JP2007514538A5 - - Google Patents
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- JP2007514538A5 JP2007514538A5 JP2006545504A JP2006545504A JP2007514538A5 JP 2007514538 A5 JP2007514538 A5 JP 2007514538A5 JP 2006545504 A JP2006545504 A JP 2006545504A JP 2006545504 A JP2006545504 A JP 2006545504A JP 2007514538 A5 JP2007514538 A5 JP 2007514538A5
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- JP
- Japan
- Prior art keywords
- temperature
- catalyst precursor
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- stage
- component
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 238000000034 method Methods 0.000 claims 25
- 239000012018 catalyst precursor Substances 0.000 claims 12
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims 6
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims 4
- 229910002651 NO3 Inorganic materials 0.000 claims 4
- NHNBFGGVMKEFGY-UHFFFAOYSA-N nitrate group Chemical group [N+](=O)([O-])[O-] NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 claims 4
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims 3
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims 3
- 230000032683 aging Effects 0.000 claims 3
- 229910052787 antimony Inorganic materials 0.000 claims 3
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical group [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 claims 3
- 239000003054 catalyst Substances 0.000 claims 3
- 229910017052 cobalt Inorganic materials 0.000 claims 3
- 239000010941 cobalt Substances 0.000 claims 3
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims 3
- 229910052749 magnesium Inorganic materials 0.000 claims 3
- 239000011777 magnesium Substances 0.000 claims 3
- 229910052759 nickel Inorganic materials 0.000 claims 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 3
- 229910052725 zinc Inorganic materials 0.000 claims 3
- 239000011701 zinc Substances 0.000 claims 3
- 229910052797 bismuth Inorganic materials 0.000 claims 2
- JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 claims 2
- 210000001217 buttock Anatomy 0.000 claims 2
- 229910052792 caesium Inorganic materials 0.000 claims 2
- TVFDJXOCXUVLDH-UHFFFAOYSA-N caesium atom Chemical compound [Cs] TVFDJXOCXUVLDH-UHFFFAOYSA-N 0.000 claims 2
- 239000010949 copper Substances 0.000 claims 2
- 238000001035 drying Methods 0.000 claims 2
- 229910052742 iron Inorganic materials 0.000 claims 2
- 239000007788 liquid Substances 0.000 claims 2
- 238000001556 precipitation Methods 0.000 claims 2
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical group [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims 1
- 229910052684 Cerium Inorganic materials 0.000 claims 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims 1
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical group [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical group [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical group [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical group [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims 1
- 238000002441 X-ray diffraction Methods 0.000 claims 1
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 150000001336 alkenes Chemical class 0.000 claims 1
- 229910052782 aluminium Inorganic materials 0.000 claims 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical group [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims 1
- 229910052788 barium Inorganic materials 0.000 claims 1
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 claims 1
- 229910052796 boron Inorganic materials 0.000 claims 1
- 229910052793 cadmium Inorganic materials 0.000 claims 1
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 claims 1
- 238000001354 calcination Methods 0.000 claims 1
