FR2396793A1 - Procede de production d'un brai deformable optiquement anisotrope et produit obtenu - Google Patents
Procede de production d'un brai deformable optiquement anisotrope et produit obtenuInfo
- Publication number
- FR2396793A1 FR2396793A1 FR7820395A FR7820395A FR2396793A1 FR 2396793 A1 FR2396793 A1 FR 2396793A1 FR 7820395 A FR7820395 A FR 7820395A FR 7820395 A FR7820395 A FR 7820395A FR 2396793 A1 FR2396793 A1 FR 2396793A1
- Authority
- FR
- France
- Prior art keywords
- optically anisotropic
- producing
- brai
- product obtained
- deformable
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10C—WORKING-UP PITCH, ASPHALT, BITUMEN, TAR; PYROLIGNEOUS ACID
- C10C3/00—Working-up pitch, asphalt, bitumen
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
- D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
- D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
- D01F9/14—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
- D01F9/145—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from pitch or distillation residues
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Civil Engineering (AREA)
- Structural Engineering (AREA)
- Materials Engineering (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Textile Engineering (AREA)
- Working-Up Tar And Pitch (AREA)
- Inorganic Fibers (AREA)
Abstract
L'invention concerne un procédé de production d'un brai déformable optiquement anisotrope. Un extraction au solvant donne une fraction de brai carboné qui peut être transformé en une matière déformable renfermant plus de 90 % d'une phase optiquement anisotrope. Application à la production d'articles façonnés en carbone, tels qu'électrodes, filaments continus de carbone et de graphite, etc.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US81393177A | 1977-07-08 | 1977-07-08 | |
US05/903,172 US4208267A (en) | 1977-07-08 | 1978-05-05 | Forming optically anisotropic pitches |
Publications (2)
Publication Number | Publication Date |
---|---|
FR2396793A1 true FR2396793A1 (fr) | 1979-02-02 |
FR2396793B1 FR2396793B1 (fr) | 1983-08-19 |
Family
ID=27123795
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR7820395A Granted FR2396793A1 (fr) | 1977-07-08 | 1978-07-07 | Procede de production d'un brai deformable optiquement anisotrope et produit obtenu |
Country Status (5)
Country | Link |
---|---|
US (1) | US4208267A (fr) |
CA (1) | CA1113876A (fr) |
DE (2) | DE2858793C2 (fr) |
FR (1) | FR2396793A1 (fr) |
GB (1) | GB2002024B (fr) |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0016661A2 (fr) * | 1979-03-26 | 1980-10-01 | Exxon Research And Engineering Company | Préparation d'un précurseur d'un brai déformable optiquement anisotrope |
EP0038669A1 (fr) * | 1980-04-23 | 1981-10-28 | Exxon Research And Engineering Company | Procédé de préparation de poix propre à la fabrication des filaments de charbon |
EP0056338A1 (fr) * | 1981-01-14 | 1982-07-21 | E.I. Du Pont De Nemours And Company | Procédé de préparation de brai propre à la fabrication de corps carbonés |
FR2575487A1 (fr) * | 1984-12-28 | 1986-07-04 | Nippon Oil Co Ltd | Brai pour la production de fibres de carbone et procede de sa preparation |
EP0243509A1 (fr) * | 1984-10-29 | 1987-11-04 | Maruzen Petrochemical Co., Ltd. | Procédé de préparation d'un brai mésophase pour la production de fibres de carbone |
EP0246591A1 (fr) * | 1986-05-19 | 1987-11-25 | Director-General of Agency of Industrial Science and Technology | Procédé pour la préparation de brai à mésophase |
EP0548918A1 (fr) * | 1991-12-25 | 1993-06-30 | Mitsubishi Chemical Corporation | Fibres de carbone à base de brai et procédé pour leur production |
