JP2007514819A5 - - Google Patents

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JP2007514819A5
JP2007514819A5 JP2006545359A JP2006545359A JP2007514819A5 JP 2007514819 A5 JP2007514819 A5 JP 2007514819A5 JP 2006545359 A JP2006545359 A JP 2006545359A JP 2006545359 A JP2006545359 A JP 2006545359A JP 2007514819 A5 JP2007514819 A5 JP 2007514819A5
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added
monool
silane
weight
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JP2006545359A
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JP4757202B2 (ja
JP2007514819A (ja
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Priority claimed from US10/741,871 external-priority patent/US7465778B2/en
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実施例２
この実施例においては、本発明によるシランを末端基とするポリウレタン（ＳＴＰ１）の調製法を説明する。攪拌機、窒素ガス導入口、滴下漏斗及び冷却器を具備したフラスコ（５リットル）内へイソホロンジイソシアネート（１５０．９ｇ；１．４当量）、当量が６４１１のポリエーテルモノオール（３６６４．１ｇ；０．６当量）（該モノオールは米国特許第４３５５１８８号明細書に記載の方法に従って調製した）、及びジブチル錫ジラウレート（０．６ｇ）を導入した。反応を６０℃で３時間おこなった後、ＮＣＯ含有量をＮＣＯ滴定によって測定したところ０．６５重量％であった（理論値：０．７９％）。次いで、実施例１で調製したシラン官能性アスパルテート（２０２．２ｇ；０．５７当量）を添加し、得られた混合物を６０℃で６０分間保持した後では、ＮＣＯ基はＩＲによって検出されなかった。この時点で、ビニルトリメトキシシラン（２０ｇ）を湿分掃去剤として添加した。粘度は１６１００ｃｐｓ／２５℃であった。
JP2006545359A 2003-12-19 2004-12-15 シランを末端基とするポリウレタン Expired - Fee Related JP4757202B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US10/741,871 US7465778B2 (en) 2003-12-19 2003-12-19 Silante terminated polyurethane
US10/741,871 2003-12-19
PCT/US2004/042033 WO2005061622A2 (en) 2003-12-19 2004-12-15 Silane terminated polyurethane

Publications (3)

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JP2007514819A JP2007514819A (ja) 2007-06-07
JP2007514819A5 true JP2007514819A5 (ja) 2011-05-06
JP4757202B2 JP4757202B2 (ja) 2011-08-24

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JP2006545359A Expired - Fee Related JP4757202B2 (ja) 2003-12-19 2004-12-15 シランを末端基とするポリウレタン

Country Status (9)

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US (1) US7465778B2 (ja)
EP (1) EP1697436B1 (ja)
JP (1) JP4757202B2 (ja)
KR (1) KR101151974B1 (ja)
CN (1) CN100484978C (ja)
HK (1) HK1095845A1 (ja)
MX (1) MXPA06006867A (ja)
RU (1) RU2367670C2 (ja)
WO (1) WO2005061622A2 (ja)

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CN109486470B (zh) * 2018-09-27 2020-06-30 新丰见微化工实业有限公司 一种咪唑封端聚氨酯作用的环氧大豆油胶粘剂及其制备方法
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