- GWXLDORMOJMVQZ-UHFFFAOYSA-N cerium Chemical compound [Ce] GWXLDORMOJMVQZ-UHFFFAOYSA-N 0.000 claims 1
- 229910052804 chromium Inorganic materials 0.000 claims 1
- 239000011651 chromium Substances 0.000 claims 1
- 229910052802 copper Inorganic materials 0.000 claims 1
- 238000010304 firing Methods 0.000 claims 1
- 125000002485 formyl group Chemical class [H]C(*)=O 0.000 claims 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 claims 1
- 229910044991 metal oxide Inorganic materials 0.000 claims 1
- 150000004706 metal oxides Chemical class 0.000 claims 1
- 229910052750 molybdenum Inorganic materials 0.000 claims 1
- 239000011733 molybdenum Substances 0.000 claims 1
- 229910052758 niobium Inorganic materials 0.000 claims 1
- 239000010955 niobium Substances 0.000 claims 1
- GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical compound [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 claims 1
- 150000002823 nitrates Chemical class 0.000 claims 1
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 claims 1
- 230000001590 oxidative effect Effects 0.000 claims 1
- 239000011574 phosphorus Chemical group 0.000 claims 1
- 229910052698 phosphorus Inorganic materials 0.000 claims 1
- 229910052700 potassium Inorganic materials 0.000 claims 1
- 239000011591 potassium Substances 0.000 claims 1
- 230000001376 precipitating effect Effects 0.000 claims 1
- 230000005855 radiation Effects 0.000 claims 1
- 229910052701 rubidium Inorganic materials 0.000 claims 1
- IGLNJRXAVVLDKE-UHFFFAOYSA-N rubidium atom Chemical compound [Rb] IGLNJRXAVVLDKE-UHFFFAOYSA-N 0.000 claims 1
- 229910052710 silicon Inorganic materials 0.000 claims 1
- 239000010703 silicon Chemical group 0.000 claims 1
- 239000002002 slurry Substances 0.000 claims 1
- 239000011593 sulfur Chemical group 0.000 claims 1
- 229910052717 sulfur Inorganic materials 0.000 claims 1
- 229910052714 tellurium Inorganic materials 0.000 claims 1
- PORWMNRCUJJQNO-UHFFFAOYSA-N tellurium atom Chemical compound [Te] PORWMNRCUJJQNO-UHFFFAOYSA-N 0.000 claims 1
- 229910052716 thallium Inorganic materials 0.000 claims 1
- BKVIYDNLLOSFOA-UHFFFAOYSA-N thallium Chemical compound [Tl] BKVIYDNLLOSFOA-UHFFFAOYSA-N 0.000 claims 1
- 229910052718 tin Inorganic materials 0.000 claims 1
- 239000010936 titanium Chemical group 0.000 claims 1
- 229910052719 titanium Inorganic materials 0.000 claims 1
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 claims 1
- 229910052721 tungsten Inorganic materials 0.000 claims 1
- 239000010937 tungsten Substances 0.000 claims 1
- 229910052720 vanadium Inorganic materials 0.000 claims 1
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 claims 1
- 238000005406 washing Methods 0.000 claims 1
- 229910052726 zirconium Inorganic materials 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10/741,383 | 2003-12-19 | ||
| US10/741,383 US7229945B2 (en) | 2003-12-19 | 2003-12-19 | Process of making mixed metal oxide catalysts for the production of unsaturated aldehydes from olefins |
| PCT/US2004/042551 WO2005062806A2 (en) | 2003-12-19 | 2004-12-19 | Process of making mixed metal oxide catalysts for the production of unsaturated aldehydes from olefins |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2007514538A JP2007514538A (ja) | 2007-06-07 |
| JP2007514538A5 true JP2007514538A5 (enExample) | 2007-10-04 |
| JP5103019B2 JP5103019B2 (ja) | 2012-12-19 |
Family
ID=34678137
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2006545504A Expired - Fee Related JP5103019B2 (ja) | 2003-12-19 | 2004-12-19 | オレフィンから不飽和アルデヒドを製造するための混合金属酸化物触媒の製造法 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US7229945B2 (enExample) |
| EP (1) | EP1694440A4 (enExample) |
