HRP20020141B1 - METHOD FOR THE PREPARATION OF 2-METHOXY-4-(N-t-BUTYLAMINO-CARBONYL)-BENZENESULFONYL CHLORIDE - Google Patents
METHOD FOR THE PREPARATION OF 2-METHOXY-4-(N-t-BUTYLAMINO-CARBONYL)-BENZENESULFONYL CHLORIDEInfo
- Publication number
- HRP20020141B1 HRP20020141B1 HR20020141A HRP20020141A HRP20020141B1 HR P20020141 B1 HRP20020141 B1 HR P20020141B1 HR 20020141 A HR20020141 A HR 20020141A HR P20020141 A HRP20020141 A HR P20020141A HR P20020141 B1 HRP20020141 B1 HR P20020141B1
- Authority
- HR
- Croatia
- Prior art keywords
- acid
- methoxy
- formula
- group
- chloride
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 2
- FQBFGERKZZFZNX-UHFFFAOYSA-N 4-(tert-butylcarbamoyl)-2-methoxybenzenesulfonyl chloride Chemical compound COC1=CC(C(=O)NC(C)(C)C)=CC=C1S(Cl)(=O)=O FQBFGERKZZFZNX-UHFFFAOYSA-N 0.000 title 1
- IJFXRHURBJZNAO-UHFFFAOYSA-N meta--hydroxybenzoic acid Natural products OC(=O)C1=CC=CC(O)=C1 IJFXRHURBJZNAO-UHFFFAOYSA-N 0.000 abstract 3
- 150000003839 salts Chemical class 0.000 abstract 3
- NGNBDVOYPDDBFK-UHFFFAOYSA-N 2-[2,4-di(pentan-2-yl)phenoxy]acetyl chloride Chemical group CCCC(C)C1=CC=C(OCC(Cl)=O)C(C(C)CCC)=C1 NGNBDVOYPDDBFK-UHFFFAOYSA-N 0.000 abstract 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 2
- 238000006243 chemical reaction Methods 0.000 abstract 2
- 150000001875 compounds Chemical class 0.000 abstract 2
- 230000011987 methylation Effects 0.000 abstract 2
- 238000007069 methylation reaction Methods 0.000 abstract 2
- 238000006277 sulfonation reaction Methods 0.000 abstract 2
- YBRBMKDOPFTVDT-UHFFFAOYSA-N tert-butylamine Chemical compound CC(C)(C)N YBRBMKDOPFTVDT-UHFFFAOYSA-N 0.000 abstract 2
- DNUYOWCKBJFOGS-UHFFFAOYSA-N 2-[[10-(2,2-dicarboxyethyl)anthracen-9-yl]methyl]propanedioic acid Chemical compound C1=CC=C2C(CC(C(=O)O)C(O)=O)=C(C=CC=C3)C3=C(CC(C(O)=O)C(O)=O)C2=C1 DNUYOWCKBJFOGS-UHFFFAOYSA-N 0.000 abstract 1
- RFXNLHJLTSWQDE-UHFFFAOYSA-N 3-hydroxy-4-sulfobenzoic acid Chemical compound OC(=O)C1=CC=C(S(O)(=O)=O)C(O)=C1 RFXNLHJLTSWQDE-UHFFFAOYSA-N 0.000 abstract 1
- VQCHPXGONTUEPJ-UHFFFAOYSA-N 3-methoxy-4-sulfobenzoic acid Chemical compound COC1=CC(C(O)=O)=CC=C1S(O)(=O)=O VQCHPXGONTUEPJ-UHFFFAOYSA-N 0.000 abstract 1
- QWEZBKWXCKXTJG-UHFFFAOYSA-N 4-chlorosulfonyl-3-methoxybenzoyl chloride Chemical compound COC1=CC(C(Cl)=O)=CC=C1S(Cl)(=O)=O QWEZBKWXCKXTJG-UHFFFAOYSA-N 0.000 abstract 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 abstract 1
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- 150000001340 alkali metals Chemical class 0.000 abstract 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-O ammonium group Chemical group [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 abstract 1
- CSKNSYBAZOQPLR-UHFFFAOYSA-N benzenesulfonyl chloride Chemical compound ClS(=O)(=O)C1=CC=CC=C1 CSKNSYBAZOQPLR-UHFFFAOYSA-N 0.000 abstract 1
- 125000002843 carboxylic acid group Chemical group 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 abstract 1
