DE60320135T2 - Herstellung von blockformen aus einem seltenerdhalogenid, dadurch hergestellte blockformen, ihre verwendung zur herstellung von einkristallen und dadurch hergestellte einkristalle - Google Patents

Herstellung von blockformen aus einem seltenerdhalogenid, dadurch hergestellte blockformen, ihre verwendung zur herstellung von einkristallen und dadurch hergestellte einkristalle Download PDF

Info

Publication number
DE60320135T2
DE60320135T2 DE60320135T DE60320135T DE60320135T2 DE 60320135 T2 DE60320135 T2 DE 60320135T2 DE 60320135 T DE60320135 T DE 60320135T DE 60320135 T DE60320135 T DE 60320135T DE 60320135 T2 DE60320135 T2 DE 60320135T2
Authority
DE
Germany
Prior art keywords
less
rare earth
weight
block
earth metal
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE60320135T
Other languages
German (de)
English (en)
Other versions
DE60320135D1 (de
Inventor
Alain Iltis
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Luxium Solutions SAS
Original Assignee
Saint Gobain Cristaux and Detecteurs SAS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Saint Gobain Cristaux and Detecteurs SAS filed Critical Saint Gobain Cristaux and Detecteurs SAS
Publication of DE60320135D1 publication Critical patent/DE60320135D1/de
Application granted granted Critical
Publication of DE60320135T2 publication Critical patent/DE60320135T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/653Processes involving a melting step
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/515Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
    • C04B35/5152Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on halogenides other than fluorides
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K11/00Luminescent, e.g. electroluminescent, chemiluminescent materials
    • C09K11/08Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials
    • C09K11/77Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals
    • C09K11/7704Halogenides
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09KMATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K11/00Luminescent, e.g. electroluminescent, chemiluminescent materials
    • C09K11/08Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials
    • C09K11/77Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals
    • C09K11/7766Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals containing two or more rare earth metals
    • C09K11/7772Halogenides
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B11/00Single-crystal growth by normal freezing or freezing under temperature gradient, e.g. Bridgman-Stockbarger method
    • CCHEMISTRY; METALLURGY
    • C30CRYSTAL GROWTH
    • C30BSINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/10Inorganic compounds or compositions
    • C30B29/12Halides
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3201Alkali metal oxides or oxide-forming salts thereof
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3224Rare earth oxide or oxide forming salts thereof, e.g. scandium oxide
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3224Rare earth oxide or oxide forming salts thereof, e.g. scandium oxide
    • C04B2235/3227Lanthanum oxide or oxide-forming salts thereof
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3224Rare earth oxide or oxide forming salts thereof, e.g. scandium oxide
    • C04B2235/3229Cerium oxides or oxide-forming salts thereof
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/44Metal salt constituents or additives chosen for the nature of the anions, e.g. hydrides or acetylacetonate
    • C04B2235/444Halide containing anions, e.g. bromide, iodate, chlorite
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/656Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
    • C04B2235/6562Heating rate
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/658Atmosphere during thermal treatment
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/74Physical characteristics
    • C04B2235/77Density

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Ceramic Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Metallurgy (AREA)
  • Structural Engineering (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)
  • Luminescent Compositions (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
DE60320135T 2002-11-27 2003-11-13 Herstellung von blockformen aus einem seltenerdhalogenid, dadurch hergestellte blockformen, ihre verwendung zur herstellung von einkristallen und dadurch hergestellte einkristalle Expired - Lifetime DE60320135T2 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR0214856A FR2847594B1 (fr) 2002-11-27 2002-11-27 Preparation de blocs d'halogenure de terre rare
FR0214856 2002-11-27
PCT/FR2003/003356 WO2004050792A1 (fr) 2002-11-27 2003-11-13 Preparation de blocs d'halogenure de terre rare

Publications (2)

Publication Number Publication Date
DE60320135D1 DE60320135D1 (de) 2008-05-15
DE60320135T2 true DE60320135T2 (de) 2009-05-20

Family

ID=32241653

Family Applications (1)

Application Number Title Priority Date Filing Date
DE60320135T Expired - Lifetime DE60320135T2 (de) 2002-11-27 2003-11-13 Herstellung von blockformen aus einem seltenerdhalogenid, dadurch hergestellte blockformen, ihre verwendung zur herstellung von einkristallen und dadurch hergestellte einkristalle

Country Status (15)

Country Link
US (3) US7670578B2 (enExample)
EP (1) EP1567611B1 (enExample)
JP (1) JP4594100B2 (enExample)
KR (1) KR20050086814A (enExample)
CN (2) CN103122483A (enExample)
AT (1) ATE391158T1 (enExample)
AU (1) AU2003290186B2 (enExample)
CA (1) CA2507283A1 (enExample)
DE (1) DE60320135T2 (enExample)
EA (1) EA009230B1 (enExample)
FR (1) FR2847594B1 (enExample)
PL (1) PL206055B1 (enExample)
SI (1) SI1567611T1 (enExample)
UA (1) UA87656C2 (enExample)
WO (1) WO2004050792A1 (enExample)