Families Citing this family (77)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4184942A (en) * | 1978-05-05 | 1980-01-22 | Exxon Research & Engineering Co. | Neomesophase formation |
US4283269A (en) * | 1979-04-13 | 1981-08-11 | Exxon Research & Engineering Co. | Process for the production of a feedstock for carbon artifact manufacture |
US4277324A (en) * | 1979-04-13 | 1981-07-07 | Exxon Research & Engineering Co. | Treatment of pitches in carbon artifact manufacture |
US4277325A (en) * | 1979-04-13 | 1981-07-07 | Exxon Research & Engineering Co. | Treatment of pitches in carbon artifact manufacture |
JPS5657881A (en) * | 1979-09-28 | 1981-05-20 | Union Carbide Corp | Manufacture of intermediate phase pitch and carbon fiber |
DE3024423C2 (de) * | 1980-06-28 | 1982-09-23 | Rütgerswerke AG, 6000 Frankfurt | Verwendung pikrierbarer Pechfraktionen zur Herstellung von anisotropem Kohlenstoff |
JPS5788016A (en) * | 1980-11-19 | 1982-06-01 | Toa Nenryo Kogyo Kk | Optically anisotropic carbonaceous pitch for carbon material, its manufacture, and manufacture of carbonaceous pitch fiber and carbon fiber |
US4402928A (en) * | 1981-03-27 | 1983-09-06 | Union Carbide Corporation | Carbon fiber production using high pressure treatment of a precursor material |
JPS5917044B2 (ja) * | 1981-06-01 | 1984-04-19 | 興亜石油株式会社 | 晶質化物質の製造方法および装置 |
US4414095A (en) * | 1981-06-12 | 1983-11-08 | Exxon Research And Engineering Co. | Mesophase pitch using steam cracker tar (CF-6) |
US4427531A (en) | 1981-08-11 | 1984-01-24 | Exxon Research And Engineering Co. | Process for deasphaltenating cat cracker bottoms and for production of anisotropic pitch |
US4464248A (en) * | 1981-08-11 | 1984-08-07 | Exxon Research & Engineering Co. | Process for production of carbon artifact feedstocks |
US4395299A (en) * | 1981-08-21 | 1983-07-26 | The United States Of America As Represented By The Secretary Of The Army | Bonded bulk graphite and process for bonding |
US4497789A (en) * | 1981-12-14 | 1985-02-05 | Ashland Oil, Inc. | Process for the manufacture of carbon fibers |
US4427530A (en) | 1982-02-08 | 1984-01-24 | Exxon Research And Engineering Co. | Aromatic pitch derived from a middle fraction of a cat cracker bottom |
US4448670A (en) * | 1982-02-08 | 1984-05-15 | Exxon Research And Engineering Co. | Aromatic pitch production from coal derived distillate |
US4431512A (en) * | 1982-02-08 | 1984-02-14 | Exxon Research And Engineering Co. | Aromatic pitch from asphaltene-free steam cracker tar fractions |
US4522701A (en) * | 1982-02-11 | 1985-06-11 | E. I. Du Pont De Nemours And Company | Process for preparing an anisotropic aromatic pitch |
US4597853A (en) * | 1982-02-23 | 1986-07-01 | Mitsubishi Oil Co., Ltd. | Pitch as a raw material for making carbon fibers and process for producing the same |
US4465586A (en) * | 1982-06-14 | 1984-08-14 | Exxon Research & Engineering Co. | Formation of optically anisotropic pitches |
JPS58220805A (ja) * | 1982-06-15 | 1983-12-22 | Nippon Oil Co Ltd | 炭素繊維用前駆体ピツチの製造方法 |
US4518482A (en) * | 1982-07-19 | 1985-05-21 | E. I. Du Pont De Nemours And Company | Pitch for direct spinning into carbon fibers derived from a coal distillate feedstock |
CA1207264A (fr) * | 1982-07-19 | 1986-07-08 | Ghazi Dickakian | Brai derive de la charge en produits de queue d'une unite de craquage catalytique, pouvant etre file directement en fibres de carbone |
US4548703A (en) * | 1982-07-19 | 1985-10-22 | E. I. Du Pont De Nemours And Company | Pitch for direct spinning into carbon fibers |
US4548704A (en) * | 1982-07-19 | 1985-10-22 | E. I. Du Pont De Nemours And Company | Pitch for direct spinning into carbon fibers derived from a steam cracker tar feedstock |