- 239000003444 phase transfer catalyst Substances 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 125000000542 sulfonic acid group Chemical group 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/32—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of salts of sulfonic acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/02—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof
- C07C303/04—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof by substitution of hydrogen atoms by sulfo or halosulfonyl groups
- C07C303/06—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof by substitution of hydrogen atoms by sulfo or halosulfonyl groups by reaction with sulfuric acid or sulfur trioxide
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/02—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof
- C07C303/22—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof from sulfonic acids, by reactions not involving the formation of sulfo or halosulfonyl groups; from sulfonic halides by reactions not involving the formation of halosulfonyl groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C309/00—Sulfonic acids; Halides, esters, or anhydrides thereof
- C07C309/01—Sulfonic acids
- C07C309/28—Sulfonic acids having sulfo groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton
- C07C309/57—Sulfonic acids having sulfo groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton containing carboxyl groups bound to the carbon skeleton
- C07C309/60—Sulfonic acids having sulfo groups bound to carbon atoms of six-membered aromatic rings of a carbon skeleton containing carboxyl groups bound to the carbon skeleton the carbon skeleton being further substituted by singly-bound oxygen atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| HU9902375A HU225150B1 (en) | 1999-07-15 | 1999-07-15 | Novel process for producing 2-methoxy-4-(t-butylaminocarbonyl)-benzenesulfonyl chloride |
| PCT/HU2000/000080 WO2001005754A1 (en) | 1999-07-15 | 2000-07-13 | Method for the preparation of 2-methoxy-4-(n-t-butylamino-carbonyl)-benzenesulfonyl chloride |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| HRP20020141A2 HRP20020141A2 (en) | 2003-10-31 |
| HRP20020141B1 true HRP20020141B1 (en) | 2010-09-30 |
Family
ID=89998737
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| HR20020141A HRP20020141B1 (en) | 1999-07-15 | 2002-02-14 | METHOD FOR THE PREPARATION OF 2-METHOXY-4-(N-t-BUTYLAMINO-CARBONYL)-BENZENESULFONYL CHLORIDE |
Country Status (17)
| Country | Link |
|---|---|
| US (1) | US6548702B1 (hu) |
| EP (1) | EP1202960B1 (hu) |
| JP (1) | JP4636761B2 (hu) |
| CN (1) | CN1164571C (hu) |
| AT (1) | ATE261430T1 (hu) |
| AU (1) | AU6308300A (hu) |
| BR (1) | BR0012430B1 (hu) |
| CA (1) | CA2378337C (hu) |
| CZ (1) | CZ2002146A3 (hu) |
| DE (1) | DE60008884T2 (hu) |
| ES (1) | ES2215699T3 (hu) |
| HR (1) | HRP20020141B1 (hu) |
| HU (1) | HU225150B1 (hu) |
| MX (1) | MXPA01013342A (hu) |
| PL (1) | PL199425B1 (hu) |
| SK (1) | SK286031B6 (hu) |
| WO (1) | WO2001005754A1 (hu) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ES2240781T3 (es) * | 2001-07-31 | 2005-10-16 | Sanofi-Aventis | Procedimiento para la preparacion de derivados de 3-spiro(ciclohexan-1,3'-(3h)indolin-2'-ona). |
