DK0668269T3 - Fremgangsmåde til sulfinylering af heterocykliske forbindelser - Google Patents
Fremgangsmåde til sulfinylering af heterocykliske forbindelserInfo
- Publication number
- DK0668269T3 DK0668269T3 DK95102219T DK95102219T DK0668269T3 DK 0668269 T3 DK0668269 T3 DK 0668269T3 DK 95102219 T DK95102219 T DK 95102219T DK 95102219 T DK95102219 T DK 95102219T DK 0668269 T3 DK0668269 T3 DK 0668269T3
- Authority
- DK
- Denmark
- Prior art keywords
- het
- halo
- substd
- opt
- alkyl
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D231/18—One oxygen or sulfur atom
- C07D231/20—One oxygen atom attached in position 3 or 5
- C07D231/22—One oxygen atom attached in position 3 or 5 with aryl radicals attached to ring nitrogen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D233/00—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings
- C07D233/54—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members
- C07D233/66—Heterocyclic compounds containing 1,3-diazole or hydrogenated 1,3-diazole rings, not condensed with other rings having two double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D233/88—Nitrogen atoms, e.g. allantoin
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D231/38—Nitrogen atoms
- C07D231/40—Acylated on said nitrogen atom
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D231/44—Oxygen and nitrogen or sulfur and nitrogen atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Plural Heterocyclic Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Pyrrole Compounds (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Coloring (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
- Cephalosporin Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR9402222A FR2716453B1 (fr) | 1994-02-22 | 1994-02-22 | Procédé de sulfinylation de composés hétérocycliques. |
Publications (1)
Publication Number | Publication Date |
---|---|
DK0668269T3 true DK0668269T3 (da) | 2002-06-17 |
Family
ID=9460460
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DK95102219T DK0668269T3 (da) | 1994-02-22 | 1995-02-17 | Fremgangsmåde til sulfinylering af heterocykliske forbindelser |
Country Status (24)
Country | Link |
---|---|
US (1) | US5618945A (ja) |
EP (1) | EP0668269B1 (ja) |
JP (3) | JP3963965B2 (ja) |
KR (1) | KR100370990B1 (ja) |
CN (1) | CN1056833C (ja) |
AT (1) | ATE218127T1 (ja) |
AU (1) | AU678876B2 (ja) |
BR (1) | BR9500858A (ja) |
CA (1) | CA2143135C (ja) |
CZ (1) | CZ294640B6 (ja) |
DE (1) | DE69526815T2 (ja) |
DK (1) | DK0668269T3 (ja) |
ES (1) | ES2173932T3 (ja) |
FI (1) | FI113764B (ja) |
FR (1) | FR2716453B1 (ja) |
HU (1) | HU214283B (ja) |
IL (1) | IL112708A (ja) |
PL (1) | PL183151B1 (ja) |
PT (1) | PT668269E (ja) |
RO (1) | RO113639B1 (ja) |
RU (1) | RU2136665C1 (ja) |
SK (1) | SK282510B6 (ja) |
UA (1) | UA44226C2 (ja) |
ZA (1) | ZA951468B (ja) |
Families Citing this family (31)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
PT976737E (pt) * | 1997-04-07 | 2009-07-31 | Nihon Nohyaku Co Ltd | Derivados de pirazole, processo para a sua preparação, produtos intermédios e agente de controlo de pragas que contém como ingrediente activo um desses derivados |
FR2784101B1 (fr) * | 1998-09-14 | 2000-11-17 | Rhodia Chimie Sa | Procede de condensation de derive(s) aromatique(s) et d'un derive sulfinique dont la chaine carbonee est attachee a la fonction sulfinique par un atome de carbone perhalogene |
