JP2008535948A - 膨張可能な微小球体とイオン性化合物とを含有する組成物、およびこれらの組成物の製造法と使用法 - Google Patents
膨張可能な微小球体とイオン性化合物とを含有する組成物、およびこれらの組成物の製造法と使用法 Download PDFInfo
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Abstract
Description
1) BCTMPや他のメカニカル繊維(mechanical fibers)等のバルキー繊維を板紙のセンタープライに組み込むマルチプライ・マシン(multi-ply machines);
2) 水の除去時における緻密化を少なくするための拡張ニッププレス・セクション;および
3) 高温ソフトカレンダリング、高温スチールカレンダリング、スチーム保湿、およびシューニップカレンダリング等のカレンダリング技術;
を使用することを含む。しかしながら、これらの有望な解決策は、必然的に高い資本経費を伴うので実行不可能である。
さらに他の実施態様は、上記組成物の製造法と使用法に関する。
さらに他の態様においては、本発明は、本発明の上記および/または下記態様のいずれかを含有し、そして本発明の上記および/または下記態様のいずれかから製造されたコートおよび/または非コートの紙基材および/または板紙基材に関する。したがって1つの実施態様においては、本発明の組成物は複数種のセルロース繊維を含有してよい。
さらに他の態様においては、本発明は、0.1〜5重量%の複数種の膨張可能な微小球体を含有する基材、物品、および/または包装材料に関し、このとき前記の基材、物品、および/または包装材料は、TAPPI試験法T538om-1による測定にて250SU未満のシェフィールド平滑度、および6以下のスキャニング2ndシアンプリントモトル(a scanning 2nd cyan print mottle)を有する。本発明の1つの実施態様においては、基材、物品、および/または包装材料はカレンダーにかけることができる。本発明のさらに他の実施態様においては、膨張可能な微小球体の外面がイオン性化合物に結びつけられている。さらに他の実施態様においては、基材、物品、および/または包装材料は、0.1〜3重量%の複数種の膨張可能な微小球体を含有する。さらに他の実施態様においては、基材、物品、および/または包装材料は、0.1〜2重量%の複数種の膨張可能な微小球体を含有する。本発明のさらに他の実施態様においては、基材、物品、および/または包装材料は、少なくとも1つのコーティング層を含有する。本発明のさらに他の実施態様においては、コーティング層は、少なくとも1つのトップコートと少なくとも1つのベースコートで構成されている。さらに他の実施態様においては、基材、物品、および/または包装材料は、TAPPI試験法T538om-1による測定にて250SU未満のシェフィールド平滑度、およびカレンダリングした後に6未満のスキャニングプリントモトルを有する。さらに他の実施態様においては、基材、物品、および/または包装材料は、TAPPI試験法T555om-99による測定にて約1.0〜0.5のパーカープリント表面平滑度を有する。
(発明の詳細な説明)
本発明者らは、密度を下げるための、バルクを増大させるための、そして優れた性能特性(例えば、紙基材中の平滑度やプリントモトル)を保持するための、より低コストでより効率的な解決策を見出した。
膨張可能な微小球体の量は変わってよく、基材、または最終的な紙製品もしくは板紙製品の総重量に依存する。紙基材は、基材の総重量を基準として0.001重量%より多い、さらに好ましくは0.02重量%より多い、そして最も好ましくは0.1重量%より多い膨張可能な微小球体を含有してよい。紙基材はさらに、基材の総重量を基準として20重量%未満の、さらに好ましくは10重量%未満の、そして最も好ましくは5重量%未満の膨張可能な微小球体を含有してよい。膨張可能な微小球体の量は、基材の総重量を基準として0.001重量%、0.002重量%、0.005重量%、0.01重量%、0.02重量%、0.05重量%、0.1重量%、0.2重量%、0.5重量%、1.0重量%、1.5重量%、2.0重量%、2.5重量%、3.0重量%、3.5重量%、4.0重量%、4.5重量%、5.0重量%、6.0重量%、7.0重量%、8.0重量%、9.0重量%、10.0重量%、11.0重量%、12.0重量%、13.0重量%、14.0重量%、15.0重量%、16.0重量%、17.0重量%、18.0重量%、19.0重量%、および20.0重量%であってよく、このとき全ての範囲と部分的な範囲を含む。