| CN105621518A (zh) * | 2015-12-29 | 2016-06-01 | 浙江奇彩环境科技股份有限公司 | 一种3,4-二氯苯磺酸废水的资源化处理方法 |
| CN110372548A (zh) * | 2018-04-12 | 2019-10-25 | 南京化学试剂股份有限公司 | 一种5-磺基水杨酸的精制方法 |
| CN113402437B (zh) * | 2021-06-29 | 2023-07-14 | 河北维达康生物科技有限公司 | 一种合成膳食补充剂褪黑素的新方法 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3953507A (en) * | 1973-08-31 | 1976-04-27 | Stauffer Chemical Company | N-t-butyl-α-(3,5-substituted phenoxy) alkyl amides and their use as herbicides |
| WO1997015556A1 (fr) * | 1995-10-24 | 1997-05-01 | Sanofi | Derives 3-spiro-indolin-2-one comme ligands des recepteurs de la vasopressine et/ou de l'ocytocine |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2757157B1 (fr) * | 1996-12-13 | 1999-12-31 | Sanofi Sa | Derives d'indolin-2-one, procede pour leur preparation et compositions pharmaceutiques les contenant |
-
1999
- 1999-07-15 HU HU9902375A patent/HU225150B1/hu not_active IP Right Cessation
-
2000
- 2000-07-13 ES ES00949824T patent/ES2215699T3/es not_active Expired - Lifetime
- 2000-07-13 WO PCT/HU2000/000080 patent/WO2001005754A1/en active IP Right Grant
- 2000-07-13 PL PL352466A patent/PL199425B1/pl not_active IP Right Cessation
- 2000-07-13 AT AT00949824T patent/ATE261430T1/de not_active IP Right Cessation
- 2000-07-13 JP JP2001511415A patent/JP4636761B2/ja not_active Expired - Fee Related
- 2000-07-13 MX MXPA01013342A patent/MXPA01013342A/es active IP Right Grant
- 2000-07-13 CA CA002378337A patent/CA2378337C/en not_active Expired - Fee Related
- 2000-07-13 AU AU63083/00A patent/AU6308300A/en not_active Abandoned
- 2000-07-13 BR BRPI0012430-3A patent/BR0012430B1/pt not_active IP Right Cessation
- 2000-07-13 SK SK47-2002A patent/SK286031B6/sk not_active IP Right Cessation
- 2000-07-13 CN CNB008102945A patent/CN1164571C/zh not_active Expired - Fee Related
- 2000-07-13 CZ CZ2002146A patent/CZ2002146A3/cs unknown
- 2000-07-13 DE DE60008884T patent/DE60008884T2/de not_active Expired - Lifetime
- 2000-07-13 EP EP00949824A patent/EP1202960B1/en not_active Expired - Lifetime
- 2000-07-13 US US10/030,655 patent/US6548702B1/en not_active Expired - Fee Related
-
2002
- 2002-02-14 HR HR20020141A patent/HRP20020141B1/xx not_active IP Right Cessation
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3953507A (en) * | 1973-08-31 | 1976-04-27 | Stauffer Chemical Company | N-t-butyl-α-(3,5-substituted phenoxy) alkyl amides and their use as herbicides |
| WO1997015556A1 (fr) * | 1995-10-24 | 1997-05-01 | Sanofi | Derives 3-spiro-indolin-2-one comme ligands des recepteurs de la vasopressine et/ou de l'ocytocine |
Also Published As
| Publication number | Publication date |
|---|---|
| CA2378337C (en) | 2008-05-20 |
| CZ2002146A3 (cs) | 2002-11-13 |
| CN1164571C (zh) | 2004-09-01 |
| CN1360569A (zh) | 2002-07-24 |
| HU225150B1 (en) | 2006-07-28 |
| ATE261430T1 (de) | 2004-03-15 |
| DE60008884T2 (de) | 2005-02-03 |
| BR0012430A (pt) | 2002-03-26 |
| AU6308300A (en) | 2001-02-05 |
| BR0012430B1 (pt) | 2011-05-17 |
| PL352466A1 (en) | 2003-08-25 |
| WO2001005754A1 (en) | 2001-01-25 |
| JP4636761B2 (ja) | 2011-02-23 |
