HUP0004623A2 - Eljárás zeolit LSX-ből álló, kis mennyiségű inert kötőanyagot tartalmazó szemcsés testek előállítására - Google Patents
Eljárás zeolit LSX-ből álló, kis mennyiségű inert kötőanyagot tartalmazó szemcsés testek előállításáraInfo
- Publication number
- HUP0004623A2 HUP0004623A2 HU0004623A HUP0004623A HUP0004623A2 HU P0004623 A2 HUP0004623 A2 HU P0004623A2 HU 0004623 A HU0004623 A HU 0004623A HU P0004623 A HUP0004623 A HU P0004623A HU P0004623 A2 HUP0004623 A2 HU P0004623A2
- Authority
- HU
- Hungary
- Prior art keywords
- zeolite
- obtaining
- binding material
- material ratio
- zeolite granular
- Prior art date
Links
- 229910021536 Zeolite Inorganic materials 0.000 title abstract 5
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 title abstract 5
- 239000010457 zeolite Substances 0.000 title abstract 5
- 239000000463 material Substances 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 abstract 3
- 239000011230 binding agent Substances 0.000 abstract 2
- 239000000047 product Substances 0.000 abstract 2
- 239000003513 alkali Substances 0.000 abstract 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 abstract 1
- 229910052782 aluminium Inorganic materials 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 229910052710 silicon Inorganic materials 0.000 abstract 1
- 239000010703 silicon Substances 0.000 abstract 1
- 239000012265 solid product Substances 0.000 abstract 1
- 238000001179 sorption measurement Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
- C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
- C01B39/20—Faujasite type, e.g. type X or Y
- C01B39/22—Type X
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
- B01J20/16—Alumino-silicates
- B01J20/18—Synthetic zeolitic molecular sieves
- B01J20/183—Physical conditioning without chemical treatment, e.g. drying, granulating, coating, irradiation
Abstract
A találmány alacsony szilícium/alumínium arányú, inert kötőanyagotcsekély mennyiségben tartalmazó faujazitagglomerátumok előállításáravonatkozik. Az eljárás a következő lépésekből áll: a) egy zeolit LSXport olyan kötőanyaggal tömörítenek, amely legalább 80 tömeg% zeolittáalakítható anyagot tartalmaz; b) az a) lépésben kapott keveréketalakozzák; c) a kapott terméket szárítják, majd 500-600 °Chőmérsékleten kalcinálják; d) a c) lépésből eredő szilárd terméketlegalább 0,5 moláris vizes lúgoldattal hozzák érintkezésbe; e) az ígykapott terméket mossák, szárítják és 500-600 °C hőmérsékletenaktiválják. A találmány tárgyát képezik azok a legalább 95 tömeg%zeolit LSX-et tartalmazó zeolittestek is, amelyek toluoladszorpcióskapacitása legalább 21,5%. Ó
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR9709283A FR2766475B1 (fr) | 1997-07-22 | 1997-07-22 | Procede pour l'obtention de corps granulaires en zeolite lsx a faible taux de liant inerte |
PCT/FR1998/001508 WO1999005063A1 (fr) | 1997-07-22 | 1998-07-10 | Procede pour l'obtention de corps granulaires en zeolite lsx a faible taux de liant inerte |
