DE69422819D1 - Verfahren zur herstellung von cyclischen estern - Google Patents

Verfahren zur herstellung von cyclischen estern

Info

Publication number
DE69422819D1
DE69422819D1 DE69422819T DE69422819T DE69422819D1 DE 69422819 D1 DE69422819 D1 DE 69422819D1 DE 69422819 T DE69422819 T DE 69422819T DE 69422819 T DE69422819 T DE 69422819T DE 69422819 D1 DE69422819 D1 DE 69422819D1
Authority
DE
Germany
Prior art keywords
cyclic esters
starting materials
recovery
production
molecular weight
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69422819T
Other languages
English (en)
Inventor
W Verser
J Eggeman
A Evanko
H Schilling
Manfred Meiser
E Allen
E Hillman
E Cremeans
S Lipinski
Alex Cheung
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Biopak Technology Ltd
Original Assignee
Biopak Technology Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Biopak Technology Ltd filed Critical Biopak Technology Ltd
Application granted granted Critical
Publication of DE69422819D1 publication Critical patent/DE69422819D1/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D319/00—Heterocyclic compounds containing six-membered rings having two oxygen atoms as the only ring hetero atoms
    • C07D319/10—1,4-Dioxanes; Hydrogenated 1,4-dioxanes
    • C07D319/12—1,4-Dioxanes; Hydrogenated 1,4-dioxanes not condensed with other rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/48—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
    • C08J5/18—Manufacture of films or sheets
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L67/00—Compositions of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Compositions of derivatives of such polymers
    • C08L67/04—Polyesters derived from hydroxycarboxylic acids, e.g. lactones
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D167/00—Coating compositions based on polyesters obtained by reactions forming a carboxylic ester link in the main chain; Coating compositions based on derivatives of such polymers
    • C09D167/04—Polyesters derived from hydroxycarboxylic acids, e.g. lactones
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/19—Details relating to the geometry of the reactor
    • B01J2219/194—Details relating to the geometry of the reactor round
    • B01J2219/1941—Details relating to the geometry of the reactor round circular or disk-shaped
    • B01J2219/1942—Details relating to the geometry of the reactor round circular or disk-shaped spherical
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2367/00—Characterised by the use of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Derivatives of such polymers
    • C08J2367/04—Polyesters derived from hydroxy carboxylic acids, e.g. lactones
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Materials Engineering (AREA)
  • Polymers & Plastics (AREA)
  • Manufacturing & Machinery (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Heterocyclic Compounds That Contain Two Or More Ring Oxygen Atoms (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
DE69422819T 1993-09-29 1994-09-13 Verfahren zur herstellung von cyclischen estern Expired - Lifetime DE69422819D1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US08/128,797 US5420304A (en) 1992-03-19 1993-09-29 Method to produce cyclic esters
PCT/US1994/010286 WO1995009142A1 (en) 1993-09-29 1994-09-13 Method to produce cyclic esters

Publications (1)

Publication Number Publication Date
DE69422819D1 true DE69422819D1 (de) 2000-03-02

Family

ID=22437018

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69422819T Expired - Lifetime DE69422819D1 (de) 1993-09-29 1994-09-13 Verfahren zur herstellung von cyclischen estern

Country Status (15)

Country Link
US (2) US5420304A (de)
EP (1) EP0722433B1 (de)
JP (1) JPH09502997A (de)
CN (1) CN1136309A (de)
AT (1) ATE189204T1 (de)
AU (1) AU7726794A (de)
BR (1) BR9407655A (de)
CA (1) CA2172798A1 (de)
DE (1) DE69422819D1 (de)
FI (1) FI961402A (de)
MY (1) MY113939A (de)
PH (1) PH30804A (de)
TW (1) TW321646B (de)
WO (1) WO1995009142A1 (de)
ZA (2) ZA961426B (de)