CA1199758A (fr) * | 1982-07-19 | 1986-01-28 | E. I. Du Pont De Nemours And Company | Brai derive de la charge de goudron de fractionnement a la vapeur, ledit brai etant destine a la filature en direct de fibres de carbone |
US4590055A (en) * | 1982-08-24 | 1986-05-20 | Director-General Of The Agency Of Industrial Science And Technology | Pitch-based carbon fibers and pitch compositions and precursor fibers therefor |
US4913889A (en) * | 1983-03-09 | 1990-04-03 | Kashima Oil Company | High strength high modulus carbon fibers |
US4502943A (en) * | 1983-03-28 | 1985-03-05 | E. I. Du Pont De Nemours And Company | Post-treatment of spinnable precursors from petroleum pitch |
JPS6034619A (ja) * | 1983-07-29 | 1985-02-22 | Toa Nenryo Kogyo Kk | 炭素繊維及び黒鉛繊維の製造方法 |
US4527754A (en) * | 1983-08-26 | 1985-07-09 | E. I. Du Pont De Nemours And Company | Non-thermal expanding spool for carbon fiber oxidation |
DE3335316A1 (de) * | 1983-09-29 | 1985-04-11 | Rütgerswerke AG, 6000 Frankfurt | Verfahren zur abtrennung harzartiger stoffe aus kohlestaemmigen schweroelen und verwendung der gewonnenen fraktion |
US4604184A (en) * | 1983-11-16 | 1986-08-05 | Domtar Inc. | Modified coal-tar pitch |
US4628001A (en) * | 1984-06-20 | 1986-12-09 | Teijin Limited | Pitch-based carbon or graphite fiber and process for preparation thereof |
US4929404A (en) * | 1984-09-25 | 1990-05-29 | Mitsubishi Petrochemical Company Limited | Graphitic or carbonaceous moldings and processes for producing the same |
DE3441727A1 (de) * | 1984-11-15 | 1986-05-15 | Bergwerksverband Gmbh, 4300 Essen | Verfahren zur herstellung von anisotropen kohlenstoffasern |
US5154908A (en) * | 1985-09-12 | 1992-10-13 | Clemson University | Carbon fibers and method for producing same |
US5149517A (en) * | 1986-01-21 | 1992-09-22 | Clemson University | High strength, melt spun carbon fibers and method for producing same |
US5156831A (en) * | 1986-01-21 | 1992-10-20 | Clemson University | Method for producing high strength, melt spun carbon fibers |
DE3603883A1 (de) * | 1986-02-07 | 1987-08-13 | Ruetgerswerke Ag | Verfahren zur herstellung von steinkohlenteerpech-rohstoffen mit verbesserten eigenschaften und deren verwendung |
DE3610375A1 (de) * | 1986-03-27 | 1987-10-01 | Ruetgerswerke Ag | Verfahren zur herstellung eines kohlenstoffaser-vorprodukts und daraus hergestellte kohlenstoffasern |
DE3636560A1 (de) * | 1986-10-28 | 1988-05-05 | Ruetgerswerke Ag | Verfahren zur entsalzung von steinkohlenteeren und -pechen |
CA1302934C (fr) * | 1987-06-18 | 1992-06-09 | Masatoshi Tsuchitani | Mode de preparation de brais mesophases |
JPH0791372B2 (ja) * | 1987-07-08 | 1995-10-04 | 呉羽化学工業株式会社 | 炭素材料用原料ピッチの製造方法 |
US4891126A (en) * | 1987-11-27 | 1990-01-02 | Mitsubishi Gas Chemical Company, Inc. | Mesophase pitch for use in the making of carbon materials and process for producing the same |
US4915926A (en) * | 1988-02-22 | 1990-04-10 | E. I. Dupont De Nemours And Company | Balanced ultra-high modulus and high tensile strength carbon fibers |
WO1990001523A1 (fr) * | 1988-08-12 | 1990-02-22 | Ube Industries, Ltd. | Fibres de carbure a resistance et module d'elasticite eleves et composition polymere utilisee dans leur fabrication |
US5032250A (en) * | 1988-12-22 | 1991-07-16 | Conoco Inc. | Process for isolating mesophase pitch |
US5238672A (en) * | 1989-06-20 | 1993-08-24 | Ashland Oil, Inc. | Mesophase pitches, carbon fiber precursors, and carbonized fibers |
US5182010A (en) * | 1989-11-29 | 1993-01-26 | Mitsubishi Gas Chemical Company, Inc. | Mesophase pitch for use in the making of carbon materials |