Publications (3)
Publication Number | Publication Date |
---|---|
HUP0004623A2 true HUP0004623A2 (hu) | 2001-04-28 |
HUP0004623A3 HUP0004623A3 (en) | 2006-04-28 |
HU225582B1 HU225582B1 (en) | 2007-03-28 |
Family
ID=9509470
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
HU0004623A HU225582B1 (en) | 1997-07-22 | 1998-07-10 | Method for obtaining lsx zeolite granular agglomerates with low inert binding material ratio |
Country Status (26)
Country | Link |
---|---|
US (1) | US6264881B1 (hu) |
EP (1) | EP0932581B1 (hu) |
JP (2) | JP4195516B2 (hu) |
KR (1) | KR100538961B1 (hu) |
CN (1) | CN1109653C (hu) |
AR (1) | AR017755A1 (hu) |
AT (1) | ATE236083T1 (hu) |
AU (1) | AU736403B2 (hu) |
BR (1) | BR9806072A (hu) |
CA (1) | CA2266385C (hu) |
CZ (1) | CZ294449B6 (hu) |
DE (1) | DE69812872T2 (hu) |
DK (1) | DK0932581T3 (hu) |
EA (1) | EA001175B1 (hu) |
ES (1) | ES2195367T3 (hu) |
FR (1) | FR2766475B1 (hu) |
HU (1) | HU225582B1 (hu) |
MY (1) | MY125860A (hu) |
PL (1) | PL192559B1 (hu) |
PT (1) | PT932581E (hu) |
SK (1) | SK284360B6 (hu) |
TR (1) | TR199900628T1 (hu) |
TW (1) | TW460411B (hu) |
UA (1) | UA61932C2 (hu) |
WO (1) | WO1999005063A1 (hu) |
ZA (1) | ZA986398B (hu) |
Families Citing this family (32)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2789914B1 (fr) | 1999-02-22 | 2001-04-06 | Ceca Sa | Adsorbants zeolitiques agglomeres a faible taux de liant inerte, leur procede d'obtention et leurs utilisations |
FR2800995B1 (fr) | 1999-10-05 | 2002-01-04 | Ceca Sa | Adsorbants zeolitiques, leur procede d'obtention et leur utilisation pour la decarbonation de flux gazeux |
FR2799646B1 (fr) | 1999-10-15 | 2001-12-07 | Oreal | Composition sous forme d'emulsion eau-dans-huile, contenant des fibres, et son utilisation dans le domaine cosmetique |
JP4830185B2 (ja) * | 1999-11-25 | 2011-12-07 | 東ソー株式会社 | 高純度低シリカx型ゼオライトバインダレス成形体およびそれを使用した気体分離方法 |
FR2803282B1 (fr) | 2000-01-04 | 2002-02-15 | Ceca Sa | Zeolites x echangees notamment au litium, leur procede de preparation et leur utilisation comme adsorbants de l'azote dans la separation des gaz de l'air |
DE60120819T2 (de) | 2000-04-04 | 2007-06-28 | Tosoh Corp., Shin-Nanyo | Verfahren zur adsorptiven Trennung von Kohlendioxid |
DE60129626T2 (de) | 2000-04-20 | 2008-05-21 | Tosoh Corp., Shinnanyo | Verfahren zum Reinigen von einem Wasserstoff enthaltenden Gasgemisch |
FR2811313B1 (fr) | 2000-07-07 | 2002-08-30 | Ceca Sa | Procede de preparation de zeolites x et lsx agglomerees et echangees au lithium |
US6416569B1 (en) | 2000-08-28 | 2002-07-09 | The Boc Group, Inc. | Temperature swing adsorption process |
US6409800B1 (en) | 2000-08-28 | 2002-06-25 | The Boc Group, Inc. | Temperature swing adsorption process |
US6432171B1 (en) | 2000-08-28 | 2002-08-13 | The Boc Group, Inc. | Thermal swing adsorption process |
US6596256B1 (en) | 2000-08-28 | 2003-07-22 | The Boc Group, Inc. | Synthesis of low silicon sodium X zeolite |
