ES2193953T3 - Procedimiento para elaborar poliol de pipa. - Google Patents

Procedimiento para elaborar poliol de pipa.

Info

Publication number
ES2193953T3
ES2193953T3 ES00925265T ES00925265T ES2193953T3 ES 2193953 T3 ES2193953 T3 ES 2193953T3 ES 00925265 T ES00925265 T ES 00925265T ES 00925265 T ES00925265 T ES 00925265T ES 2193953 T3 ES2193953 T3 ES 2193953T3
Authority
ES
Spain
Prior art keywords
polyol
temperature
particulate material
high shear
maintaining
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES00925265T
Other languages
English (en)
Inventor
Gabriel Albert Verhelst
Alphonse Elisabeth Bruyninckx
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Huntsman International LLC
Original Assignee
Huntsman International LLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Huntsman International LLC filed Critical Huntsman International LLC
Application granted granted Critical
Publication of ES2193953T3 publication Critical patent/ES2193953T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/409—Dispersions of polymers of C08G in organic compounds having active hydrogen
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/0838—Manufacture of polymers in the presence of non-reactive compounds
    • C08G18/0842—Manufacture of polymers in the presence of non-reactive compounds in the presence of liquid diluents
    • C08G18/0861—Manufacture of polymers in the presence of non-reactive compounds in the presence of liquid diluents in the presence of a dispersing phase for the polymers or a phase dispersed in the polymers
    • C08G18/0871—Manufacture of polymers in the presence of non-reactive compounds in the presence of liquid diluents in the presence of a dispersing phase for the polymers or a phase dispersed in the polymers the dispersing or dispersed phase being organic
    • C08G18/0876—Manufacture of polymers in the presence of non-reactive compounds in the presence of liquid diluents in the presence of a dispersing phase for the polymers or a phase dispersed in the polymers the dispersing or dispersed phase being organic the dispersing or dispersed phase being a polyol
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30—Low-molecular-weight compounds
    • C08G18/32—Polyhydroxy compounds; Polyamines; Hydroxyamines
    • C08G18/3271—Hydroxyamines
    • C08G18/3278—Hydroxyamines containing at least three hydroxy groups
    • C08G18/3281—Hydroxyamines containing at least three hydroxy groups containing three hydroxy groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Polyethers (AREA)

Abstract

Procedimiento para preparar un poliol que comprende material en partículas en forma dispersada, siendo la cantidad de material en partículas 30-80% en peso calculado sobre la composición total, en el que: - un compuesto reactivo con isocianato que comprende una pluralidad de grupos hidroxilo, amina primaria y/o amina secundaria y que tiene un peso equivalente de hasta 400 se emulsifica en un poliol, que tiene un peso equivalente de 1000-5000 y una funcionalidad de hidróxido nominal media de 2-6, a una temperatura de 60-100ºC bajo condiciones de mezcladura de alto cizallamiento, - se añade gradualmente un poliisocianato a la emulsión así formada mientras se mantiene la temperatura entre 60-120ºC y mientras se mantienen condiciones de alto cizallamiento, - la mezcla de reacción, obtenida después de que se haya añadido todo el poliisocianato, se deja reaccionar adicionalmente durante un período de tiempo de 10 minutos- 2 horas mientras se mantiene la temperatura entre 60- 120ºC, . - la mezcladura de alto cizallamiento se interrumpe y opcionalmente - el poliol así obtenido y que comprende el material en partículas en una cantidad de 30-80% en peso en forma dispersada se enfría hasta temperatura ambiente.
ES00925265T 1999-05-31 2000-05-05 Procedimiento para elaborar poliol de pipa. Expired - Lifetime ES2193953T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
EP99110479 1999-05-31

Publications (1)

Publication Number Publication Date
ES2193953T3 true ES2193953T3 (es) 2003-11-16

Family

ID=8238268

Family Applications (1)

Application Number Title Priority Date Filing Date
ES00925265T Expired - Lifetime ES2193953T3 (es) 1999-05-31 2000-05-05 Procedimiento para elaborar poliol de pipa.

Country Status (22)

Country Link
US (1) US6881783B1 (es)
EP (1) EP1189960B1 (es)
JP (1) JP4907812B2 (es)
KR (1) KR100608961B1 (es)
CN (1) CN1134477C (es)
AR (1) AR025167A1 (es)
AT (1) ATE234333T1 (es)
AU (1) AU763481B2 (es)
BR (1) BR0011064B1 (es)
CA (1) CA2374418C (es)
CZ (1) CZ296030B6 (es)
DE (1) DE60001658T2 (es)
ES (1) ES2193953T3 (es)
HK (1) HK1047120B (es)
MX (1) MXPA01012311A (es)
PL (1) PL204258B1 (es)
RU (1) RU2235734C2 (es)
SI (1) SI1189960T1 (es)
TR (1) TR200103424T2 (es)
TW (1) TWI252239B (es)
WO (1) WO2000073364A1 (es)
ZA (1) ZA200109611B (es)