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RU2179550C2 (ru) 1995-06-07 2002-02-20 Новус Интернэшнл, Инк. Способ получения 2-гидрокси-4-метилтиомасляной кислоты или ее солей
US5856567A (en) * 1995-06-07 1999-01-05 Novus International, Inc. Continuous hydrolysis process for preparing 2-hydroxy-4-methylthiobutanioc acid or salts thereof
US5830991A (en) * 1996-02-09 1998-11-03 Kureha Kagaku Kagyo Kk Preparation process and purification process of dimeric cyclic ester of hydroxycarboxylic acid
US6229046B1 (en) 1997-10-14 2001-05-08 Cargill, Incorported Lactic acid processing methods arrangements and products
US6475759B1 (en) * 1997-10-14 2002-11-05 Cargill, Inc. Low PH lactic acid fermentation
US6313319B1 (en) 1998-09-25 2001-11-06 Shimadzu Corporation Method for purifying lactide and lactide for food additives
US7074603B2 (en) * 1999-03-11 2006-07-11 Zeachem, Inc. Process for producing ethanol from corn dry milling
CN100575331C (zh) * 1999-03-11 2009-12-30 齐凯姆公司 一种生产乙醇的方法
IL132289A (en) 1999-10-08 2003-12-10 Staley Mfg Co A E Process for conversion of an extracted carboxylic acid to a non-ionized product
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FR2802923B1 (fr) * 1999-12-28 2002-03-08 Roquette Freres Procede de preparation d'une composition d'ester d'acide lactique et son utilisation en tant que solvant
US6509179B1 (en) 2000-10-12 2003-01-21 Barbara I. Veldhuis-Stribos Continuous process for preparing lactic acid
US6984293B2 (en) * 2001-03-15 2006-01-10 Tate & Lyle Ingredients Azeotropic distillation of cyclic esters of hydroxy organic acids
US6916959B2 (en) * 2001-05-11 2005-07-12 Nippon Shokubai Co., Ltd. Halogen-containing aromatic compound
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ES2290466T3 (es) 2002-05-30 2008-02-16 Natureworks Llc Metodos y materiales para la produccion de acido d-lactico en levadura.
EP1626979B1 (de) 2003-05-02 2012-06-06 Cargill, Incorporated Genetisch modifizierte hefeart und fermentationsverfahren, bei denen die genetisch modifizierte hefe eingesetzt wird
CN1938257A (zh) * 2004-01-29 2007-03-28 齐凯姆公司 有机酸的回收
US7652167B2 (en) * 2004-07-19 2010-01-26 Board Of Trustees Of Michigan State University Process for production of organic acid esters
WO2006124899A2 (en) * 2005-05-13 2006-11-23 Cargill, Incorporated Production of derivatives of lactide, production of lactides, and use of lactide in foods and to produce polymers
ZA200711038B (en) 2005-06-02 2009-06-24 Cargill Inc Genetically modified yeast of the species Issatchenkia orientalis and closely related species and fermentation processes using same
JP5121070B2 (ja) 2005-11-23 2013-01-16 ネイチャーワークス・エル・エル・シー Ｌ−又はｄ−ラクタート：フェリチトクロームｃ酸化還元酵素遺伝子が機能しない乳酸産生酵母
CN100545159C (zh) * 2005-12-19 2009-09-30 奇美实业股份有限公司 α-羟基有机酸环酯类化合物的制造方法
BRPI0709607B1 (pt) 2006-03-13 2018-05-08 Cargill Inc cédulas de levedura tendo via rompida de diidroxi acetona fosfato para glicerol e processo de fermentação"
WO2007114017A1 (ja) 2006-03-29 2007-10-11 Bio-Energy Corporation 乳酸発酵液からの乳酸成分の分離方法および分離装置
DE102006055427A1 (de) * 2006-11-22 2008-05-29 Evonik Röhm Gmbh Verfahren zur Herstellung von Tetramethylglycolid
US8329436B2 (en) * 2007-02-09 2012-12-11 Zeachem, Inc. Method of making propanol and ethanol from plant material by biological conversion and gasification