US6506236B2 (en) * | 2001-03-28 | 2003-01-14 | Air Products And Chemicals, Inc. | Process for reducing the level of carbon dioxide in a gaseous mixture |
EP1633475B1 (en) * | 2003-06-06 | 2010-06-23 | Zeochem AG | Method for sulfur compounds removal from contaminated gas and liquid streams |
FR2863909B1 (fr) * | 2003-12-22 | 2006-05-26 | Ceca Sa | Methode de purification de flux gazeux pollue par co2 et hydrocarbure(s) et/ou oxyde(s) d'azote par adsorbant zeolitique agglomere |
FR2925366B1 (fr) * | 2007-12-20 | 2011-05-27 | Ceca Sa | Adsorbants zeolitiques agglomeres, leur procede de preparation et leurs utilisations |
FR2925478B1 (fr) * | 2007-12-20 | 2009-12-18 | Ceca Sa | Zeolite de type lsx a granulometrie controlee |
KR101073682B1 (ko) | 2008-07-31 | 2011-10-14 | 한국지질자원연구원 | Fe-제올라이트를 사용한 암모니아 가스흡착제 제조방법 |
US7812208B2 (en) * | 2008-09-22 | 2010-10-12 | Uop Llc | Binderless adsorbents with improved mass transfer properties and their use in the adsorptive separation of para-xylene |
GB201012287D0 (en) * | 2010-07-22 | 2010-09-08 | Ibr Consult B V | Production of fired ceramic articles |
DE102011104006A1 (de) | 2010-12-10 | 2012-06-14 | Süd-Chemie AG | Granulierte Zeolithe mit hoher Adsorptionskapazität zur Adsorption von organischen Molekülen |
RU2465046C1 (ru) * | 2011-08-01 | 2012-10-27 | Учреждение Российской академии наук Институт катализа им. Г.К. Борескова Сибирского отделения РАН | Композитный адсорбционно-каталитический материал для фотокаталитического окисления |
WO2013115878A2 (en) * | 2011-11-10 | 2013-08-08 | Sandia Corporation | Pelletized molecular sieves and method of making pelletized molecular sieves |
FR3009299B1 (fr) * | 2013-08-05 | 2019-11-15 | Arkema France | Materiau zeolithique a base de zeolithe mesoporeuse |
FR3013236B1 (fr) * | 2013-11-20 | 2015-12-11 | Ceca Sa | Materiau granulaire zeolithique a structure connexe |
RU2625873C1 (ru) * | 2016-06-09 | 2017-07-19 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Тамбовский государственный технический университет" ФГБОУ ВО "ТГТУ" | Способ получения композиционного сорбционно-активного материала |
CN106629763B (zh) * | 2016-12-27 | 2018-12-04 | 苏州立昂新材料有限公司 | 低硅八面沸石及其制备方法 |
WO2019068135A1 (en) * | 2017-10-04 | 2019-04-11 | Neomaterials Pty Ltd | SYNTHESIS OF ZEOLITES |
CN110508241B (zh) * | 2018-05-22 | 2022-12-09 | 中国石油化工股份有限公司 | 一种聚结型吸附剂及其制备方法 |
CN110508240B (zh) * | 2018-05-22 | 2021-12-17 | 中国石油化工股份有限公司 | 一种聚结型吸附剂的制备方法 |
CN109485058A (zh) * | 2018-12-11 | 2019-03-19 | 中国地质科学院郑州矿产综合利用研究所 | 一种无粘结剂lsx分子筛的制备方法 |
CN112592148B (zh) * | 2021-01-24 | 2022-06-28 | 湖南科技大学 | 高掺量利用砖混类建筑固废再生砂粉制备结构材料的方法 |
Family Cites Families (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE299635C (hu) | ||||
US3119660A (en) | 1960-09-26 | 1964-01-28 | Union Carbide Corp | Process for producing molecular sieve bodies |
US3906076A (en) * | 1973-10-03 | 1975-09-16 | Grace W R & Co | Process for producing zeolite X molecular sieve bodies |
US4603040A (en) * | 1985-03-27 | 1986-07-29 | Air Products And Chemicals, Inc. | Massive bodies of Maximum Aluminum X-type zeolite |