US5308598A (en) * | 1990-02-01 | 1994-05-03 | E. I. Du Pont De Nemours And Company | Plexifilamentary fibers from pitch |
CA2055092C (fr) * | 1990-12-14 | 2002-01-15 | Conoco Inc. | Brais mesomorphes contenant des composes organometalliques pour le filage de fibres de carbone dans le brai |
JPH0517782A (ja) * | 1991-07-09 | 1993-01-26 | Tonen Corp | 高圧縮強度炭素繊維製造用液晶ピツチ及び高圧縮強度炭素繊維の製造方法 |
WO1993024590A1 (fr) * | 1992-06-04 | 1993-12-09 | Conoco Inc. | Procede de production de brai mesophase solvate, et articles en carbone obtenus a partir de ce dernier |
US5382392A (en) * | 1993-02-05 | 1995-01-17 | Alliedsignal Inc. | Process for fabrication of carbon fiber-reinforced carbon composite material |
US5437780A (en) * | 1993-10-12 | 1995-08-01 | Conoco Inc. | Process for making solvated mesophase pitch |
DE19736575C5 (de) * | 1997-08-22 | 2007-07-19 | Xperion Gmbh | Kunstoffwalze, Verfahren zur Herstellung derselben und Vorrichtung zur Durchführung des Verfahrens |
US6596438B2 (en) | 2001-06-13 | 2003-07-22 | The Gillette Company | Alkaline cell with improved cathode |
US6833012B2 (en) * | 2001-10-12 | 2004-12-21 | Touchstone Research Laboratory, Ltd. | Petroleum pitch-based carbon foam |
US8337730B2 (en) * | 2009-01-05 | 2012-12-25 | The Boeing Company | Process of making a continuous, multicellular, hollow carbon fiber |
JP5934711B2 (ja) | 2010-10-15 | 2016-06-15 | エメカ ウゾー、キプリアン | 光電池及び光電池の製造方法 |
US9376626B1 (en) | 2011-04-28 | 2016-06-28 | Advanced Carbon Products, LLC | Turbulent mesophase pitch process and products |
US9683312B2 (en) | 2011-12-10 | 2017-06-20 | The Boeing Company | Fiber with gradient properties and method of making the same |
US9683310B2 (en) | 2011-12-10 | 2017-06-20 | The Boeing Company | Hollow fiber with gradient properties and method of making the same |
JP6301885B2 (ja) * | 2015-08-31 | 2018-03-28 | 日東電工株式会社 | 光学補償層付偏光板およびそれを用いた有機elパネル |
US10358767B2 (en) | 2016-07-15 | 2019-07-23 | GM Global Technology Operations LLC | Carbon fiber pre-pregs and methods for manufacturing thereof |
US10427349B2 (en) * | 2016-09-23 | 2019-10-01 | GM Global Technology Operations LLC | Components molded with moldable carbon fiber and methods of manufacturing thereof |
US10612163B2 (en) | 2017-08-24 | 2020-04-07 | GM Global Technology Operations LLC | Modification of continuous carbon fibers during precursor formation for composites having enhanced moldability |
US10941510B2 (en) | 2017-12-08 | 2021-03-09 | GM Global Technology Operations LLC | Equipment for perforated pre-impregnated reinforcement materials |
WO2019240949A1 (fr) | 2018-06-15 | 2019-12-19 | Exxonmobil Research And Engineering Company | Modification de la dépendance à la température de la viscosité du brai pour la fabrication d'articles en carbone |
CN109179371A (zh) * | 2018-10-24 | 2019-01-11 | 武汉科技大学 | 一种中间相炭微球及利用沥青热裂油制备中间相炭微球的方法 |
US11498318B2 (en) | 2019-12-05 | 2022-11-15 | GM Global Technology Operations LLC | Class-A components comprising moldable carbon fiber |
WO2021173735A1 (fr) * | 2020-02-24 | 2021-09-02 | Carbon Holdings Intellectual Properties, Llc | Systèmes et procédés de fabrication d'hydrocarbures à haut point de fusion à partir du charbon |
WO2022155029A1 (fr) | 2021-01-15 | 2022-07-21 | Exxonmobil Chemical Patents Inc. | Procédés de production de brai-mésophase |
KR20230162712A (ko) | 2021-04-08 | 2023-11-28 | 엑손모빌 케미칼 패턴츠 인코포레이티드 | 중질 탄화수소의 중간상 피치로의 열 변환 |
CN117280013A (zh) | 2021-04-28 | 2023-12-22 | 埃克森美孚化学专利公司 | 通过改变溶剂sbn经由溶剂脱沥青控制中间相软化点和产率 |
US11898101B2 (en) | 2021-08-26 | 2024-02-13 | Koppers Delaware, Inc. | Method and apparatus for continuous production of mesophase pitch |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2113351A5 (fr) * | 1970-10-28 | 1972-06-23 | Great Lakes Carbon Corp | |
