JP2006290796A - 毛髪化粧料 - Google Patents
毛髪化粧料 Download PDFInfo
- Publication number
- JP2006290796A JP2006290796A JP2005113692A JP2005113692A JP2006290796A JP 2006290796 A JP2006290796 A JP 2006290796A JP 2005113692 A JP2005113692 A JP 2005113692A JP 2005113692 A JP2005113692 A JP 2005113692A JP 2006290796 A JP2006290796 A JP 2006290796A
- Authority
- JP
- Japan
- Prior art keywords
- hair
- acid
- weight
- component
- fatty acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
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- 125000004432 carbon atom Chemical group C* 0.000 claims description 32
- 239000000203 mixture Substances 0.000 claims description 27
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- 238000001035 drying Methods 0.000 description 19
- KWIUHFFTVRNATP-UHFFFAOYSA-N glycine betaine Chemical compound C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 description 19
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- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 3
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- ODKSFYDXXFIFQN-UHFFFAOYSA-N arginine Natural products OC(=O)C(N)CCCNC(N)=N ODKSFYDXXFIFQN-UHFFFAOYSA-N 0.000 description 3
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- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
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Classifications
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A—HUMAN NECESSITIES
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
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- A61Q5/00—Preparations for care of the hair
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- A—HUMAN NECESSITIES
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Emergency Medicine (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
【解決手段】 (a)アミドアミン(I)、(b)有機酸及び(c)炭素数8〜30の脂肪族アルコールを含有し、(b)成分の含有量が(a)成分のアミン当量に対して1.5〜10モル倍である毛髪化粧料。
【化1】
[式中、R1COは全脂肪酸残基中、C20以上の脂肪酸残基の割合が60重量%以上、C20の脂肪酸残基の割合が3重量%以上、及びC22の脂肪酸残基の割合が50〜95重量%である脂肪酸残基を示す。]
【選択図】 なし
Description
(a)一般式(I)で表されるアミドアミン(以下アミドアミン(I)という)
(b)有機酸
(c)炭素数8〜30の脂肪族アルコール
(d2) 窒素原子に炭素数1〜18のアルキル基が結合したN−アルキルピロリドン
(d3) アルキレン基の炭素数2〜4のアルキレンカーボネート
(d4) 分子量200〜5000のポリプロピレングリコール
(d5) 一般式(III)、(IV)又は(V)で表されるラクトン又は環状ケトン
(d1)としては、例えばp=q=0でかつZが水酸基ものとして、エタノール、1−プロパノール、2−プロパノール、ブタノール、イソブタノール等の一価のアルコール類が挙げられる。また、基R3−Ph−R4−を有するものとして、ベンジルアルコール、シンナミルアルコール、フェネチルアルコール、p−アニシルアルコール、p−メチルベンジルアルコール、フェノキシエタノール、2−ベンジルオキシエタノール等の芳香族アルコール類が挙げられる。さらに、エチレングリコール、プロピレングリコール、1,3−ブタンジオール、グリセリン等の多価アルコール類、メチルカルビトール、エチルカルビトール、プロピルカルビトール、ブチルカルビトール、トリエチレングリコールモノエチルエーテル、トリエチレングリコールモノブチルエーテル等が挙げられる。