| HU9902375D0 (en) | 1999-10-28 |
| ES2215699T3 (es) | 2004-10-16 |
| EP1202960B1 (en) | 2004-03-10 |
| EP1202960A1 (en) | 2002-05-08 |
| HRP20020141A2 (en) | 2003-10-31 |
| CA2378337A1 (en) | 2001-01-25 |
| HUP9902375A2 (hu) | 2001-05-28 |
| MXPA01013342A (es) | 2002-08-20 |
| DE60008884D1 (de) | 2004-04-15 |
| SK286031B6 (sk) | 2008-01-07 |
| SK472002A3 (en) | 2003-02-04 |
| PL199425B1 (pl) | 2008-09-30 |
| HUP9902375A3 (en) | 2002-11-28 |
| US6548702B1 (en) | 2003-04-15 |
| JP2003505366A (ja) | 2003-02-12 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US6001831A (en) | Process for producing quinazoline derivatives | |
| GB779389A (en) | A stable solid diazonium compound and process for making it | |
| HRP20020141B1 (en) | METHOD FOR THE PREPARATION OF 2-METHOXY-4-(N-t-BUTYLAMINO-CARBONYL)-BENZENESULFONYL CHLORIDE | |
| ITMI20101076A1 (it) | Procedimento per la preparazione di derivati pteridinici | |
| HRP20010798B1 (en) | Processes for preparing pesticidal intermediates | |
| JPH01146860A (ja) | ポリアルキレングリコールナフチル−３−スルホプロピルジエーテル化合物およびその塩、その調製方法並びにこれらを含有する電気めっき浴 | |
| ES2169891T3 (es) | Procedimiento para la produccion de compuestos de alcoxicarboniltioarilio. | |
| US4188320A (en) | Ester of higher fatty acid and reagent for determination of activity of lipase | |
| PL85216B1 (hu) | ||
| KR20120100977A (ko) | 2-티오히스티딘 및 이것의 유사체의 합성법 | |
| US4266057A (en) | Process for the preparation of 2-isopropylamino pyrimidine | |
| US3480636A (en) | Process for preparing alpha-nitrosulfonic acids | |
| PL91814B1 (hu) | ||
| JPS60258155A (ja) | アシルオキシベンゾールスルホン酸、そのアルカリ金属塩及びアルカリ土類金属塩の製法 | |
| PL128450B1 (en) | Process for preparing derivatives of benzimidazole | |
| US4113738A (en) | Conversion of N-tosylsulfoximides to sulfoximines | |
| US3074948A (en) | Heterocyclic nitrogen compounds containing sulfonyl fluoride groups and method of producing same | |
| PL444846A1 (pl) | Sposób otrzymywania czwartorzędowych soli amoniowych z kationem 3-karbamoilo-1-alkilopirydyniowym i anionem salicylanowym | |
| SU1402598A1 (ru) | Способ получени 2,4-динитробензолсульфоната натри | |
| PL205784B1 (pl) | Sposób otrzymywania tiofenolu | |
| CA2320173A1 (en) | Synthesis of 1-(2-sulphoethyl)-pyridinium betaine | |
| DE60020539D1 (de) | Verfahren zur herstellung von thiobarbitursäurederivaten | |
| PL94941B1 (hu) | ||
| DE4444694A1 (de) | Verfahren zur Herstellung von Methylsulfonylaromaten durch Methylierung von Arylsulfinsäuren unter Verwendung von Methylchlorid | |
| JPH07242638A (ja) | アリールスルホナート誘導体の製造方法 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A1OB | Publication of a patent application | ||
| ARAI | Request for the grant of a patent on the basis of the submitted results of a substantive examination of a patent application | ||
| PNAN | Change of the applicant name, address/residence |
Owner name: SANOFI-AVENTIS, FR |
|
| ODRP | Renewal fee for the maintenance of a patent |
Payment date: 20100813 Year of fee payment: 11 |
|
| B1PR | Patent granted | ||
| PBON | Lapse due to non-payment of renewal fee |
Effective date: 20110714 |