DE69423027T2 - Verfahren zum Herstellen von Essigsäureestern aus Methanol - Google Patents
Verfahren zum Herstellen von Essigsäureestern aus MethanolInfo
- Publication number
- DE69423027T2 DE69423027T2 DE69423027T DE69423027T DE69423027T2 DE 69423027 T2 DE69423027 T2 DE 69423027T2 DE 69423027 T DE69423027 T DE 69423027T DE 69423027 T DE69423027 T DE 69423027T DE 69423027 T2 DE69423027 T2 DE 69423027T2
- Authority
- DE
- Germany
- Prior art keywords
- methanol
- acetic acid
- acid esters
- producing acetic
- producing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/03—Preparation of carboxylic acid esters by reacting an ester group with a hydroxy group
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/02—Preparation of carboxylic acid esters by interreacting ester groups, i.e. transesterification
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/36—Preparation of carboxylic acid esters by reaction with carbon monoxide or formates
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
- C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
- C07C69/02—Esters of acyclic saturated monocarboxylic acids having the carboxyl group bound to an acyclic carbon atom or to hydrogen
- C07C69/12—Acetic acid esters
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/584—Recycling of catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Carbon And Carbon Compounds (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR1019930014392A KR960006546B1 (ko) | 1993-07-28 | 1993-07-28 | 초산에스테르의 제조 방법 |
Publications (2)
Publication Number | Publication Date |
---|---|
DE69423027D1 DE69423027D1 (de) | 2000-03-23 |
DE69423027T2 true DE69423027T2 (de) | 2000-10-19 |
Family
ID=19360210
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE69423027T Expired - Fee Related DE69423027T2 (de) | 1993-07-28 | 1994-07-26 | Verfahren zum Herstellen von Essigsäureestern aus Methanol |
Country Status (6)
Country | Link |
---|---|
US (1) | US5430178A (de) |
EP (1) | EP0640583B1 (de) |
JP (1) | JP2807176B2 (de) |
KR (1) | KR960006546B1 (de) |
DE (1) | DE69423027T2 (de) |
ES (1) | ES2144472T3 (de) |
Families Citing this family (22)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ID22495A (id) * | 1996-12-12 | 1999-10-21 | Sasol Tech Pty Ltd | Pembuatan ester-ester asam organik karboksilat |
US6127432A (en) * | 1998-01-29 | 2000-10-03 | Union Carbide Chemicals & Plastics Technology Corporation | Processes for preparing oxygenates and catalysts therefor |
ATE239691T1 (de) | 1998-03-25 | 2003-05-15 | Sulzer Chemtech Ag | Verfahren und einrichtung zum herstellen von butylacetat und isobutylacetat |
JP2000016966A (ja) * | 1998-07-01 | 2000-01-18 | Mitsubishi Gas Chem Co Inc | アクリル酸エステルまたはメタクリル酸エステルの製造方法 |
US6355837B1 (en) * | 1999-08-25 | 2002-03-12 | Eastman Chemical Company | Vapor phase carbonylation process using group 4 metal promoted iridium catalyst |
CZ292620B6 (cs) | 1999-10-14 | 2003-11-12 | Sulzer Chemtech Ltd. | Způsob výroby etylacetátu a zařízení k provádění tohoto způsobu |
US6441222B1 (en) * | 2000-05-22 | 2002-08-27 | Eastman Chemical Company | Vapor phase carbonylation process using iridium-gold co-catalysts |
US6506933B1 (en) * | 2000-05-22 | 2003-01-14 | Eastman Chemical Company | Vapor phase carbonylation process using gold catalysts |
CA2496839A1 (en) | 2004-07-19 | 2006-01-19 | Woodland Chemical Systems Inc. | Process for producing ethanol from synthesis gas rich in carbon monoxide |
WO2007117590A2 (en) | 2006-04-05 | 2007-10-18 | Woodland Biofuels Inc. | System and method for converting biomass to ethanol via syngas |
JP5072251B2 (ja) * | 2006-04-06 | 2012-11-14 | 三菱重工業株式会社 | モノ低級アルキルモノアルカノールアミンの製造方法および装置 |
CN103189125A (zh) * | 2010-11-12 | 2013-07-03 | 伊士曼化工公司 | 羰基化过程产生的气流的处理 |
CN105330538A (zh) | 2011-05-27 | 2016-02-17 | 瑞来斯实业有限公司 | 采用离子流体进行酯化反应的工艺 |
CA2872354C (en) * | 2012-05-02 | 2017-04-25 | Niels Christian Schjodt | Process for the production of chemical compounds from carbon dioxide |
CN106140156A (zh) * | 2015-04-20 | 2016-11-23 | 中国科学院大连化学物理研究所 | 一种活性炭负载的铑基催化剂及其制备方法和应用 |
CN106316846B (zh) * | 2016-08-26 | 2018-12-25 | 西南化工研究设计院有限公司 | 一种乙酸甲酯的生产方法 |
CN108067226A (zh) * | 2016-11-15 | 2018-05-25 | 中国科学院大连化学物理研究所 | 一种活性炭负载的铱基催化剂及其制备与应用 |
CN108069857A (zh) * | 2016-11-15 | 2018-05-25 | 中国科学院大连化学物理研究所 | 一种用于甲醇气相羰基化制乙酸甲酯的活性炭负载铱基催化剂及其应用 |
CN106810450B (zh) * | 2017-02-23 | 2023-08-08 | 天津大学 | 一种催化反应精馏制备邻苯二甲酸二丁酯的装置和方法 |