| JP (1) | JP5103019B2 (enExample) |
| KR (1) | KR101122346B1 (enExample) |
| CN (1) | CN100457267C (enExample) |
| WO (1) | WO2005062806A2 (enExample) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4691359B2 (ja) * | 2002-07-05 | 2011-06-01 | 三菱レイヨン株式会社 | メタクリル酸製造用触媒の製造方法 |
| US7452843B2 (en) * | 2003-12-29 | 2008-11-18 | Umicore Ag & Co. Kg | Exhaust treatment devices, catalyst, and methods of making and using the same |
| US7494952B2 (en) * | 2006-01-17 | 2009-02-24 | Saudi Basic Industries Corporation | Process of making mixed metal oxide catalysts for the production of unsaturated aldehydes from olefins |
| US7888281B2 (en) * | 2007-01-19 | 2011-02-15 | Evernu Technology, Llc | Selective oxidation of alkanes and/or alkenes to valuable oxygenates |
| JP4639247B2 (ja) * | 2008-07-23 | 2011-02-23 | 石油資源開発株式会社 | 炭化水素リフォーミング用触媒およびその製造方法ならびにこれを用いた合成ガスの製法 |
| CN101746733B (zh) | 2008-12-11 | 2012-10-03 | 中科合成油技术有限公司 | 一种连续化制备金属氧化物材料和催化剂的方法及设备 |
| CN102247862B (zh) * | 2010-05-18 | 2013-12-04 | 中国石油天然气股份有限公司 | 一种多层复合金属氧化物催化剂及其制备方法 |
| US8722940B2 (en) | 2012-03-01 | 2014-05-13 | Saudi Basic Industries Corporation | High molybdenum mixed metal oxide catalysts for the production of unsaturated aldehydes from olefins |
| JP6238354B2 (ja) * | 2014-02-07 | 2017-11-29 | 日本化薬株式会社 | 不飽和アルデヒドおよび／または不飽和カルボン酸製造用触媒およびその製造方法ならびに不飽和アルデヒドおよび／または不飽和カルボン酸の製造方法 |
| CN107684927B (zh) * | 2016-08-03 | 2020-07-28 | 万华化学集团股份有限公司 | 一种用于氯化氢氧化制备氯气的催化剂及其制备方法和用途 |
| JP6205044B2 (ja) * | 2016-10-24 | 2017-09-27 | 旭化成株式会社 | 酸化物触媒の製造方法 |
| WO2020115678A1 (en) * | 2018-12-04 | 2020-06-11 | Sabic Global Technologies B.V. | Catalyst composition for the production c2 hydrocarbons from methane |
| US11478784B2 (en) | 2020-02-04 | 2022-10-25 | Saudi Arabian Oil Company | Catalyst compositions for ammonia decomposition |
| CN113522301A (zh) * | 2021-06-28 | 2021-10-22 | 谷育英 | 烯烃氧化制不饱和醛催化剂及其制备方法和应用 |
Family Cites Families (39)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3984477A (en) * | 1973-12-11 | 1976-10-05 | Daicel, Ltd. | Catalyst for production of α,β-unsaturated aldehydes |
| DE2431511C3 (de) * | 1974-07-01 | 1980-10-02 | Institut Chimitscheskoj Fisiki Akademii Nauk Ssr, Moskau | Verfahren zur Herstellung von a , ß -ungesättigten Säuren und Aldehyden |
| US4049577A (en) * | 1975-12-15 | 1977-09-20 | The Dow Chemical Company | Catalyst for making acrolein |
| DE2626887B2 (de) * | 1976-06-16 | 1978-06-29 | Basf Ag, 6700 Ludwigshafen | Katalysator für die Oxadation von (Methacrolein zu (Meth)Acrylsäure |
| US4556731A (en) * | 1977-07-28 | 1985-12-03 | The Standard Oil Company | Process for the oxidation of olefins using catalysts containing various promoter elements |
| JPS58119346A (ja) * | 1982-01-06 | 1983-07-15 | Nippon Shokubai Kagaku Kogyo Co Ltd | プロピレン酸化用触媒 |
| JPS5946132A (ja) * | 1982-09-06 | 1984-03-15 | Nippon Shokubai Kagaku Kogyo Co Ltd | メタクロレイン合成用触媒 |
| US4537874A (en) * | 1982-10-22 | 1985-08-27 | Nippon Shokubai Kagaku Kogyo Co Ltd | Catalyst for production of unsaturated aldehydes |
| JPS6122040A (ja) * | 1984-07-10 | 1986-01-30 | Mitsubishi Rayon Co Ltd | メタクロレイン及びメタクリル酸の製造法 |
| DE3740271A1 (de) * | 1987-11-27 | 1989-06-01 | Basf Ag | Verfahren zur herstellung einer fuer die gasphasenoxidation von propylen zu acrolein und acrylsaeure katalytisch aktiven masse |
| US4837191A (en) * | 1988-05-16 | 1989-06-06 | The Standard Oil Company | Catalytic mixture for the ammoxidation of paraffins |
| JPH0813332B2 (ja) * | 1989-09-25 | 1996-02-14 | 三菱レイヨン株式会社 | メタクロレイン及びメタクリル酸の製造用触媒の調製法 |
| US5276178A (en) * | 1989-12-06 | 1994-01-04 | Nippon Shokubai Co., Ltd. | Process for producing methacrolein and methacrylic acid |
| JPH0784400B2 (ja) * | 1990-04-03 | 1995-09-13 | 株式会社日本触媒 | 不飽和アルデヒドおよび不飽和酸の製造方法 |