例えば、BY11−026、BY22−19(東レ・ダウコーニング・シリコーン(株))、FZ−3125(日本ユニカー(株))等が挙げられる。
具体的には、SH200Cシリーズ、粘度1cs、50cs、200cs、1000cs、5000cs(東レ・ダウコーニング・シリコーン(株))等の市販品が含まれる。
具体的には、オクタメチルシクロテトラシロキサン、デカメチルシクロペンタシロキサン、ドデカメチルシクロヘキサシロキサン等が挙げられる。また、市販品としては、SH244やSH245(東レ・ダウコーニング・シリコーン(株))が挙げられる。
例えば、SS−3551、SF8452C、DC8500、DC929(以上東レ・ダウコーニング・シリコーン(株))、KT 1989(GE東芝社)が挙げられる。アミノ変性シリコーンを水性乳濁液として用いる場合、該水性乳濁液中に含まれるアミノ変性シリコーンの量は20〜60重量%が好ましく、30〜50重量%が更に好ましい。好ましいアミノ変性シリコーン水性乳濁液としては、SM8704C(東レ・ダウコーニング・シリコーン(株))等が挙げられる。
例えば、SH3771M(東レ・ダウコーニング・シリコーン(株))、SILSOFT A−843、SILSOFT SHINE(ともに日本ユニカー(株))等が挙げられる。
(vii)アルキル変性シリコーン
(viii)アミノ変性シロキサン−ポリオキシアルキレンブロック共重合体
一般式(IX)で表される共重合体が好ましく、例えばFZ−3789(日本ユニカー(株))等が挙げられる。
これらシリコーン類のうち、(i)高重合ジメチルポリシロキサン、(ii)ジメチルポリシロキサンオイル、(iii)環状シリコーン、(iv)アミノ変性シリコーン、(viii)アミノ変性シロキサン−ポリオキシアルキレンブロック共重合体、或いはそれらの混合物が好ましく、その中でも(iv)アミノ変性シリコーン、(viii)アミノ変性シロキサン−ポリオキシアルキレンブロック共重合体が特に好ましい。
カチオン性界面活性剤としては、一般式(X)で表される化合物が好ましい。
ここでR14、R15がアルキル基である場合は、炭素数16〜24、特に22のものが好ましく、また直鎖アルキル基であるのが好ましい。アニオンAn-としては、塩化物イオン、臭化物イオン等のハロゲン化物イオン、エチル硫酸イオン、炭酸メチルイオン等の有機アニオン等が挙げられ、ハロゲン化物イオン、特に塩化物イオンが好ましい。カチオン性界面活性剤としては、モノ長鎖四級アンモニウム塩が好ましく、具体的には、塩化ベヘニルトリメチルアンモニウム、塩化ステアリルトリメチルアンモニウム、塩化セチルトリメチルアンモニウム、塩化アラキルトリメチルアンモニウム等が挙げられ、特に塩化ベヘニルトリメチルアンモニウムが好ましい。
アニオン性界面活性剤としては、硫酸系、スルホン酸系及びカルボン酸系のものが挙げられる。具体的には、ポリオキシエチレンアルキルエーテル硫酸塩、ポリオキシエチレンアルケニルエーテル硫酸塩、アルキル硫酸塩、ポリオキシアルキレンアルキルフェニルエーテル硫酸塩、スルホコハク酸アルキルエステル塩、ポリオキシアルキレンスルホコハク酸アルキルエステル塩、アルカンスルホン酸塩、高級脂肪酸塩等が挙げられる。両性界面活性剤としては、ベタイン系界面活性剤等が挙げられる。このうち、アルキルジメチルアミノ酢酸ベタイン、脂肪酸アミドプロピルベタイン等のベタイン系界面活性剤がより好ましく、脂肪酸アミドプロピルベタインが特に好ましい。脂肪酸アミドプロピルベタインは、炭素数8〜18、特に炭素数10〜16のアシル基を有するものが好ましく、特にラウリン酸アミドプロピルベタイン、パーム核油脂肪酸アミドプロピルベタイン、ヤシ油脂肪酸アミドプロピルベタイン等が好ましい。
ベヘン酸(花王(株)ルナックBA)とジメチルアミノプロピルアミンを原料にアミド化反応して、ベヘン酸ジメチルアミノプロピルアミドを得た。純度は98%で、その他成分として、未反応原料のベヘン酸、アミン、水分などを含む。脂肪酸残基(R4CO)の組成は、C17H35CO/C19H39CO/C21H43CO/C23H47CO=1%/9%/88%/2%であった。
表1に示す組成の毛髪化粧料(ヘアコンディショナー)を以下の方法で調製し、以下の方法で粘度を測定し、以下の方法で官能評価を行い、更に以下の方法で毛髪内部の空洞補修率を測定した。結果を表1に示す。
(1)60℃に加熱した精製水に(b)成分を添加する(水相)。
(2)(a)成分、(c)成分及びその他成分を70℃で混合融解する(油相)。
(3)プロペラ攪拌(1L程度の製造で約250rpm)している水相に、(2)の油相を添加し、約30分間撹拌して乳化した。
粘度は、東機産業(株)のVISCOMETER TV−10を用い、30℃にて測定した。
毛髪束(パーマネントウェーブ処理を1回行った日本人女性毛髪20g、20cm)を、シャンプー3gを用いて洗浄した。このシャンプー組成は、ポリオキシエチレンアルキル(C12)エーテル硫酸ナトリウム(エチレンオキシド平均付加モル数2.5)15%、ジエタノールアミド3%、残部は水である。その後、調製したヘアコンディショナー2gを塗布し、およそ30秒間約40℃の流水下で濯ぎ、この毛髪に塗布してから濯ぎまで(湿潤時)について、滑らかさの評価を行った。ついでタオルドライを行い、ドライヤーで乾燥させた後に、滑らかさ、まとまり、つやの評価を行った。評価はパネラー8名が行い、下記の基準でランクづけした。
