method and apparatus for the production of chemical compounds |
| CN113318471B (zh) * | 2021-07-08 | 2024-05-31 | 山东友道化学有限公司 | 二甲苯氧化反应液的处理方法及系统 |
| CN113416623B (zh) * | 2021-08-10 | 2022-12-23 | 肖斌 | 一种白酒生产用分序排酸设备 |
| CN114057252B (zh) * | 2021-12-07 | 2024-05-03 | 天华化工机械及自动化研究设计院有限公司 | 改善精对苯二甲酸装置脱水塔水质的系统及其方法 |
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| KR101432517B1 (ko) * | 2005-03-21 | 2014-08-22 | 비피 코포레이션 노쓰 아메리카 인코포레이티드 | 순수 형태를 포함하는 방향족 카르복실산의 제조 방법 및제조 장치 |
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