EP0413796A1 - Procede en plusieurs etapes d'extraction du sucre de la betterave sucriere et sucre brut special ainsi obtenu. - Google Patents
Procede en plusieurs etapes d'extraction du sucre de la betterave sucriere et sucre brut special ainsi obtenu.Info
- Publication number
- EP0413796A1 EP0413796A1 EP90904176A EP90904176A EP0413796A1 EP 0413796 A1 EP0413796 A1 EP 0413796A1 EP 90904176 A EP90904176 A EP 90904176A EP 90904176 A EP90904176 A EP 90904176A EP 0413796 A1 EP0413796 A1 EP 0413796A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- sugar
- juice
- production
- special raw
- beet
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 title claims abstract description 26
- 241000219310 Beta vulgaris subsp. vulgaris Species 0.000 title claims abstract description 14
- 235000021536 Sugar beet Nutrition 0.000 title claims abstract description 14
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 57
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims abstract description 28
- 238000004519 manufacturing process Methods 0.000 claims abstract description 24
- 235000013379 molasses Nutrition 0.000 claims abstract description 11
- 229930006000 Sucrose Natural products 0.000 claims description 26
- 235000016068 Berberis vulgaris Nutrition 0.000 claims description 15
- 241000335053 Beta vulgaris Species 0.000 claims description 15
- 238000000605 extraction Methods 0.000 claims description 12
- 206010033546 Pallor Diseases 0.000 claims description 8
- 239000004615 ingredient Substances 0.000 claims description 7
- 238000003825 pressing Methods 0.000 claims description 6
- 239000005720 sucrose Substances 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 5
- 239000000463 material Substances 0.000 claims description 4
- 150000001413 amino acids Chemical class 0.000 claims description 3
- 235000019156 vitamin B Nutrition 0.000 claims description 3
- 239000011720 vitamin B Substances 0.000 claims description 3
- 229960004903 invert sugar Drugs 0.000 claims description 2
- 239000006227 byproduct Substances 0.000 claims 1
- 239000000047 product Substances 0.000 claims 1
- 239000000126 substance Substances 0.000 abstract description 14
- 230000005923 long-lasting effect Effects 0.000 abstract 1
- 235000020357 syrup Nutrition 0.000 description 8
- 239000006188 syrup Substances 0.000 description 8
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 6
- 238000004140 cleaning Methods 0.000 description 6
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 5
- 235000011941 Tilia x europaea Nutrition 0.000 description 5
- 239000004571 lime Substances 0.000 description 5
- 238000002425 crystallisation Methods 0.000 description 4
- 230000008025 crystallization Effects 0.000 description 4
- 230000008719 thickening Effects 0.000 description 4
- 238000001035 drying Methods 0.000 description 3
- 235000010987 pectin Nutrition 0.000 description 3
- 229920001277 pectin Polymers 0.000 description 3
- 239000001814 pectin Substances 0.000 description 3
- 229930091371 Fructose Natural products 0.000 description 2
- 239000005715 Fructose Substances 0.000 description 2
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 2
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 2
- 102000003425 Tyrosinase Human genes 0.000 description 2
- 108060008724 Tyrosinase Proteins 0.000 description 2
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 2
- 239000008103 glucose Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 229930182490 saponin Natural products 0.000 description 2
- 150000007949 saponins Chemical class 0.000 description 2
- 235000017709 saponins Nutrition 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- CZMRCDWAGMRECN-UHFFFAOYSA-N Rohrzucker Natural products OCC1OC(CO)(OC2OC(CO)C(O)C(O)C2O)C(O)C1O CZMRCDWAGMRECN-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 238000003776 cleavage reaction Methods 0.000 description 1
- 235000008504 concentrate Nutrition 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000004108 freeze drying Methods 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000007017 scission Effects 0.000 description 1
- 239000010802 sludge Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000010025 steaming Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 150000003445 sucroses Chemical class 0.000 description 1
- 238000001291 vacuum drying Methods 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B50/00—Sugar products, e.g. powdered, lump or liquid sugar; Working-up of sugar
- C13B50/002—Addition of chemicals or other foodstuffs
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B10/00—Production of sugar juices
Definitions
- the present invention relates to a multi-stage process for the extraction of sugar from sugar beets.