・評価基準
A;7人以上が効果あると回答
B;5〜6人が効果あると回答
C;3〜4人が効果あると回答
D;2人以下が効果あると回答
<毛髪内部の空洞補修率>
カラーダメージによりダメージの発生している毛束0.5gを上述シャンプー1gで洗浄した。軽く水を切った後、調製したヘアコンディショナー1gを塗布し、1分間放置してから更に4gを塗布して35℃で15分間放置した。次いで、流水で15秒間濯いだ後、タオルドライし、1分間ドライヤーで熱風乾燥した。以上の毛髪に対する処理は、日常におけるヘアコンディショナーの1週間連続使用に相当する。この処理を合計4回繰り返した。
下記組成のヘアコンディショナーを調製した。
製造例1のアミドアミン(I) 1.8%
ステアリルアルコール 6.0%
ベンジルオキシエタノール 0.7%
ジメチルポリシロキサン(重合度600) 1.0%
高重合ジメチルポリシロキサン(重合度2600) 1.2%
デカメチルシクロペンタシロキサン 1.5%
アミノ変性シリコーン−ポリオキシアルキレンブロック共重合体*1 0.2%
アミノ変性シリコーン*2 0.2%
乳酸 2.1%
グリコール酸 0.2%
ジペンタエリスルトール脂肪酸エステル*3 0.2%
ヒドロキシエチルセルロース*4 0.3%
香料、メチルパラベン 適量
精製水 残量
(pH3.2)
*1 日本ユニカー(株) FZ−3789
*2 東レ・ダウコーニング・シリコーン(株) SM−8704C
*3 日清製油(株) コスモール168AR
*4 ダイセル化学工業(株)SE−850K
このヘアコンディショナーは、毛髪を処理する際(湿潤時)のリッチ感、柔らかさ、滑らかさ、及び乾燥後の毛髪の柔らかさ、滑らかさ、まとまり、つや感が良好であった。
下記組成のトリートメント剤を調製した。
製造例1のアミドアミン(I) 2.0%
塩化ベヘニルトリメチルアンモニウム 0.3%
ステアリルアルコール 6.5%
ベヘニルアルコール 1.5%
イソノナン酸イソノニル 0.5%
ジメチルポリシロキサン(重合度600) 2.5%
高重合ジメチルポリシロキサン(重合度2600) 1.5%
アミノ変性シリコーン*2 1.0%
乳酸 0.5%
グリコール酸 1.5%
リンゴ酸 0.1%
ジプロピレングリコール 3.0%
ベンジルアルコール 0.2%
ベンジルオキシエタノール 1.5%
アルギニン*5 0.2%
パントテニルエチルエーテル 0.1%
香料、メチルパラベン 適量
精製水 残量
(pH3.2)
*5 川研ファインケミカル(株) L−アルギニン
このヘアトリートメント剤は、毛髪を処理する際(湿潤時)のリッチ感、柔らかさ、滑らかさ、及び乾燥後の毛髪の柔らかさ、滑らかさ、まとまり、つや感が良好であった。
Claims (4)
- 毛髪化粧料中の(c)成分の含有量が0.1〜20重量%である請求項1記載の毛髪化粧料。
- (b)成分の有機酸がヒドロキシカルボン酸又はジカルボン酸である請求項1又は2記載の毛髪化粧料。
- 更に、(d)有機溶剤を含有する請求項1〜3のいずれかに記載の毛髪化粧料。
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JP2005113692A JP4964428B2 (ja) | 2005-04-11 | 2005-04-11 | 毛髪化粧料 |
EP06731928.5A EP1870080A4 (en) | 2005-04-11 | 2006-04-10 | hair cosmetic |
PCT/JP2006/307992 WO2006109877A1 (ja) | 2005-04-11 | 2006-04-10 | 毛髪化粧料 |
US11/911,011 US7780956B2 (en) | 2005-04-11 | 2006-04-10 | Hair cosmetic |
CN2006800116923A CN101155575B (zh) | 2005-04-11 | 2006-04-10 | 毛发化妆品 |
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EP (1) | EP1870080A4 (ja) |
JP (1) | JP4964428B2 (ja) |
CN (1) | CN101155575B (ja) |
WO (1) | WO2006109877A1 (ja) |
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JP2021024807A (ja) * | 2019-08-05 | 2021-02-22 | 日本精化株式会社 | 毛髪空洞修復剤、及び、これを用いた毛髪空洞修復方法 |
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EP1870080A1 (en) | 2007-12-26 |
US7780956B2 (en) | 2010-08-24 |
JP4964428B2 (ja) | 2012-06-27 |
CN101155575A (zh) | 2008-04-02 |
CN101155575B (zh) | 2011-05-18 |
US20090068134A1 (en) | 2009-03-12 |
EP1870080A4 (en) | 2013-05-15 |
WO2006109877A1 (ja) | 2006-10-19 |
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