FR2983628A1 - Condensateur electrolytique humide contenant un electrolyte de travail gelifie - Google Patents
Condensateur electrolytique humide contenant un electrolyte de travail gelifie Download PDFInfo
- Publication number
- FR2983628A1 FR2983628A1 FR1203255A FR1203255A FR2983628A1 FR 2983628 A1 FR2983628 A1 FR 2983628A1 FR 1203255 A FR1203255 A FR 1203255A FR 1203255 A FR1203255 A FR 1203255A FR 2983628 A1 FR2983628 A1 FR 2983628A1
- Authority
- FR
- France
- Prior art keywords
- acid
- electrolytic capacitor
- weight
- electrolyte
- wet electrolytic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
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Classifications
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- H01G9/00—Electrolytic capacitors, rectifiers, detectors, switching devices, light-sensitive or temperature-sensitive devices; Processes of their manufacture
- H01G9/004—Details
- H01G9/022—Electrolytes; Absorbents
- H01G9/035—Liquid electrolytes, e.g. impregnating materials
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- H—ELECTRICITY
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- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G13/00—Apparatus specially adapted for manufacturing capacitors; Processes specially adapted for manufacturing capacitors not provided for in groups H01G4/00 - H01G11/00
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- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G9/00—Electrolytic capacitors, rectifiers, detectors, switching devices, light-sensitive or temperature-sensitive devices; Processes of their manufacture
- H01G9/0029—Processes of manufacture
- H01G9/0036—Formation of the solid electrolyte layer
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G9/00—Electrolytic capacitors, rectifiers, detectors, switching devices, light-sensitive or temperature-sensitive devices; Processes of their manufacture
- H01G9/004—Details
- H01G9/022—Electrolytes; Absorbents
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- H01G9/028—Organic semiconducting electrolytes, e.g. TCNQ
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- H—ELECTRICITY
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- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G9/00—Electrolytic capacitors, rectifiers, detectors, switching devices, light-sensitive or temperature-sensitive devices; Processes of their manufacture
- H01G9/145—Liquid electrolytic capacitors
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/54—Electrolytes
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/54—Electrolytes
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/54—Electrolytes
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G9/00—Electrolytic capacitors, rectifiers, detectors, switching devices, light-sensitive or temperature-sensitive devices; Processes of their manufacture
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- H01G9/04—Electrodes or formation of dielectric layers thereon
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G9/00—Electrolytic capacitors, rectifiers, detectors, switching devices, light-sensitive or temperature-sensitive devices; Processes of their manufacture
- H01G9/004—Details
- H01G9/04—Electrodes or formation of dielectric layers thereon
- H01G9/048—Electrodes or formation of dielectric layers thereon characterised by their structure
- H01G9/052—Sintered electrodes
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T29/00—Metal working
- Y10T29/43—Electric condenser making
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Microelectronics & Electronic Packaging (AREA)
- Manufacturing & Machinery (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Electric Double-Layer Capacitors Or The Like (AREA)
Abstract
Description
Claims (42)
- REVENDICATIONS1. Condensateur électrolytique humide comprenant : une anode comprenant une pastille oxydée anodiquement formée à partir d'une poudre pressée et frittée ; une cathode qui comprend un substrat de métal revêtu avec un polymère conducteur ; et un électrolyte de travail en communication avec l'anode et la cathode, dans lequel l'électrolyte de travail se présente sous la forme d'un gel et comprend 10 un sel d'ammonium d'un acide organique, des particules d'oxyde inorganiques, et un acide, et un système de solvants qui comprend de l'eau, dans lequel l'électrolyte de travail a une valeur de pH d'environ 5,0 à environ 8,0. 15
- 2. Condensateur électrolytique humide selon la revendication 1, dans lequel l'électrolyte de travail a une valeur de pH d'environ 6,0 à environ 7,0.
- 3. Condensateur électrolytique humide selon la revendication 1, dans lequel l'électrolyte de travail a 20 une conductivité d'environ 10 à environ 80 milliSiemens par centimètre, déterminée à une température de 25 °C.
- 4. Condensateur électrolytique humide selon la revendication 1, dans lequel l'électrolyte de travail a une conductivité d'environ 20 à environ 60 milliSiemens 25 par centimètre, déterminée à une température de 25 °C.
- 5. Condensateur électrolytique humide selon la revendication 1, dans lequel l'électrolyte de travail affiche un angle de phase S de 0° à environ 20°.
- 6. Condensateur électrolytique humide selon la revendication 1, dans lequel l'électrolyte de travail affiche un angle de phase b d'environ 0,2° à environ 2°.