- White sugar is freed of non-sugar substances by juice cleaning using a lime-carbonic acid process and subsequent crystallization and has a good shelf life with a wide range of uses; it is precisely this purity that nutritional physiologists accuse the product of.
- Hibe syrup which is made by heating sugar beet and thickening juice, is valued by some consumers for its non-sugar content.
- maintaining high temperatures over a long period of time causes a targeted splitting of sucrose into glucose and fructose.
- the syrup does not tend to crystallize, but it also cannot be converted into a more manageable dryer product.
- German patent 806825 describes a process for producing beet herb (beet syrup) with a high pectin content and high juice yield.
- Beet herb should be crystal-free, as it is known to be used as a spread.
- acid is formed by thermal cleavage of pectin and half of this sucrose is broken down into glucose and fructose.
- This goal can be achieved in various ways by varying process parameters such as steaming times, steam temperatures and number of process stages.
- a two-stage process is carried out in which the necessary pectin digestion is switched on before the second pressing stage, i.e. is brought about in a targeted manner.
- the new special raw sugar should be powdery and easy to handle and contain the essential beet ingredients.
- This aim is achieved by the process according to the invention in that a first juice is obtained from the sugar beets for the production of white sugar, then a second juice for the production of the new special raw sugar and finally a third juice for the production of white sugar.
- the first process step is necessary because sugar beets contain undesirable bitter substances, odorous substances and enzymes that would impair the taste of special raw sugar. These substances are not disruptive in the production of white sugar, as they are eliminated with lime and carbon dioxide as part of juice cleaning.
- FIG.1 Sugar beets or parts thereof, hereinafter referred to as beets for short, obtained by peeling, peeling or deliberate cutting are washed and then preferably shredded.
- the chips are then introduced into a preferably continuously operating blanching device and quickly heated to temperatures of about 70-90 ° C. by direct heating with steam. This creates a condensate in which beet ingredients dissolve into a first juice (juice 1 or brewed juice).
- the substances contained in this portion which are undesirable in the special raw sugar, such as saponins, phenol oxidases and odorous substances, are added to the classic white sugar production and destroyed or excreted in the course of juice cleaning with lime and carbonic acid.
- the blanching time is calculated in such a way that the schnitzel material emerging from the BlancMei ⁇ no longer turns dark. From a blanching time of around 40 seconds, discoloration after heating is prevented. With such short heating times it is also achieved that sucrose and other valuable ingredients (e.g. vitamins) are achieved to a high degree and an inversion is held up, which means that the prerequisites for the production of a high-quality dry product are met.
- sucrose and other valuable ingredients e.g. vitamins
- a third juice (juice 3) is finally obtained from the residue from the second juice extraction.
- a pressing process after adding water or a conventional extraction process can be used.
- the residual sugar content should be reduced to almost zero.
- Juices 1 and 3 are combined and subjected to classic juice cleaning with lime and carbonic acid. Then the mixed juice of juice 1 + juice 3 is thickened and white sugar is obtained by crystallization.
- the juice 2 obtained for the production of special raw sugar can be thickened without additives, since the foam-forming saponins contained in the beet are essentially contained in the juice 1.
- the tendency to form deposits on the juice 2 is also very reduced.
- This juice is thickened, preferably using a multi-stage process, to a concentrate of 67-70% dry matter.
- the separated ingredients are separated off. This is preferably done by separation at 35-45% dry matter.
- the syrup obtained can be temporarily stored in tanks in compliance with the relevant thick juice storage regulations.
- the syrup drawn off for the production of special raw sugar is processed into a dryer product with the aid of a suitable drying process, such as vacuum drying, sprürite drying or freeze drying.