GB9907458D0 (en) * | 1999-03-31 | 1999-05-26 | Rhone Poulenc Agrochimie | Processes for preparing pesticidal intermediates |
CA2377236C (en) | 1999-06-29 | 2010-08-17 | Mitsubishi Chemical Corporation | Pyrazole derivative, production process thereof, and pest control agent containing the same as active ingredient |
ES2222743T3 (es) * | 1999-10-22 | 2005-02-01 | Bayer Cropscience S.A. | Procedimiento para preparar un derivado 4-trifluorometilsulfinilpirazol. |
EP1331222A1 (en) * | 2002-01-28 | 2003-07-30 | Virbac S.A. | Environment friendly reagents and process for halogenoalkylsulfinylation of organic compounds |
US20060182808A1 (en) * | 2003-04-29 | 2006-08-17 | Akzo Nobel N.V. | Antisolvent solidification process |
AU2005223483B2 (en) * | 2004-03-18 | 2009-04-23 | Zoetis Llc | N-(1-arylpyrazol-4l)sulfonamides and their use as parasiticides |
CA2630849C (en) | 2005-12-14 | 2013-05-14 | Makhteshim Chemical Works Ltd. | Polymorphs and amorphous forms of 5-amino-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-4-[(trifluoromethyl)sulfinyl]-1h-pyrazole-3-carbonitrile |
CN101168529B (zh) * | 2006-10-24 | 2011-03-23 | 温州大学 | 氟虫腈、乙虫腈及其衍生物的合成方法 |
CN101562980B (zh) | 2006-11-10 | 2014-04-16 | 巴斯夫欧洲公司 | 锐劲特的晶型 |
EP2083628A1 (en) | 2006-11-10 | 2009-08-05 | Basf Se | Crystalline modification of fipronil |
NZ576593A (en) * | 2006-11-10 | 2011-12-22 | Basf Se | Process for the sulfinylation of a pyrazole derivative |
UA110598C2 (uk) | 2006-11-10 | 2016-01-25 | Басф Се | Спосіб одержання кристалічної модифікації фіпронілу |
BRPI0718758A2 (pt) * | 2006-11-10 | 2013-12-03 | Basf Se | " processo para a sulfinilação de um derivado de pirazol, composto, composição pesticida ou parasiticida, uso de um composto, métodos para o controle de insetos, acarídeos ou nematódeos, para proteger plantas em crescimento, e para tratar, controlar, prevenir ou proteger animais, e, processo para a preparação de uma composição." |
AU2007316639B2 (en) | 2006-11-10 | 2012-12-20 | Basf Se | Crystalline modification of fipronil |
ES2422296T3 (es) * | 2006-11-10 | 2013-09-10 | Basf Se | Proceso para la sulfinilación de un derivado pirazol |
US7378547B1 (en) | 2006-11-28 | 2008-05-27 | E.I. Du Pont De Nemours And Company | Process for the synthesis of hydroxy aromatic acids |
FR2925493B1 (fr) * | 2007-12-19 | 2011-09-30 | Vetoquinol | Procede de preparation du fipronil et d'analogues de celui-ci. |
AU2009299905B2 (en) * | 2008-10-02 | 2013-10-10 | Boehringer Ingelheim Animal Health USA Inc. | Method for producing and purifying trifluoromethanesulfinic acid |
US9198421B2 (en) | 2011-01-14 | 2015-12-01 | Keki Hormusji Gharda | Polymorphism in 5-amino-1-(2,6-dichloro-4-trifluoromethylphenyl)-3-cyano-4-trifluoro methyl sulfinyl pyrazole |
CN102093295A (zh) * | 2011-03-10 | 2011-06-15 | 江苏长青农化股份有限公司 | 一种农药杀虫剂氟虫腈的合成方法 |
TWI579274B (zh) | 2012-04-20 | 2017-04-21 | 龍馬躍公司 | 製備1-芳基-5-烷基吡唑化合物的改良方法 |
US8993613B2 (en) | 2013-04-17 | 2015-03-31 | The Hartz Mountain Corporation | Ectoparasiticidal formulations |
CN104557713B (zh) * | 2013-10-22 | 2018-08-21 | 江苏托球农化股份有限公司 | 高纯度氟虫腈制备方法 |
EP3412659A1 (en) * | 2017-06-09 | 2018-12-12 | Solvay Sa | Processes for the manufacture of sulfur-substituted pyrazole derivatives |