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100624030B1 (ko) * 1999-06-19 2006-09-19 에이에스엠지니텍코리아 주식회사 화학 증착 반응기 및 이를 이용한 박막 형성 방법
KR20060009322A (ko) * 2003-05-12 2006-01-31 헌트스만 인터내셔날, 엘엘씨 Ｐｉｐａ-폴리올의 제조 방법
EP1809679B1 (en) * 2004-10-15 2010-01-13 Huntsman International Llc Process for making a pipa-polyol
DE102005050701A1 (de) * 2005-10-22 2007-05-03 Bayer Materialscience Ag Verfahren zur Herstellung von PIPA-Polyolen
CA2668072A1 (en) * 2006-10-30 2008-05-08 Johnson Controls Technology Company Non-petroleum-based polyurethane foam products having improved performance specifications and method of production
DE102006060376A1 (de) * 2006-12-20 2008-06-26 Bayer Materialscience Ag Verfahren zur Herstellung von PIPA-Polyolen zur Herstellung von hochelastischen Polyurethan-Weichschaumstoffen
DE102007004769A1 (de) * 2007-01-31 2008-08-07 Bayer Materialscience Ag Nanoharnstoff-Dispersionen
US9115246B2 (en) 2010-04-30 2015-08-25 Basf Se Polyether polyols, process for preparing polyether polyols and their use for producing polyurethanes
CN102958977A (zh) 2010-04-30 2013-03-06 巴斯夫欧洲公司 聚醚多元醇、制备聚醚多元醇的方法及其用于生产聚氨酯的用途
US8946313B2 (en) 2011-12-16 2015-02-03 Bayer Materialscience Llc Hybrid PHD/PMPO polyols for polyurethane foam applications
EP2831135B1 (en) * 2012-03-30 2020-04-29 Dow Global Technologies LLC Tin-free polymer polyols
CN105518048B (zh) 2013-09-13 2019-05-21 陶氏环球技术有限责任公司 基于pipa多元醇的粘弹性发泡体
US9840579B2 (en) * 2013-09-13 2017-12-12 Dow Global Technologies Llc Thixotropic polyol compositions containing dispersed urethane-modified polyisocyanurates
EP3044247B1 (en) * 2013-09-13 2020-06-24 Dow Global Technologies LLC Pipa based combustion-modified polyurethane foam
WO2018063959A1 (en) * 2016-09-29 2018-04-05 Dow Global Technologies Llc Reduced flammability flexible polyurethane foam
EP3545010B1 (en) 2016-11-28 2021-03-31 Univation Technologies, LLC Producing a polyethylene polymer
CN108752557B (zh) * 2018-06-11 2021-06-04 成都科大博创科技有限公司 一种聚氨酯改性多元醇及由其制得的聚氨酯泡沫塑料

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0072096B2 (en) 1981-08-11 1988-04-06 Imperial Chemical Industries Plc Polymer-modified polyols, a method of forming them, their use in the manufacture of polyurethane products and the products so obtained
DE3270603D1 (en) * 1981-10-28 1986-05-22 Ici Plc Polymer-modified polyols
EP0116758A1 (en) 1983-01-13 1984-08-29 Texaco Development Corporation Polyurethane polymer polyols made with aromatic nitrogen-containing polyols and polyurethanes therefrom
US4785026A (en) 1987-11-24 1988-11-15 Arco Chemical Company Polymer polyols with high solids content
US5068280A (en) * 1989-09-12 1991-11-26 The Dow Chemical Company Polyurethane and/or polyurea dispersions in active hydrogen-containing compositions
US5292778A (en) * 1992-11-20 1994-03-08 Woodbridge Foam Corporation Polymer-modified polyol dispersions and processes for production and use thereof
PL176376B1 (pl) * 1993-03-05 1999-05-31 Shell Int Research Sposób wytwarzania poliolu modyfikowanego polimerem
US5688861A (en) * 1995-11-30 1997-11-18 Arco Chemical Technology, L.P. Process for the preparation of polyol polymer dispersions
CZ351996A3 (en) 1995-12-07 1997-06-11 Shell Int Research Polyol formulation for preparing flexible polyurethane foam similar to latex
JP4023831B2 (ja) * 1997-03-25 2007-12-19 ハンツマン・インターナショナル・エルエルシー 軟質ポリウレタン発泡体を製造するための方法

Also Published As

Publication number Publication date
BR0011064B1 (pt) 2010-02-09
HK1047120A1 (en) 2003-02-07
JP4907812B2 (ja) 2012-04-04
AU4404300A (en) 2000-12-18
DE60001658T2 (de) 2003-09-25
BR0011064A (pt) 2002-03-19
JP2003501502A (ja) 2003-01-14
TR200103424T2 (tr) 2002-04-22
CA2374418A1 (en) 2000-12-07
SI1189960T1 (en) 2003-08-31
CA2374418C (en) 2009-04-21
CZ296030B6 (cs) 2005-12-14
DE60001658D1 (de) 2003-04-17
KR20020030746A (ko) 2002-04-25
CN1353728A (zh) 2002-06-12
MXPA01012311A (es) 2002-07-30
EP1189960B1 (en) 2003-03-12
RU2235734C2 (ru) 2004-09-10
ATE234333T1 (de) 2003-03-15
CN1134477C (zh) 2004-01-14
US6881783B1 (en) 2005-04-19
WO2000073364A1 (en) 2000-12-07
TWI252239B (en) 2006-04-01
AR025167A1 (es) 2002-11-13
AU763481B2 (en) 2003-07-24
PL204258B1 (pl) 2009-12-31
EP1189960A1 (en) 2002-03-27
HK1047120B (zh) 2004-12-03
ZA200109611B (en) 2003-04-30
CZ20014195A3 (cs) 2002-02-13
KR100608961B1 (ko) 2006-08-09
PL352291A1 (en) 2003-08-11

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