- 7. Condensateur électrolytique humide selon la revendication 1, dans lequel l'électrolyte de travail affiche un module de conservation G' d'environ 5 kilopascals ou plus.
- 8. Condensateur électrolytique humide selon la revendication 1, dans lequel le condensateur est capable d'être chargé à une tension de service d'environ 200 volts à environ 240 volts, et dans lequel la pastille de l'anode est oxydée anodiquement à une tension de formation d'environ 220 volts à environ 250 volts.
- 9. Condensateur électrolytique humide selon la revendication 1, dans lequel l'acide organique du sel d'ammonium est un acide polyprotique.
- 10. Condensateur électrolytique humide selon la 20 revendication 9, dans lequel l'acide polyprotique est l'acide adipique, l'acide a-tartrique, l'acide méso- tartrique, l'acide oxalique, l'acide lactique, ou une combinaison de ceux-ci.
- 11. Condensateur électrolytique humide selon la 25 revendication 1, dans lequel des sels d'ammonium d'acides organiques constituent d'environ 5 % en poids à environ 35 % en poids de l'électrolyte de travail.
- 12. Condensateur électrolytique humide selon la revendication 1, dans lequel l'acide inclut l'acide 30 éthylènediaminetétraacétique.
- 13. Condensateur électrolytique humide selon la revendication 1, dans lequel les acides constituent d'environ 0,01 % en poids à environ 10 % en poids de l'électrolyte de travail.
- 14. Condensateur électrolytique humide selon la revendication 1, dans lequel le système de solvants inclut en outre un solvant secondaire.
- 15. Condensateur électrolytique humide selon la revendication 14, dans lequel le solvant secondaire est l'éthylène glycol.
- 16. Condensateur électrolytique humide selon la revendication 14, dans lequel l'eau constitue d'environ 35 % en poids à environ 66 % en poids de l'électrolyte et les solvants secondaires constituent d'environ 10 % en poids à environ 35 % en poids de l'électrolyte.
- 17. Condensateur électrolytique humide selon la revendication 1, dans lequel les particules d'oxyde inorganiques constituent d'environ 1 % en poids à environ 15 % en poids de l'électrolyte.
- 18. Condensateur électrolytique humide selon la revendication 1, dans lequel les particules d'oxyde inorganiques ont une taille moyenne de particule d'environ 1 à environ 500 nanomètres et une surface spécifique d'environ 100 m2/g à environ 600 m2/g.
- 19. Condensateur électrolytique humide selon la revendication 1, dans lequel les particules d'oxyde inorganiques sont des particules de silice fumée.
- 20. Condensateur électrolytique humide selon la revendication 1, dans lequel l'anode est plane et a une 30 épaisseur d'environ 5 millimètres ou moins.
- 21. Condensateur électrolytique humide selon la revendication 20, dans lequel un fil de sortie s'étend depuis l'anode plane qui a une configuration courbée.
- 22. Condensateur électrolytique humide selon la 5 revendication 20, dans lequel l'anode a la forme d'un D.
- 23. Condensateur électrolytique humide selon la revendication 1, dans lequel la poudre est formée à partir de particules de tantale.
- 24. Condensateur électrolytique humide selon la 10 revendication 23, dans lequel les particules de tantale sont des particules de flocon ayant un rapport de côté d'environ 2 à environ 100.
- 25. Condensateur électrolytique humide selon la revendication 1, dans lequel le substrat de métal 15 inclut du titane.
- 26. Condensateur électrolytique humide selon la revendication 1, dans lequel le polymère conducteur est un poly(thiophène) substitué.
- 27. Condensateur électrolytique humide selon la 20 revendication 24, dans lequel le poly(thiophène) substitué est le poly(3,4-éthylènedioxythiophène).
- 28. Dispositif médical implantable comprenant le condensateur électrolytique humide de la revendication 1. 25
- 29. Electrolyte de travail pour un condensateur électrolytique humide, l'électrolyte de travail comprenant d'environ 1 % en poids à environ 40 % en poids d'au moins un sel d'ammonium d'un acide organique, d'environ 0,01 % en poids à environ 10 % en poids d'au 30 moins un acide, d'environ 0,5 % en poids à environ 20 % en poids de particules d'oxyde inorganiques, d'environ30 % en poids à environ 70 % en poids d'eau, et d'environ 5 % en poids à environ 40 % en poids d'au moins un solvant secondaire, dans lequel l'électrolyte de travail se présente sous la forme d'un gel et a une valeur de pH d'environ 5,0 à environ 8,0 et a une conductivité d'environ 10 à environ 80 milliSiemens par centimètre, déterminée à une température de 25 °C.