CN107963993A (zh) * | 2018-01-06 | 2018-04-27 | 江苏托球农化股份有限公司 | 一种高纯度氟虫腈的制备方法 |
AU2020243450A1 (en) * | 2019-03-19 | 2021-11-04 | Gharda Chemicals Limited | A process for synthesis of Fipronil |
CN113149873A (zh) * | 2021-03-10 | 2021-07-23 | 浙江埃森化学有限公司 | 一种三氟甲基亚磺酰氯的制备方法 |
CN115650919A (zh) * | 2022-04-13 | 2023-01-31 | 华东理工大学 | 一种自三氯甲基亚磺酰氯制备氟虫腈的方法 |
CN115353490A (zh) * | 2022-09-26 | 2022-11-18 | 安徽美诺华药物化学有限公司 | 一种氟虫腈的纯化工艺 |
Family Cites Families (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5187185A (en) * | 1988-12-09 | 1993-02-16 | Rhone-Poulenc Ag Company | Pesticidal 1-arylpyrroles |
JPS55157570A (en) * | 1979-05-26 | 1980-12-08 | Nissan Chem Ind Ltd | Sulfamylimidazole derivative, and agricultural and horticultural fungicide |
US5232940A (en) * | 1985-12-20 | 1993-08-03 | Hatton Leslie R | Derivatives of N-phenylpyrazoles |
GB8713768D0 (en) * | 1987-06-12 | 1987-07-15 | May & Baker Ltd | Compositions of matter |
DE3820190A1 (de) * | 1988-06-14 | 1989-12-21 | Cassella Ag | Pyrrolderivate, ihre herstellung und ihre verwendung als pharmazeutische wirkstoffe |
CA2004776C (fr) * | 1988-12-13 | 2000-04-25 | Claude Wakselman | Procede de preparation de perfluoroalkylthioethers |
US5223525A (en) * | 1989-05-05 | 1993-06-29 | Rhone-Poulenc Ag Company | Pesticidal 1-arylimidazoles |
GB9120641D0 (en) * | 1991-09-27 | 1991-11-06 | Ici Plc | Heterocyclic compounds |
-
1994
- 1994-02-22 FR FR9402222A patent/FR2716453B1/fr not_active Expired - Lifetime
-
1995
- 1995-02-16 UA UA95028159A patent/UA44226C2/uk unknown
- 1995-02-17 DK DK95102219T patent/DK0668269T3/da active
- 1995-02-17 EP EP95102219A patent/EP0668269B1/fr not_active Expired - Lifetime
- 1995-02-17 PT PT95102219T patent/PT668269E/pt unknown
- 1995-02-17 ES ES95102219T patent/ES2173932T3/es not_active Expired - Lifetime
- 1995-02-17 AT AT95102219T patent/ATE218127T1/de active
- 1995-02-17 DE DE69526815T patent/DE69526815T2/de not_active Expired - Lifetime
- 1995-02-20 IL IL11270895A patent/IL112708A/xx not_active IP Right Cessation
- 1995-02-20 SK SK234-95A patent/SK282510B6/sk not_active IP Right Cessation
- 1995-02-21 RU RU95102481A patent/RU2136665C1/ru active
- 1995-02-21 PL PL95307393A patent/PL183151B1/pl unknown
- 1995-02-21 CZ CZ1995461A patent/CZ294640B6/cs not_active IP Right Cessation
- 1995-02-21 HU HU9500522A patent/HU214283B/hu unknown
- 1995-02-21 BR BR9500858A patent/BR9500858A/pt active IP Right Grant
- 1995-02-21 FI FI950800A patent/FI113764B/fi not_active IP Right Cessation
- 1995-02-22 ZA ZA951468A patent/ZA951468B/xx unknown
- 1995-02-22 CN CN95100789A patent/CN1056833C/zh not_active Expired - Lifetime
- 1995-02-22 CA CA002143135A patent/CA2143135C/fr not_active Expired - Lifetime
- 1995-02-22 KR KR1019950003467A patent/KR100370990B1/ko not_active IP Right Cessation
- 1995-02-22 US US08/392,243 patent/US5618945A/en not_active Expired - Lifetime
- 1995-02-22 JP JP03385695A patent/JP3963965B2/ja not_active Expired - Lifetime
- 1995-02-22 AU AU12383/95A patent/AU678876B2/en not_active Expired
- 1995-02-22 RO RO95-00361A patent/RO113639B1/ro unknown
-
2005
- 2005-01-26 JP JP2005017759A patent/JP4447478B2/ja not_active Expired - Lifetime
-
2007
- 2007-02-07 JP JP2007027926A patent/JP4731503B2/ja not_active Expired - Lifetime
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