JP2006527293A - 耐摩耗性光学層及び成形体 - Google Patents
耐摩耗性光学層及び成形体 Download PDFInfo
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- JP2006527293A JP2006527293A JP2006515901A JP2006515901A JP2006527293A JP 2006527293 A JP2006527293 A JP 2006527293A JP 2006515901 A JP2006515901 A JP 2006515901A JP 2006515901 A JP2006515901 A JP 2006515901A JP 2006527293 A JP2006527293 A JP 2006527293A
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- active hydrogen
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Abstract
【解決手段】該組成物によって得ることが可能な成形体又は被覆基材は、高い透明性及び高い耐摩耗性(attrition resistance)を示し、従って、特に光学用途に好適である。
Description
Rh(R)bSiX(3−b) (I)
式中、Rh基は、エポキシ基又はヒドロキシル基を有する非加水分解性の置換基を表し、R基は、同一又は異なって、それぞれ非加水分解性置換基であり、X基は、同一又は異なって、それぞれ加水分解性基又はヒドロキシル基であり、bは0、1又は2である。値bは、好ましくは0、すなわち、式RhSiX3のシランが好ましい。
Ra(R)bSiX(3−b) (Ia)
式中、Ra基はアミノ(例えば、上記−NHR’基)、チオあるいはカルボキシル又は無水カルボン酸基を有する非加水分解性置換基を表し、R、X及びbは、それぞれ式(I)において定義される通りである。Raは、式(I)のR基に対応し、官能基は、アミノ、チオあるいはカルボキシル又は無水カルボン酸基であり、式(I)においてRに対して定義された全てのものが、同様に適用される。
Ri(R)bSiX(3−b) (II)
式中、Ri基は、イソシアネート基を有する非加水分解性置換基を表し、R基は、同一又は異なって、他の非加水分解性置換基であり、X基は、同一又は異なって、加水分解性基又はヒドロキシル基であり、bは、0、1又は2、あるいはこれらのイソシアナートシランに基づく縮合物である。置換基RおよびXは、それぞれ、式(I)において定義され、Rは好ましくは官能基を有さない非加水分解性置換基であり、より好ましくは1〜10の炭素原子を有するアルキル基であり、Xは好ましくは1〜10の炭素原子を有するアルコキシ基であり、好ましくはメトキシ又はエトキシである。
RaSiX(4−a)(III)
式中、R基は同一又は異なって、非加水分解性基であり、X基は、同一又は異なって、加水分解性基又はヒドロキシル基であり、aは1、2又は3、あるいはそれから得られたオリゴマーである。aは好ましくは1である。R及びX基は、上記式(I)及び(II)に定義される通りである。非加水分解性R基は、互いに同一又は異なって、官能基を有する非加水分解性R基又は好ましくはそのような官能基を有さない非加水分解性R基であり得る。
式中、X及びRは、それぞれ式(I)に定義されるとおりであり、Rfは、好ましくは、少なくとも2つの原子によってSiから分離された炭素原子に結合した1〜30のフッ素原子を有する非加水分解性基、好ましくはエチレン基であり、bは0、1又は2である。Rは、特に、官能基を有さない基であり、好ましくはメチル又はエチル等のアルキル基である。
SiX4 (V)
式中、Xは式(I)において定義される通りである。具体例としては、Si(OCH3)4、Si(OC2H5)4、Si(O−n−又はi−C3H7)4、Si(OC4H9)4、SiCl4、HSiCl3、Si(OOCC3H)4である。これらのシランのうち、テトラメトキシシラン及びテトラエトキシシランが好ましい。しばしば、式(III)のシラン、特にアルキルトリアルコキシシラン、及び式(V)のシランに基づく重縮合物が好ましい。
Claims (24)
- 表面上に、活性水素又はその前駆体を有する基を持つ有機基を有する表面改質されたナノスケール固体粒子、及びイソシアネート基がブロックされ得る少なくとも1種のイソシアネートを含む組成物。
- 活性水素又はその前駆体を有する基が、ヒドロキシル基及び/又はエポキシ基、チオール基、アミノ基、あるいはカルボキシル基及び/又は無水カルボン酸基であることを特徴とする、請求項1に記載の組成物。
- 活性水素又はその前駆体を有する基が、ヒドロキシル基及び/又はエポキシ基であることを特徴とする、請求項2に記載の組成物。
- ナノスケール固体粒子が、非加水分解性置換基上に、エポキシ又はヒドロキシル基、チオール基、アミノ基、あるいはカルボキシル基又は無水カルボン酸基を有する加水分解性シランによって表面改質されたことを特徴とする、請求項1〜3のいずれかに記載の組成物。
- 表面改質ナノスケール固体粒子が、第1表面改質剤で処理され、その後、活性水素又はその前駆体を有する基を持つ有機基を提供する第2表面改質剤で処理されたことを特徴とする、請求項1〜4のいずれかに記載の組成物。
- ヒドロキシル基及び/又はエポキシ基を有する有機基が、グリシドキシプロピルトリメトキシシラン、グリシドキシプロピルトリエトキシシラン、3,4−エポキシブチルトリメトキシシラン、3,4−エポキシブチルトリエトキシシラン及び/又は2−(3,4−エポキシシクロヘキシル)エチルトリエトキシシラン、2−(3,4−エポキシシクロヘキシル)エチルトリメトキシシランに由来することを特徴とする、請求項1〜5のいずれかに記載の組成物。
- ナノスケール固体粒子が、無機ナノスケール固体粒子であることを特徴とする、請求項1〜6のいずれかに記載の組成物。
- ナノスケール固体粒子が、金属粒子、酸化物(oxidic)粒子又は硫化物(sulfidic)粒子或いは半導体粒子であることを特徴とする、請求項1〜7のいずれかに記載の組成物。