CN107162257A (zh) * | 2017-05-24 | 2017-09-15 | 北京师范大学 | 一种饮用水净化系统及其净化方法 |
CN108821967A (zh) * | 2018-08-07 | 2018-11-16 | 中国天辰工程有限公司 | 一种高纯度酯类物质的合成工艺 |
CN111195516B (zh) * | 2018-11-20 | 2021-04-23 | 中国科学院大连化学物理研究所 | 一种原子级单分散铑基催化剂、其制备方法及在甲醇气相羰基化制备乙酸甲酯中的应用 |
Family Cites Families (25)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CA593337A (en) * | 1960-03-01 | G. Hess Lawrence | Synthesis of organic oxygen-containing compounds | |
GB247050A (en) | 1925-05-21 | 1926-02-11 | Basf Ag | Improvements in the purification of gases |
US1864643A (en) * | 1926-01-20 | 1932-06-28 | Celanese Corp | Manufacture of aliphatic acids and esters |
CH459971A (fr) * | 1966-11-01 | 1968-07-31 | Mini Ind Chimice | Procédé de transestérification des esters méthyliques des acides organiques inférieurs |
SE364255B (de) * | 1967-04-05 | 1974-02-18 | Monsanto Co | |
US3717670A (en) * | 1968-08-02 | 1973-02-20 | Monsanto Co | Production of carboxylic acids and esters |
US4690912A (en) * | 1968-08-15 | 1987-09-01 | Monsanto Company | Rhodium-containing carbonylation catalysts with halogen-containing promoter |
US4246195A (en) * | 1978-10-06 | 1981-01-20 | Halcon Research And Development Corporation | Purification of carbonylation products |
JPS56164838A (en) * | 1980-05-24 | 1981-12-18 | Unitika Ltd | Dipping treatment of polyester fibrous material used for reinforcing rubber |
US4810821A (en) * | 1981-10-09 | 1989-03-07 | Monsanto Company | Preparation of alkylidene diesters |
US4514336A (en) * | 1982-05-28 | 1985-04-30 | Shell Oil Company | Homologous carboxylic acids production |
JPS59116115A (ja) * | 1982-12-20 | 1984-07-04 | Osaka Gas Co Ltd | 一酸化炭素の回収方法 |
CA1234147A (en) * | 1983-07-06 | 1988-03-15 | Eit Drent | Process for the preparation of ethanol and/or ethyl acetate |
DE3329781A1 (de) * | 1983-08-18 | 1985-02-28 | Hoechst Ag, 6230 Frankfurt | Verfahren zur abtrennung von jod und dessen verbindungen aus den bei der carbonylierung von dimethylether, methylacetat oder methanol erhaltenen carbonylierungsprodukten |
US5214203A (en) * | 1983-09-02 | 1993-05-25 | Daicel Chemical Industries, Ltd. | Process for producing carboxylic acids |
JPS6054334A (ja) * | 1983-09-02 | 1985-03-28 | Daicel Chem Ind Ltd | カルボン酸の製造法 |
JPS60199853A (ja) * | 1984-03-22 | 1985-10-09 | Daicel Chem Ind Ltd | アセチル化合物の製造法 |
US5144068A (en) * | 1984-05-03 | 1992-09-01 | Hoechst Celanese Corporation | Methanol carbonylation process |
US5026908A (en) * | 1984-05-03 | 1991-06-25 | Hoechst Celanese Corporation | Methanol carbonylation process |
US5185462A (en) * | 1987-01-08 | 1993-02-09 | Bp Chemicals Limited | Production of carboxylic acids and esters thereof |
DK158221C (da) * | 1987-06-30 | 1990-09-10 | Haldor Topsoe As | Fremgangsmaade til fremstilling af eddikesyre, metylacetat, eddikesyreanhydrid eller blandinger deraf |
GB8729267D0 (en) * | 1987-12-15 | 1988-01-27 | Shell Int Research | Process for production of propionate esters |
US5218140A (en) * | 1988-08-02 | 1993-06-08 | Union Carbide Chemicals & Plastics Technology Corporation | Carbonylation reaction and catalyst therefor |
KR960007736B1 (ko) * | 1993-07-27 | 1996-06-11 | 한국과학기술연구원 | 원료 가스 중에 함유된 철 카르보닐 화합물의 제거 방법 |
DE4321766C2 (de) * | 1992-06-30 | 1996-11-28 | Korea Inst Sci & Tech | Verfahren zur gleichzeitigen Herstellung von Essigsäure, Methylacetat und Essigsäureanhydrid |
-
1993
- 1993-07-28 KR KR1019930014392A patent/KR960006546B1/ko not_active IP Right Cessation
-
1994
- 1994-07-26 DE DE69423027T patent/DE69423027T2/de not_active Expired - Fee Related
- 1994-07-26 EP EP94111650A patent/EP0640583B1/de not_active Expired - Lifetime
- 1994-07-26 ES ES94111650T patent/ES2144472T3/es not_active Expired - Lifetime
- 1994-07-27 US US08/281,187 patent/US5430178A/en not_active Expired - Fee Related
- 1994-07-28 JP JP6176537A patent/JP2807176B2/ja not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
EP0640583B1 (de) | 2000-02-16 |
EP0640583A3 (de) | 1995-08-02 |
JPH07149691A (ja) | 1995-06-13 |
DE69423027D1 (de) | 2000-03-23 |
KR950003254A (ko) | 1995-02-16 |
KR960006546B1 (ko) | 1996-05-17 |
ES2144472T3 (es) | 2000-06-16 |
EP0640583A2 (de) | 1995-03-01 |
US5430178A (en) | 1995-07-04 |
JP2807176B2 (ja) | 1998-10-08 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
8364 | No opposition during term of opposition | ||
8339 | Ceased/non-payment of the annual fee |