- a suitable drying process such as vacuum drying, sprürite drying or freeze drying.
- the product obtained by drying has, for example, the following typical analysis result (data per 100 g of product):
- Non-sugar 8.9 g Inverted sugar 1.4 g
- the new special raw sugar according to the invention is as natural as possible, the varying raw material composition is included in the composition of the ingredients of the product. Areas of characteristic ingredients typical for the new special raw sugar can therefore be specified as follows (data per 100 g product):
- the pressed material obtained in this example in the production of special raw sugar is extracted with the aid of the extraction methods belonging to the state of the art, while maintaining an extraction loss of 0.25 t of sugar.
- the mixed juice obtained for the white sugar production (juice 1 + 3) contains 10.25 t dry substance and 9.35 t sugar.
- a quantity of 8.3 t of white sugar and 2.1 t is made from it in the presence of a molasses unit of 62.5% and a molasses dry substance of 80% Molasses with 50% sugar content.
- the extracted, pressed chips are dried in the usual way either as such or together with a molasses portion.
- the juice for the production of special raw sugar is obtained by pressing, but a larger amount of white sugar and a smaller amount of special raw sugar are produced.
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Medicines Containing Plant Substances (AREA)
- Preparation Of Fruits And Vegetables (AREA)
- Seasonings (AREA)
- Saccharide Compounds (AREA)
- Jellies, Jams, And Syrups (AREA)
- Non-Alcoholic Beverages (AREA)
Abstract
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
AT0055789A AT401776B (de) | 1989-03-10 | 1989-03-10 | Mehrstufiges verfahren zur zuckergewinnung aus zuckerrüben |
AT557/89 | 1989-03-10 | ||
PCT/AT1990/000020 WO1990010719A2 (fr) | 1989-03-10 | 1990-03-09 | Procede en plusieurs etapes d'extraction du sucre de la betterave sucriere et sucre brut special ainsi obtenu |
Publications (2)
Publication Number | Publication Date |
---|---|
EP0413796A1 true EP0413796A1 (fr) | 1991-02-27 |
EP0413796B1 EP0413796B1 (fr) | 1994-11-09 |
Family
ID=3493764
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP90904176A Expired - Lifetime EP0413796B1 (fr) | 1989-03-10 | 1990-03-09 | Procede en plusieurs etapes d'extraction du sucre de la betterave sucriere et sucre brut special ainsi obtenu |
Country Status (12)
Country | Link |
---|---|
EP (1) | EP0413796B1 (fr) |
JP (1) | JPH03505162A (fr) |
AT (2) | AT401776B (fr) |
BG (1) | BG60592B1 (fr) |
CA (1) | CA2028854A1 (fr) |
DE (1) | DE59007682D1 (fr) |
DK (1) | DK0413796T3 (fr) |
ES (1) | ES2064722T3 (fr) |
FI (1) | FI95813C (fr) |
HU (1) | HU210512B (fr) |
RO (1) | RO112119B1 (fr) |
WO (1) | WO1990010719A2 (fr) |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE19736080A1 (de) * | 1997-08-20 | 1999-02-25 | Heinz Dipl Ing Heyer | Verfahren und Anlage zur Gewinnung von Saft aus Zuckerrüben |
DE19817897A1 (de) * | 1998-04-22 | 1999-10-28 | Grafschafter Krautfabrik Josef | Verfahren zum Herstellen von Rübenkraut und Vorrichtung hierfür |
FR2788785B1 (fr) * | 1999-01-21 | 2001-04-06 | Maguin | Procede et unite d'extraction d'un jus sucre a partir de betteraves ou chicoree |