DD299635A5 (de) * | 1990-02-20 | 1992-04-30 | Bitterfeld Chemie | Verfahren zur herstellung von zeolithischen adsorptionsmitteln |
JPH04198011A (ja) * | 1990-11-28 | 1992-07-17 | Tosoh Corp | バインダーレスx型ゼオライト成形体の製造方法 |
JP3066430B2 (ja) * | 1991-12-10 | 2000-07-17 | 東ソー株式会社 | ゼオライトx型成形体の製造方法 |
US5152813A (en) * | 1991-12-20 | 1992-10-06 | Air Products And Chemicals, Inc. | Nitrogen adsorption with a Ca and/or Sr exchanged lithium X-zeolite |
JP3066850B2 (ja) * | 1992-12-22 | 2000-07-17 | 東ソー株式会社 | バインダーレスx型ゼオライト成形体およびその製造方法 |
EP0826631B1 (en) * | 1996-08-30 | 2001-12-05 | Tosoh Corporation | Heat-resistant low-silica zeolite, and process for production and application thereof |
JP3257509B2 (ja) * | 1997-11-27 | 2002-02-18 | 東ソー株式会社 | 低シリカフォージャサイト型ゼオライトおよびその製造方法 |
-
1997
- 1997-07-22 FR FR9709283A patent/FR2766475B1/fr not_active Expired - Fee Related
-
1998
- 1998-07-10 PL PL332286A patent/PL192559B1/pl unknown
- 1998-07-10 US US09/269,078 patent/US6264881B1/en not_active Expired - Lifetime
- 1998-07-10 JP JP50939899A patent/JP4195516B2/ja not_active Expired - Fee Related
- 1998-07-10 CN CN98801034A patent/CN1109653C/zh not_active Expired - Fee Related
- 1998-07-10 ES ES98937616T patent/ES2195367T3/es not_active Expired - Lifetime
- 1998-07-10 PT PT98937616T patent/PT932581E/pt unknown
- 1998-07-10 SK SK362-99A patent/SK284360B6/sk not_active IP Right Cessation
- 1998-07-10 EA EA199900318A patent/EA001175B1/ru not_active IP Right Cessation
- 1998-07-10 CA CA002266385A patent/CA2266385C/fr not_active Expired - Fee Related
- 1998-07-10 HU HU0004623A patent/HU225582B1/hu not_active IP Right Cessation
- 1998-07-10 AU AU86349/98A patent/AU736403B2/en not_active Ceased
- 1998-07-10 CZ CZ19991008A patent/CZ294449B6/cs not_active IP Right Cessation
- 1998-07-10 DE DE69812872T patent/DE69812872T2/de not_active Expired - Lifetime
- 1998-07-10 BR BR9806072A patent/BR9806072A/pt not_active IP Right Cessation
- 1998-07-10 WO PCT/FR1998/001508 patent/WO1999005063A1/fr active IP Right Grant
- 1998-07-10 AT AT98937616T patent/ATE236083T1/de not_active IP Right Cessation
- 1998-07-10 KR KR10-1999-7002376A patent/KR100538961B1/ko not_active IP Right Cessation
- 1998-07-10 EP EP98937616A patent/EP0932581B1/fr not_active Expired - Lifetime
- 1998-07-10 TR TR1999/00628T patent/TR199900628T1/xx unknown
- 1998-07-10 DK DK98937616T patent/DK0932581T3/da active
- 1998-07-15 TW TW087111531A patent/TW460411B/zh active
- 1998-07-17 ZA ZA986398A patent/ZA986398B/xx unknown
- 1998-07-22 MY MYPI98003359A patent/MY125860A/en unknown
- 1998-07-22 AR ARP980103584A patent/AR017755A1/es active IP Right Grant
- 1998-10-07 UA UA99042261A patent/UA61932C2/uk unknown
-
2008
- 2008-05-01 JP JP2008119499A patent/JP4302766B2/ja not_active Expired - Fee Related
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Legal Events
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MM4A | Lapse of definitive patent protection due to non-payment of fees |