- ナノスケール粒子が、SiO2、Al2O3、ITO、ATO、AlOOH、Ta2O5、ZrO2及び/又はTiO2の金属酸化物粒子であることを特徴とする、請求項8に記載の組成物。
- 少なくとも1つのイソシアネートがブロックされていることを特徴とする、請求項1〜9のいずれかに記載の組成物。
- イソシアネートが、有機ポリイソシアネート又はイソシアネートシラン或いはそれらの縮合物であることを特徴とする、請求項1〜10のいずれかに記載の組成物。
- さらに、有機ポリオールを含むことを特徴とする、請求項1〜11のいずれかに記載の組成物。
- さらに、有機的に改質された無機重縮合物を含むことを特徴とする、請求項1〜12のいずれかに記載の組成物。
- さらに、活性水素を有する基とイソシアネート間の反応のための触媒を含むことを特徴とする、請求項1〜13のいずれかに記載の組成物。
- エポキシ基を有する有機表面基が存在する場合、これらのエポキシ基がウレタン結合形成のためのヒドロキシル基に変換され得ることを特徴とする、請求項1〜14のいずれかに記載の組成物。
- ナノスケール固体粒子が、表面上に、活性水素又はその前駆体を有する少なくとも2つの基を持つ有機基を有することを特徴とする、請求項1〜15のいずれかに記載の組成物。
- 成形体(molding)又は被覆基材であって、前記成形体又は前記被覆基材の層が、請求項1〜16のいずれかに記載の硬化組成物であり、固体粒子の表面上に存在するエポキシ基又は無水カルボン酸基が、存在する場合には、硬化前又は硬化中にさらなる反応のためにヒドロキシル基及びカルボキシル基にそれぞれ変換された、成形体又は被覆基材。
- 光学部品(optical component)又は光学部品上の透明層を含む、請求項17に記載の成形体又は被覆基材。
- 基材が、金属、ガラス、プラスチック、木又は紙で作られている、請求項17又は18に記載の被覆基材。
- 基材がレンズである、請求項17〜19のいずれかに記載の被覆基材。
- 請求項17〜20のいずれかに記載の成形体又は被覆基材の製造方法であって、ここで、
a)表面上に、活性水素又はその前駆体を有する基を持つ有機基を有する表面改質ナノスケール固体粒子を、イソシアネート基がブロックされ得る少なくとも1種のイソシアネートと混合する、
b)結果として得られた組成物を、基材に塗布又は金型中に導入する、及び
c)ナノ粒子上の活性水素を有する基とイソシアネート間の結合形成によって、硬化が起こり、
ブロックされたイソシアネートが用いられる場合、硬化前又は硬化中にイソシアネートが脱ブロック(deblock)され、表面改質ナノ粒子が前駆体を含む場合、前駆体が活性水素を有する基に変換される、成形体又は被覆基材の製造方法。 - 有機基が、ヒドロキシル基及び/又はエポキシ基、チオール基、アミノ基、あるいはカルボキシル基及び/又は無水カルボン酸基を含み、ウレタン、チオウレタン又はウレア架橋を形成するために硬化され、表面改質ナノ粒子がエポキシ基又は無水カルボン酸基を含む場合、エポキシ基がヒドロキシル基に変換され、無水カルボン酸基がカルボキシル基に変換されることを特徴とする、請求項21に記載の方法。
- 光学的用途のための請求項17〜20のいずれかに記載の成形体又は被覆基材の使用。
- 光学的ハイバリュー層で基材をコーティングするための請求項1〜16のいずれかに記載の組成物の使用。
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2004
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- 2004-06-11 CA CA002527771A patent/CA2527771A1/en not_active Abandoned
- 2004-06-11 WO PCT/EP2004/006325 patent/WO2004110926A1/de active Application Filing
- 2004-06-11 EP EP04739815.1A patent/EP1631523B1/de active Active
- 2004-06-11 JP JP2006515901A patent/JP5072356B2/ja active Active
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2005
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Cited By (2)
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JP2011518747A (ja) * | 2008-04-23 | 2011-06-30 | メルク パテント ゲゼルシャフト ミット ベシュレンクテル ハフツング | 反応的に表面修飾した粒子 |
JP2017071724A (ja) * | 2015-10-09 | 2017-04-13 | セコ コーポレイション リミテッド | 防曇剤 |
Also Published As
Publication number | Publication date |
---|---|
EP1631523B1 (de) | 2019-11-27 |
JP5072356B2 (ja) | 2012-11-14 |
CA2527771A1 (en) | 2004-12-23 |
US8388859B2 (en) | 2013-03-05 |
KR20060024794A (ko) | 2006-03-17 |
US20060159923A1 (en) | 2006-07-20 |
WO2004110926A1 (de) | 2004-12-23 |
DE10326538A1 (de) | 2005-01-05 |
KR101088613B1 (ko) | 2011-11-30 |
EP1631523A1 (de) | 2006-03-08 |
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