FR2795428B1 (fr) * | 1999-06-25 | 2001-08-31 | Maguin | Procede et installation d'extraction d'un jus sucre |
FR2928817B1 (fr) * | 2008-03-19 | 2010-12-17 | Ecopsi | Procede et unite de production de dreches de betteraves et de jus sucre a partir de betteraves |
CN102766702B (zh) * | 2012-07-24 | 2014-04-02 | 广西大学 | 一种高速沉降装置 |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR331717A (fr) * | 1903-05-04 | 1903-09-28 | Joseph Dziengielowski | Procédé pour préparer les betteraves de facon à obtenir par un procédé quelconque un jus d'un haut degré de pureté |
FR640523A (fr) * | 1927-02-17 | 1928-07-16 | Procédé de fabrication de sirop de betteraves | |
DE806192C (de) * | 1948-10-02 | 1951-06-11 | Joergen Meyer Dr Ing | Verfahren zur Saftgewinnung fuer die Herstellung von Ruebensirup |
DE806825C (de) * | 1949-07-22 | 1951-06-18 | Grafschafter Krautfabrik Josef | Verfahren zur Gewinnung von Ruebensaeften |
US2754233A (en) * | 1955-06-02 | 1956-07-10 | Harry S Owens | Inactivation of enzymes in beet cossettes prior to diffusion |
DE3150314C2 (de) * | 1981-12-18 | 1986-03-27 | Fried. Krupp Gmbh, 4300 Essen | Verfahren zur Gewinnung einer Saccharose-Lösung aus Zuckerrüben und anderen saccharosehaltigen Pflanzen |
DE3407364A1 (de) * | 1984-02-29 | 1985-08-29 | Pfeifer & Langen, 5000 Köln | Naturbelassener vollrohrzucker und verfahren zu seiner herstellung |
-
1989
- 1989-03-10 AT AT0055789A patent/AT401776B/de not_active IP Right Cessation
-
1990
- 1990-03-09 JP JP2504488A patent/JPH03505162A/ja active Pending
- 1990-03-09 EP EP90904176A patent/EP0413796B1/fr not_active Expired - Lifetime
- 1990-03-09 WO PCT/AT1990/000020 patent/WO1990010719A2/fr active IP Right Grant
- 1990-03-09 DK DK90904176.6T patent/DK0413796T3/da not_active Application Discontinuation
- 1990-03-09 ES ES90904176T patent/ES2064722T3/es not_active Expired - Lifetime
- 1990-03-09 AT AT90904176T patent/ATE113995T1/de not_active IP Right Cessation
- 1990-03-09 CA CA002028854A patent/CA2028854A1/fr not_active Abandoned
- 1990-03-09 HU HU902390A patent/HU210512B/hu not_active IP Right Cessation
- 1990-03-09 RO RO146289A patent/RO112119B1/ro unknown
- 1990-03-09 DE DE59007682T patent/DE59007682D1/de not_active Expired - Fee Related
- 1990-11-09 FI FI905557A patent/FI95813C/fi not_active IP Right Cessation
- 1990-12-10 BG BG93427A patent/BG60592B1/bg unknown
Non-Patent Citations (1)
Title |
---|
See references of WO9010719A3 * |
Also Published As
Publication number | Publication date |
---|---|
DK0413796T3 (da) | 1995-02-27 |
HUT57834A (en) | 1991-12-30 |
BG60592B1 (en) | 1995-09-29 |
WO1990010719A3 (fr) | 1990-11-01 |
DE59007682D1 (de) | 1994-12-15 |
ATE113995T1 (de) | 1994-11-15 |
FI95813C (fi) | 1996-03-25 |
BG93427A (bg) | 1993-12-24 |
CA2028854A1 (fr) | 1990-09-11 |
FI95813B (fi) | 1995-12-15 |
FI905557A0 (fi) | 1990-11-09 |
AT401776B (de) | 1996-11-25 |
ATA55789A (de) | 1996-04-15 |
WO1990010719A2 (fr) | 1990-09-20 |
EP0413796B1 (fr) | 1994-11-09 |
HU210512B (en) | 1995-04-28 |
RO112119B1 (ro) | 1997-05-30 |
ES2064722T3 (es) | 1995-02-01 |
JPH03505162A (ja) | 1991-11-14 |
HU902390D0 (en) | 1991-03-28 |
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