| KR950004031B1 (ko) * | 1991-02-27 | 1995-04-22 | 미쓰이도오아쓰가가꾸 가부시끼가이샤 | 메타크롤레인의 제조방법 및 메타크롤레인의 제조에 사용하는 촉매의 제조방법 |
| US5532199A (en) * | 1992-06-19 | 1996-07-02 | Mitsubishi Rayon Co., Ltd. | Carrier-supported catalyst for the synthesis of unsaturated aldehydes and unsaturated carboxylic acids and process for preparing the same |
| KR100277241B1 (ko) * | 1993-06-25 | 2001-02-01 | 고오사이 아끼오 | 불포화 알데하이드 및 불포화 카복실산의 제조방법 |
| KR100247524B1 (ko) * | 1994-05-31 | 2000-03-15 | 겐지 아이다 | 아크릴산 제조용 촉매 및 이 촉매를 이용한 아크릴산의 제조방법 |
| ES2140684T3 (es) * | 1994-06-22 | 2000-03-01 | Asahi Chemical Ind | Metodo para la fabricacion de metacroleina. |
| JP3342794B2 (ja) * | 1994-12-21 | 2002-11-11 | 三菱レイヨン株式会社 | メタクロレイン及びメタクリル酸合成用担持触媒の製造法 |
| WO1996019290A1 (en) * | 1994-12-21 | 1996-06-27 | Mitsubishi Rayon Co., Ltd. | Process for the preparation of supported catalyst for synthesis of methacrolein and methacrylic acid |
| JP3786297B2 (ja) * | 1995-03-03 | 2006-06-14 | 日本化薬株式会社 | 触媒の製造方法 |
| JP3793317B2 (ja) * | 1996-05-14 | 2006-07-05 | 日本化薬株式会社 | 触媒及び不飽和アルデヒドおよび不飽和酸の製造方法 |
| JP3775872B2 (ja) * | 1996-12-03 | 2006-05-17 | 日本化薬株式会社 | アクロレイン及びアクリル酸の製造方法 |
| CN1108865C (zh) * | 1997-09-03 | 2003-05-21 | 中国石油化工集团公司 | 生产丙烯腈的催化剂 |
| WO1999041012A1 (en) * | 1998-02-13 | 1999-08-19 | Korea Research Institute Of Chemical Technology | A solid catalyst with core-shell catalytic phase and a method of preparation thereof |
| DE19815278A1 (de) * | 1998-04-06 | 1999-10-07 | Basf Ag | Multimetalloxidmassen |
| US6632772B2 (en) * | 1998-09-23 | 2003-10-14 | Lg Chemical, Ltd. | Method of coating a catalyst to a support for use in acrolein oxidation |
| DE19855913A1 (de) * | 1998-12-03 | 2000-06-08 | Basf Ag | Multimetalloxidmasse zur gasphasenkatalytischen Oxidation organischer Verbindungen |
| JP4185217B2 (ja) * | 1999-05-25 | 2008-11-26 | 株式会社日本触媒 | 複合酸化物触媒、並びに（メタ）アクロレインおよび（メタ）アクリル酸の製造方法 |
| JP3819192B2 (ja) * | 1999-10-18 | 2006-09-06 | ダイヤニトリックス株式会社 | アクリロニトリルの製造法 |
| US6693059B2 (en) * | 2000-02-09 | 2004-02-17 | Rohm And Haas Company | Process for preparing a catalyst and catalytic oxidation therewith |
| DE10046957A1 (de) * | 2000-09-21 | 2002-04-11 | Basf Ag | Verfahren zur Herstellung eines Multimetalloxid-Katalysators, Verfahren zur Herstellung ungesättigter Aldehyde und/oder Carbonsäuren und Bandcalziniervorrichtung |
| DE10046928A1 (de) * | 2000-09-21 | 2002-04-11 | Basf Ag | Verfahren zur Herstellung von Multimetalloxidmassen |
| JP3892244B2 (ja) * | 2001-03-21 | 2007-03-14 | 株式会社日本触媒 | 不飽和アルデヒドおよび不飽和カルボン酸製造用触媒の製造方法 |
| EP2343124B1 (en) * | 2001-11-08 | 2021-01-06 | Mitsubishi Chemical Corporation | METHOD FOR PREPARATION of a COMPOSITE OXIDE CATALYST |
| US6946422B2 (en) * | 2002-12-12 | 2005-09-20 | Saudi Basic Industries Corporation | Preparation of mixed metal oxide catalysts for catalytic oxidation of olefins to unsaturated aldehydes |
| US20040192973A1 (en) * | 2003-03-31 | 2004-09-30 | Saudi Basic Industries Corporation | Mixed metal oxide catalysts for the production of unsaturated aldehydes from olefins |
| JP4421558B2 (ja) * | 2003-05-30 | 2010-02-24 | 日本化薬株式会社 | メタクリル酸製造用触媒の製造方法 |
-
2003
- 2003-12-19 US US10/741,383 patent/US7229945B2/en not_active Expired - Lifetime
-
2004
- 2004-12-19 CN CNB2004800418977A patent/CN100457267C/zh not_active Expired - Fee Related
- 2004-12-19 EP EP04814700A patent/EP1694440A4/en not_active Ceased
- 2004-12-19 JP JP2006545504A patent/JP5103019B2/ja not_active Expired - Fee Related
- 2004-12-19 KR KR1020067014281A patent/KR101122346B1/ko not_active Expired - Fee Related
- 2004-12-19 WO PCT/US2004/042551 patent/WO2005062806A2/en not_active Ceased
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