本発明の組成物および/または粒子において、膨張可能な微小球体は、中性であっても、マイナスに帯電していても、あるいはプラスに帯電していてもよいが、マイナスに帯電しているのが好ましい。
本発明の紙基材は、針葉樹から得られるセルロース繊維を、紙基材中のセルロース繊維の総重量を基準として1〜100重量%の量にて含有してよく、10〜60重量%の量にて含有するのが好ましい。この範囲は、紙基材中のセルロース繊維の総重量を基準として1重量%、2重量%、5重量%、10重量%、15重量%、20重量%、25重量%、30重量%、35重量%、40重量%、45重量%、50重量%、55重量%、60重量%、65重量%、70重量%、75重量%、80重量%、85重量%、90重量%、95重量%、および100重量%を含み、このとき全ての範囲と部分的な範囲を含む。
トビアス=スキャナーモトル*8.8+188
上記の式をセットアップする手順と詳細が、2004年9月20日付け出願の米国特許出願第10/945,306号(該特許出願の全開示内容を参照により本明細書に含める)に記載されている。
本発明の物品の例は、封筒業界において一般的に知られている任意のサイズと形状の封筒であってよい。本発明の物品はさらに、複数の形態を含んだ封筒であってもよい。本発明の封筒は、増量手段を有する紙基材を含有するのが好ましく、このとき好ましい増量手段は、本発明の膨張可能な微小球体、組成物、および粒子である。
例えば折り畳み式段ボール箱として有用なコート紙基材を、通常の紙製造プロセスを使用して製造する。コート紙基材を10psiの圧力にてカレンダー仕上げし、従来の塗被手段を使用してコート紙基材に従来のコーティングを施した。基材にコーティング層を塗被した後、プリントモトルの測定〔目視によって、および極めて感覚的かつ客観的な基準によって(スキャニング)〕を行った。この2ndシアンスキャナーモトルシステムからのデータ間の関係を、主観的な視覚認識に相関付けることもできるし(ゼロ-to-テン・ガイドラインを使用して)、あるいはトビアス・アソシエーツ社から市販のトビアスモトル試験機を使用して、下記の式に基づいて測定される同等のモトル値に変換することもできる。
上記の式をセットアップする手順と詳細が、2004年9月20日付け出願の米国特許出願第10/945,306号(該特許出願の全開示内容を参照により本明細書に含める)に記載されている。次いでその後の実験において、基材の総重量を基準として1重量%〜2重量%の膨張可能な微小球体を含有する紙が得られるよう、上記の従来のプロセスに膨張可能な微小球体を組み込んだ。それぞれ10psiと20psiに等しいカレンダー圧力手段を使用して、2セットの実験を行った。得られた結果を、それぞれに関して表1に示す。
例えば折り畳み式段ボール箱として有用なコート紙基材を、通常の紙製造プロセスを使用して製造する。基材にコーティング層を塗被した後、プリントモトルの測定〔目視によって、および極めて感覚的かつ客観的な基準によって(スキャニング)〕ならびに他の特性の測定を行った(表2)。次いでその後の実験において、膨張可能な微小球体を含有する紙が得られるよう、上記の従来のプロセスに膨張可能な微小球体を、10ポンド/トン、5ポンド/トン、2ポンド/トン、および1ポンド/トンの量にて組み込んだ。得られた結果を、それぞれに関して表2に示す。図1はさらに、2ndシアンスキャナーモトルを、紙製造プロセスに加えられる膨張可能な微小球体の量の関数として示している。対照標準1と2は、紙製造プロセスに膨張可能な微小球体を加えなかった。
上記の開示内容を考慮して、本発明に対する多くの改良や変更が可能である。したがって、添付したクレームの範囲内にて、本明細書中に特定的に説明されている仕方とは別の仕方で本発明を実施できることは言うまでもない。