- 30. Electrolyte de travail selon la revendication 29, dans lequel l'électrolyte affiche un angle de phase ô d'environ 0,2° à environ 2°.
- 31. Electrolyte de travail selon la revendication 29, dans lequel l'électrolyte affiche un module de conservation G' d'environ 5 kilopascals ou plus.
- 32. Electrolyte de travail selon la revendication 15 29, dans lequel l'acide organique du sel d'ammonium est l'acide adipique, l'acide a-tartrique, l'acide méso- tartrique, l'acide oxalique, l'acide lactique, ou une combinaison de ceux-ci.
- 33. Electrolyte de travail selon la revendication 20 29, dans lequel l'acide inclut l'acide éthylènediaminetétraacétique.
- 34. Electrolyte de travail selon la revendication 29, dans lequel le solvant secondaire est l'éthylène glycol. 25
- 35. Electrolyte de travail selon la revendication 29, dans lequel les particules d'oxyde inorganiques sont des particules de silice fumée.
- 36. Procédé de formation d'un condensateur électrolytique humide, le procédé comprenant : 30 la formation d'un mélange qui comprend un sel d'ammonium d'un acide organique, des particules d'oxydeinorganiques, un acide et un système de solvants qui comprend de l'eau ; l'induction d'une gélification du mélange de sorte qu'il affiche un premier angle de phase 6 d'environ 50° à 90° ; le placement du mélange gélifié en communication avec une anode, une cathode ou les deux, où l'anode comprend une pastille oxydée anodiquement formée à partir d'une poudre pressée et frittée et la cathode comprend un substrat de métal revêtu avec un polymère conducteur ; et après cela, le fait de laisser le mélange gélifier davantage pour former un électrolyte de travail qui affiche un second angle de phase 6 de 0° à environ 20°, où l'électrolyte de travail a en outre une valeur de pH d'environ 5,0 à environ 8,0.
- 37. Procédé selon la revendication 36, dans lequel la gélification est induite ultrasoniquement.
- 38. Procédé selon la revendication 36, dans lequel 20 l'anode est imprégnée avec le mélange gélifié.
- 39. Procédé selon la revendication 36, dans lequel le mélange gélifié affiche une viscosité d'environ 1 à environ 40 centipoises telle que déterminée à l'aide d'un viscosimètre Brookfield LVT (broche n° 3 à 25 60 tr/min) à une température de 25 °C.
- 40. Procédé selon la revendication 36, dans lequel le mélange gélifié affiche un angle de phase d'environ 80° à 90° et l'électrolyte de travail affiche un angle de phase S de 0,2° à environ 2°. 30
- 41. Procédé selon la revendication 36, dans lequel le mélange gélifié affiche un module de conservation G'd'environ 0,01 kPa ou moins et l'électrolyte de travail affiche un module de conservation G' d'environ 5 kPa ou plus.
- 42. Procédé selon la revendication 36, dans lequel on laisse l'électrolyte gélifier davantage pendant au moins 48 heures.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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US201161566160P | 2011-12-02 | 2011-12-02 |
Publications (2)
Publication Number | Publication Date |
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FR2983628A1 true FR2983628A1 (fr) | 2013-06-07 |
FR2983628B1 FR2983628B1 (fr) | 2024-02-16 |
Family
ID=47560819
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Application Number | Title | Priority Date | Filing Date |
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FR1203255A Active FR2983628B1 (fr) | 2011-12-02 | 2012-11-30 | Condensateur electrolytique humide contenant un electrolyte de travail gelifie |
Country Status (5)
Country | Link |
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US (1) | US9105401B2 (fr) |
CN (1) | CN103137330B (fr) |
DE (1) | DE102012221861A1 (fr) |
FR (1) | FR2983628B1 (fr) |
GB (1) | GB2497199B (fr) |
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- 2012-11-29 DE DE102012221861A patent/DE102012221861A1/de active Pending
- 2012-11-30 FR FR1203255A patent/FR2983628B1/fr active Active
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Also Published As
Publication number | Publication date |
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CN103137330B (zh) | 2017-08-29 |
US9105401B2 (en) | 2015-08-11 |
DE102012221861A1 (de) | 2013-06-06 |
CN103137330A (zh) | 2013-06-05 |
GB2497199B (en) | 2015-12-30 |
US20130141841A1 (en) | 2013-06-06 |
GB2497199A (en) | 2013-06-05 |
FR2983628B1 (fr) | 2024-02-16 |
GB201221405D0 (en) | 2013-01-09 |
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