DE762522A - - Google Patents

Info

Publication number

DE762522A

DE762522A DE762522A DE 762522 A DE762522 A DE 762522A DE 762522 A DE762522 A DE 762522A

Authority

DE

Germany

Prior art keywords

diazo

compounds

light

aminodiazo

acid

Prior art date

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Pending

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• 150000001875 compounds Chemical class 0.000 claims description 7
• 125000000664 diazo group Chemical group [N-]=[N+]=[*] 0.000 claims description 4
• 125000001424 substituent group Chemical group 0.000 claims description 4
• 238000000034 method Methods 0.000 claims description 2
• 150000008049 diazo compounds Chemical class 0.000 description 8
• 235000002639 sodium chloride Nutrition 0.000 description 7
• 150000003839 salts Chemical class 0.000 description 6
• JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 description 6
• ROSDSFDQCJNGOL-UHFFFAOYSA-N Dimethylamine Chemical compound CNC ROSDSFDQCJNGOL-UHFFFAOYSA-N 0.000 description 4
• 239000002253 acid Substances 0.000 description 3
• 238000004519 manufacturing process Methods 0.000 description 3
• 230000011514 reflex Effects 0.000 description 3
• 239000000243 solution Substances 0.000 description 3
• 235000005074 zinc chloride Nutrition 0.000 description 3
• 239000011592 zinc chloride Substances 0.000 description 3
• JLDKNVUJLUGIBQ-UHFFFAOYSA-N 1-chloro-3-methyl-2-nitrobenzene Chemical compound CC1=CC=CC(Cl)=C1[N+]([O-])=O JLDKNVUJLUGIBQ-UHFFFAOYSA-N 0.000 description 2
• VCHSXYHBMFKRBK-UHFFFAOYSA-N 4771-47-5 Chemical compound OC(=O)C1=CC=CC(Cl)=C1[N+]([O-])=O VCHSXYHBMFKRBK-UHFFFAOYSA-N 0.000 description 2
• QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
• 239000005711 Benzoic acid Substances 0.000 description 2
• FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 2
• YKYOUMDCQGMQQO-UHFFFAOYSA-L cadmium dichloride Chemical compound Cl[Cd]Cl YKYOUMDCQGMQQO-UHFFFAOYSA-L 0.000 description 2
• 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 2
• 238000010168 coupling process Methods 0.000 description 2
• 238000005859 coupling reaction Methods 0.000 description 2
• 238000006193 diazotization reaction Methods 0.000 description 2
• 235000002906 tartaric acid Nutrition 0.000 description 2
• 239000011975 tartaric acid Substances 0.000 description 2
• FYSNRJHAOHDILO-UHFFFAOYSA-N thionyl chloride Chemical compound ClS(Cl)=O FYSNRJHAOHDILO-UHFFFAOYSA-N 0.000 description 2
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
• NGNBDVOYPDDBFK-UHFFFAOYSA-N 2-[2,4-di(pentan-2-yl)phenoxy]acetyl chloride Chemical compound CCCC(C)C1=CC=C(OCC(Cl)=O)C(C(C)CCC)=C1 NGNBDVOYPDDBFK-UHFFFAOYSA-N 0.000 description 1
• -1 2-methyl-6-dimethylamino-i-benzene diazonium chloride Chemical compound 0.000 description 1
• FGMRHNYMZYMARX-UHFFFAOYSA-N 3-amino-2-nitrobenzoic acid Chemical compound NC1=CC=CC(C(O)=O)=C1[N+]([O-])=O FGMRHNYMZYMARX-UHFFFAOYSA-N 0.000 description 1
• AFBPFSWMIHJQDM-UHFFFAOYSA-N N-methylaniline Chemical compound CNC1=CC=CC=C1 AFBPFSWMIHJQDM-UHFFFAOYSA-N 0.000 description 1
• 229920001131 Pulp (paper) Polymers 0.000 description 1
• FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 1
• HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
• ZBHADFXDTSTADC-UHFFFAOYSA-M [Cd]Cl Chemical compound [Cd]Cl ZBHADFXDTSTADC-UHFFFAOYSA-M 0.000 description 1
• 150000007513 acids Chemical class 0.000 description 1
• 239000000654 additive Substances 0.000 description 1
• 239000012670 alkaline solution Substances 0.000 description 1
• 125000000217 alkyl group Chemical group 0.000 description 1
• 229910052782 aluminium Inorganic materials 0.000 description 1
• XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
• 229910021529 ammonia Inorganic materials 0.000 description 1
• 239000007864 aqueous solution Substances 0.000 description 1
• 239000012876 carrier material Substances 0.000 description 1
• 238000006243 chemical reaction Methods 0.000 description 1
• 239000003795 chemical substances by application Substances 0.000 description 1
• 230000008878 coupling Effects 0.000 description 1
• 230000001419 dependent effect Effects 0.000 description 1
• 230000002349 favourable effect Effects 0.000 description 1
• 238000010438 heat treatment Methods 0.000 description 1
• 150000002500 ions Chemical class 0.000 description 1
• 238000002844 melting Methods 0.000 description 1
• 230000008018 melting Effects 0.000 description 1
• 229910052751 metal Inorganic materials 0.000 description 1
• 239000002184 metal Substances 0.000 description 1
• 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
• FCAMUPIRWKNASD-UHFFFAOYSA-N n,n-dimethyl-1-(2-nitrophenyl)methanamine Chemical compound CN(C)CC1=CC=CC=C1[N+]([O-])=O FCAMUPIRWKNASD-UHFFFAOYSA-N 0.000 description 1
• LGQLOGILCSXPEA-UHFFFAOYSA-L nickel sulfate Chemical compound [Ni+2].[O-]S([O-])(=O)=O LGQLOGILCSXPEA-UHFFFAOYSA-L 0.000 description 1
• 229910000363 nickel(II) sulfate Inorganic materials 0.000 description 1
• RNVCVTLRINQCPJ-UHFFFAOYSA-N o-toluidine Chemical compound CC1=CC=CC=C1N RNVCVTLRINQCPJ-UHFFFAOYSA-N 0.000 description 1
• 239000011541 reaction mixture Substances 0.000 description 1
• 230000035945 sensitivity Effects 0.000 description 1
• 239000011780 sodium chloride Substances 0.000 description 1
• 239000000126 substance Substances 0.000 description 1
• 238000004383 yellowing Methods 0.000 description 1