Claims (39)
- 少なくとも1種の膨張可能な微小球体、および
少なくとも1種のイオン性化合物
を含み、約9.0以下のpHにおいて、10-6M〜0.1Mのイオン強度にてゼロmV以上のゼータ電位を有する組成物。 - 前記ゼータ電位がゼロmVより大きい、請求項1に記載の組成物。
- 前記ゼータ電位がゼロより大きい値〜+150mVの範囲である、請求項1に記載の組成物。
- 前記ゼータ電位が+20mVより大きい値〜+150mVの範囲である、請求項1に記載の組成物。
- 前記イオン性化合物が、イオン性有機化合物とイオン性無機化合物からなる群から選択される少なくとも1種の化合物である、請求項1に記載の組成物。
- 前記イオン性化合物が少なくとも1種のポリ有機化合物である、請求項1に記載の組成物。
- 前記イオン性化合物が少なくとも1種のポリアミン化合物である、請求項1に記載の組成物。
- 前記イオン性化合物が、架橋化合物、分岐化合物、またはこれらの組み合わせ物である、請求項1に記載の組成物。
- 前記イオン性化合物が少なくとも1種のポリエチレンイミン化合物である、請求項1に記載の組成物。
- 前記イオン性化合物が、少なくとも600の重量平均分子量を有する少なくとも1種のポリエチレンイミン化合物である、請求項1に記載の組成物。
- 前記イオン性化合物が、600〜40,000の重量平均分子量を有する少なくとも1種のポリエチレンイミン化合物である、請求項1に記載の組成物。
- 前記イオン性化合物がカチオン性である、請求項1に記載の組成物。
- 前記イオン性化合物が、アルミナとシリカからなる群から選択される少なくとも1種の物質を含む、請求項1に記載の組成物。
- 前記イオン性化合物が、シリカ、アルミナ、酸化スズ、ジルコニア、酸化アンチモン、酸化鉄、および希土類金属酸化物からなる群から選択される少なくとも1種の物質を含んだコロイドを含む、請求項1に記載の組成物。
- 前記イオン性化合物が、シリカ、アルミナ、酸化スズ、ジルコニア、酸化アンチモン、酸化鉄、および希土類金属酸化物からなる群から選択される少なくとも1種の物質を含んだゾルを含む、請求項1に記載の組成物。
- 組成物が粒子である、請求項1に記載の組成物。
- 少なくとも1種の膨張可能な微小球体の外面がイオン性化合物に結びつけられている、請求項16に記載の組成物。
- 少なくとも1種の膨張可能な微小球体の外面がイオン性化合物に非共有結合的に結びつけられている、請求項16に記載の組成物。
- 少なくとも1種の膨張可能な微小球体の外面がアニオン性である、請求項16に記載の粒子。
- 前記イオン性がカチオン性である、請求項16に記載の粒子。
- 少なくとも1種の膨張可能な微小球体と少なくとも1種のイオン性化合物とを接触させて混合物を作製することを含む、請求項1に記載の組成物の製造法。
- 混合物を遠心分離にかけて、少なくとも1種のイオン性化合物を含んだ第1の相と、粒子を含んだ第2の相を作製することをさらに含む、請求項21に記載の製造法。
- 少なくとも1種のイオン性化合物を少なくとも1種の膨張可能な微小球体に吸着させることを含む、請求項1に記載の組成物の製造法。
- 複数種のセルロース繊維をさらに含む、請求項1に記載の組成物。
- 少なくとも1種の膨張可能な微小球体の外面がイオン性化合物に結びつけられている、請求項24に記載の組成物。
- 少なくとも1種の膨張可能な微小球体の外面がイオン性化合物に非共有結合的に結びつけられている、請求項24に記載の組成物。
- 少なくとも1種の膨張可能な微小球体と少なくとも1種のイオン性化合物とを接触させて粒子を作製すること;および前記粒子と前記複数種のセルロース繊維とを接触させること;を含む、請求項24に記載の組成物の製造法。
- 少なくとも1種の膨張可能な微小球体と少なくとも1種のイオン性化合物とを接触させて粒子を作製すること;および複数種のセルロース繊維を含んだ溶液中に前記粒子を注入すること;を含む、請求項24に記載の組成物の製造法。
- 複数種のセルロース繊維;
0.1〜5重量%の複数種の膨張可能な微小球体;および