JP2008239601A (ja) * 2007-02-26 2008-10-09 Sumitomo Chemical Co Ltd ラクチド化合物の製造方法
EP2133346A1 (de) * 2008-06-12 2009-12-16 Ktanton Ltd Herstellungsverfahren eines zyklischen Diesters einer Alphahydroxylsäure (AHA)
KR101154029B1 (ko) 2009-05-20 2012-06-07 한국화학연구원 젖산에스테르로부터 락타이드의 직접 전환용 촉매 및 이를 이용한 락타이드의 제조방법
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WO2012055998A1 (en) 2010-10-28 2012-05-03 Total S.A. Use of monascus in organic acid production
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EP2668281A4 (de) 2011-01-25 2015-08-26 Cargill Inc Zusammensetzungen und verfahren zur succinatherstellung
RS57845B1 (sr) 2012-02-09 2018-12-31 Novus Int Inc Ciklični dimeri koji sadrže heteroatom
CN107753462B (zh) 2012-07-12 2021-01-08 诺华丝国际股份有限公司 用于保护生物活性剂的基质和层组合物
WO2014018757A1 (en) 2012-07-25 2014-01-30 Cargill Incorporated Yeast cells having reductive tca pathway from pyruvate to succinate and overexpressing an exogenous nad(p)+ transhydrogenase enzyme
EP2725019B1 (de) * 2012-10-26 2015-04-08 Uhde Inventa-Fischer GmbH Verfahren zur Herstellung cyclischer Diester, insbesondere Dilactid
US9365875B2 (en) 2012-11-30 2016-06-14 Novozymes, Inc. 3-hydroxypropionic acid production by recombinant yeasts
WO2015017721A1 (en) 2013-07-31 2015-02-05 Novozymes A/S 3-hydroxypropionic acid production by recombinant yeasts expressing an insect aspartate 1-decarboxylase
US20170362613A1 (en) 2014-12-19 2017-12-21 Novozymes A/S Recombinant Host Cells For The Production Of 3-Hydroxypropionic Acid
EP3056490A1 (de) * 2015-02-13 2016-08-17 PURAC Biochem BV Verfahren zur Herstellung von Lactid
WO2016138303A1 (en) 2015-02-27 2016-09-01 Novozymes A/S Mutant host cells for the production of 3-hydroxypropionic acid
WO2017035270A1 (en) 2015-08-24 2017-03-02 Novozymes A/S Beta-alanine aminotransferases for the production of 3-hydroxypropionic acid
KR102547252B1 (ko) * 2016-01-08 2023-06-23 에스케이이노베이션 주식회사 유기물질 기상탈수반응 원료의 제조방법
CN106397389B (zh) * 2016-09-07 2019-01-29 南京大学 一种合成乙交酯的工艺方法
CN106554342A (zh) * 2016-10-26 2017-04-05 中国地质大学（武汉） 3，6‑二氯甲基乙交酯及其制备方法和用途
WO2018207904A1 (ja) 2017-05-12 2018-11-15 中外製薬株式会社 環状有機化合物の製造方法
US10584306B2 (en) 2017-08-11 2020-03-10 Board Of Regents Of The University Of Oklahoma Surfactant microemulsions
CN112574165B (zh) * 2020-12-30 2022-01-07 安徽丰原生物技术股份有限公司 一步转化生成丙交酯的方法
CN113387921B (zh) * 2021-06-18 2022-08-19 华东理工大学 一种合成乙交酯的方法
EP4134365A1 (de) * 2021-08-12 2023-02-15 Sulzer Management AG Anlage und effizientes verfahren zur herstellung von lactid aus milchsäure
CN115028615B (zh) * 2022-07-27 2024-01-09 万华化学(四川)有限公司 一种l,l-丙交酯及其制备方法和应用
CN115417851A (zh) * 2022-08-30 2022-12-02 中国科学院长春应用化学研究所 一种乳酸直接制备丙交酯的方法
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Also Published As

Publication number Publication date
FI961402A0 (fi) 1996-03-27
PH30804A (en) 1997-10-17
CA2172798A1 (en) 1995-04-06
MY113939A (en) 2002-06-29
EP0722433A4 (de) 1996-07-31
BR9407655A (pt) 1997-01-28
ZA961426B (en) 1996-06-18
CN1136309A (zh) 1996-11-20
US5420304A (en) 1995-05-30
US5750732A (en) 1998-05-12
WO1995009142A1 (en) 1995-04-06
FI961402A (fi) 1996-03-27
ATE189204T1 (de) 2000-02-15
ZA947211B (en) 1996-06-18
EP0722433A1 (de) 1996-07-24
JPH09502997A (ja) 1997-03-25
AU7726794A (en) 1995-04-18
EP0722433B1 (de) 2000-01-26
TW321646B (de) 1997-12-01

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