FR2276366A1 (fr) * | 1974-06-24 | 1976-01-23 | Kureha Chemical Ind Co Ltd | Procede pour convertir du brai en une forme cristalloidale, et produit obtenu |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3919387A (en) * | 1972-12-26 | 1975-11-11 | Union Carbide Corp | Process for producing high mesophase content pitch fibers |
US3974264A (en) * | 1973-12-11 | 1976-08-10 | Union Carbide Corporation | Process for producing carbon fibers from mesophase pitch |
US4005187A (en) * | 1974-06-03 | 1977-01-25 | Data Diagnostic Corporation | Diagnostic test method |
-
1978
- 1978-05-05 US US05/903,172 patent/US4208267A/en not_active Expired - Lifetime
- 1978-07-04 DE DE2858793A patent/DE2858793C2/de not_active Expired - Lifetime
- 1978-07-04 DE DE19782829288 patent/DE2829288A1/de active Granted
- 1978-07-07 CA CA306,991A patent/CA1113876A/fr not_active Expired
- 1978-07-07 GB GB7829095A patent/GB2002024B/en not_active Expired
- 1978-07-07 FR FR7820395A patent/FR2396793A1/fr active Granted
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2113351A5 (fr) * | 1970-10-28 | 1972-06-23 | Great Lakes Carbon Corp | |
FR2276366A1 (fr) * | 1974-06-24 | 1976-01-23 | Kureha Chemical Ind Co Ltd | Procede pour convertir du brai en une forme cristalloidale, et produit obtenu |
Cited By (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0016661A2 (fr) * | 1979-03-26 | 1980-10-01 | Exxon Research And Engineering Company | Préparation d'un précurseur d'un brai déformable optiquement anisotrope |
EP0016661A3 (en) * | 1979-03-26 | 1980-11-12 | Exxon Research And Engineering Company | Preparation of an optically anisotropic deformable pitch precursor |
EP0038669A1 (fr) * | 1980-04-23 | 1981-10-28 | Exxon Research And Engineering Company | Procédé de préparation de poix propre à la fabrication des filaments de charbon |
EP0038669B1 (fr) * | 1980-04-23 | 1984-03-07 | Exxon Research And Engineering Company | Procédé de préparation de poix propre à la fabrication des filaments de charbon |
EP0056338A1 (fr) * | 1981-01-14 | 1982-07-21 | E.I. Du Pont De Nemours And Company | Procédé de préparation de brai propre à la fabrication de corps carbonés |
EP0243509A1 (fr) * | 1984-10-29 | 1987-11-04 | Maruzen Petrochemical Co., Ltd. | Procédé de préparation d'un brai mésophase pour la production de fibres de carbone |
US4705618A (en) * | 1984-10-29 | 1987-11-10 | Maruzen Petrochemical Co., Ltd. | Process for the preparation of an intermediate pitch for manufacturing carbon products |
FR2575487A1 (fr) * | 1984-12-28 | 1986-07-04 | Nippon Oil Co Ltd | Brai pour la production de fibres de carbone et procede de sa preparation |
EP0246591A1 (fr) * | 1986-05-19 | 1987-11-25 | Director-General of Agency of Industrial Science and Technology | Procédé pour la préparation de brai à mésophase |
EP0548918A1 (fr) * | 1991-12-25 | 1993-06-30 | Mitsubishi Chemical Corporation | Fibres de carbone à base de brai et procédé pour leur production |
US5601794A (en) * | 1991-12-25 | 1997-02-11 | Mitsubishi Chemical Corporation | Pitch type carbon fibers and process for their production |
Also Published As
Publication number | Publication date |
---|---|
DE2829288C2 (fr) | 1990-07-12 |
GB2002024B (en) | 1982-02-17 |
CA1113876A (fr) | 1981-12-08 |
FR2396793B1 (fr) | 1983-08-19 |
US4208267A (en) | 1980-06-17 |
DE2858793C2 (fr) | 1990-12-20 |
DE2829288A1 (de) | 1979-01-25 |
GB2002024A (en) | 1979-02-14 |
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Legal Events
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TP | Transmission of property |