6以下のスキャニング2ndシアンプリントモトル;
を含み、TAPPI試験法T538om-1による測定にて250SU未満のシェフィールド平滑度を有する紙基材または板紙基材。 - 膨張可能な微小球体の外面がイオン性化合物に結びつけられている、請求項29に記載の基材。
- 0.1〜3重量%の複数種の膨張可能な微小球体を含む、請求項29に記載の基材。
- 0.1〜2重量%の複数種の膨張可能な微小球体を含む、請求項29に記載の基材。
- 少なくとも1つのコーティング層をさらに含む、請求項29に記載の基材。
- コーティング層が、少なくとも1つのトップコートと少なくとも1つのベースコートを含む、請求項29に記載の基材。
- TAPPI試験法T538om-1による測定にて、シェフィールド平滑度が250SU未満であり、前記基材をカレンダリングした後のスキャニングプリントモトルが6未満である、請求項29に記載の基材。
- TAPPI試験法T555om-99による測定にて、基材が約1.0〜0.5のパーカープリント表面平滑度を有する、請求項29に記載の基材。
- 請求項29に記載の基材を含む物品。
- 前記物品が折り畳み式段ボール箱である、請求項34に記載の物品。
- セルロース繊維のウェブと増量剤を含んだ少なくとも1種の紙基材または板紙基材を含む物品であって、物品の重量が1オンス以下であり、1オンスとの差が、同じ数の層を有する従来の包装材料のそれより大きい絶対値となるような重量を物品が有する、前記物品。
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2006
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US20100032114A1 (en) | 2010-02-11 |
CN101137790A (zh) | 2008-03-05 |
CA2600801C (en) | 2012-07-10 |
US20110277949A1 (en) | 2011-11-17 |
AU2006223142B2 (en) | 2011-04-07 |
WO2006099364A1 (en) | 2006-09-21 |
CA2600801A1 (en) | 2006-09-21 |
RU2506363C2 (ru) | 2014-02-10 |
EP1856326A1 (en) | 2007-11-21 |
US20100032115A1 (en) | 2010-02-11 |
US8034847B2 (en) | 2011-10-11 |
US8377526B2 (en) | 2013-02-19 |
BRPI0608029A2 (pt) | 2009-11-03 |
US20130146240A1 (en) | 2013-06-13 |
KR101329927B1 (ko) | 2013-11-20 |
CA2750039A1 (en) | 2006-09-21 |
MX2007011113A (es) | 2007-11-15 |
JP2013151780A (ja) | 2013-08-08 |
RU2425068C2 (ru) | 2011-07-27 |
AU2006223142A1 (en) | 2006-09-21 |
EP2357279A1 (en) | 2011-08-17 |
EP2295633A1 (en) | 2011-03-16 |
KR101192031B1 (ko) | 2012-10-16 |
RU2007138972A (ru) | 2009-05-27 |
US20070044929A1 (en) | 2007-03-01 |
US8030365B2 (en) | 2011-10-04 |
KR20070114313A (ko) | 2007-11-30 |
KR20120074315A (ko) | 2012-07-05 |
JP5302670B2 (ja) | 2013-10-02 |
RU2011112006A (ru) | 2012-10-20 |
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