Families Citing this family (61)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL1014401C2 (nl) * 2000-02-17 2001-09-04 Stichting Tech Wetenschapp Ceriumhoudend anorganisch scintillatormateriaal.
FR2840926B1 (fr) * 2002-06-12 2005-03-04 Saint Gobain Cristaux Detecteu Utilisation d'un creuset comprenant du carbone pour la croissance de cristaux comprenant un halogenure de terre rare
FR2855830B1 (fr) * 2003-06-05 2005-07-08 Stichting Tech Wetenschapp Cristaux scintillateurs du type iodure de terre rare
US7576329B2 (en) * 2003-10-17 2009-08-18 General Electric Company Scintillator compositions, and related processes and articles of manufacture
FR2869115B1 (fr) * 2004-04-14 2006-05-26 Saint Gobain Cristaux Detecteu Materiau scintillateur a base de terre rare a bruit de fond nucleaire reduit
US7202477B2 (en) * 2005-03-04 2007-04-10 General Electric Company Scintillator compositions of cerium halides, and related articles and processes
US20100230601A1 (en) * 2005-03-30 2010-09-16 General Electric Company Composition, article, and method
US20060226368A1 (en) * 2005-03-30 2006-10-12 General Electric Company Scintillator compositions based on lanthanide halides and alkali metals, and related methods and articles
US7700003B2 (en) 2005-03-30 2010-04-20 General Electric Company Composition, article, and method
CN1327043C (zh) * 2005-04-12 2007-07-18 北京工物科技有限责任公司 掺铈氯化镧闪烁晶体的制备方法
US7767971B2 (en) * 2005-09-16 2010-08-03 Stichting Voor De Technische Wetenschappen High light yield fast scintillator
US7541589B2 (en) * 2006-06-30 2009-06-02 General Electric Company Scintillator compositions based on lanthanide halides, and related methods and articles
JP5103879B2 (ja) 2006-09-20 2012-12-19 日立化成工業株式会社 シンチレータ用結晶及び放射線検出器
US20080131347A1 (en) * 2006-12-04 2008-06-05 General Electric Company Scintillation compositions and method of manufacture thereof
US20080131348A1 (en) * 2006-12-04 2008-06-05 General Electric Company Scintillation compositions and method of manufacture thereof
US9404036B2 (en) * 2007-10-30 2016-08-02 The Regents Of The University Of California Alkali metal and alkali earth metal gadolinium halide scintillators
EP2220515A2 (en) * 2007-11-09 2010-08-25 Koninklijke Philips Electronics N.V. Protection of hygroscopic scintillators
US7767975B2 (en) * 2007-12-04 2010-08-03 Saint-Gobain Cristaux Et Detecteurs Ionizing radiation detector
FR2929296B1 (fr) * 2008-03-31 2011-01-21 Saint Gobain Cristaux Detecteurs Recuit de monocristaux
US20100224798A1 (en) * 2008-09-11 2010-09-09 Stichting Voor De Technische Wetenschappen Scintillator based on lanthanum iodide and lanthanum bromide
CN101824646B (zh) * 2009-03-02 2012-05-30 北京滨松光子技术股份有限公司 真空封闭式坩埚下降法生长掺铊碘化钠单晶体
US8673179B2 (en) * 2009-10-09 2014-03-18 Hellma Materials Gmbh Scintillation materials of low oxygen content and process for producing same
US20110085957A1 (en) * 2009-10-09 2011-04-14 Johann-Christoph Von Saldern Process for producing scintillation materials of low strain birefringence and high refractive index uniformity
FR2954760B1 (fr) 2009-12-28 2013-12-27 Saint Gobain Cristaux Et Detecteurs Scintillateur en halogenure de terre rare cristallin a face sensible polie
US8598530B2 (en) * 2010-05-10 2013-12-03 Siemens Medical Solutions Usa, Inc. Chloride scintillator for radiation detection
US8834745B2 (en) 2010-05-27 2014-09-16 Ocean's King Lighting Science & Technology Co., Ltd. Oxyhalide luminescent material doped with rare earth containing metal particle and production method thereof
CN101913766B (zh) * 2010-08-04 2012-05-30 宁波大学 一种稀土离子掺杂的卤氧硅酸盐玻璃及其制备方法
US8519347B2 (en) * 2010-08-10 2013-08-27 Northwestern University Methods and compositions for the detection of X-ray and gamma-ray radiation
WO2012066425A2 (en) 2010-11-16 2012-05-24 Saint-Gobain Cristaux Et Detecteurs Scintillation compound including a rare earth element and a process of forming the same
EP3670633A1 (en) * 2011-06-06 2020-06-24 Saint-Gobain Ceramics and Plastics, Inc. Scintillation crystal including a rare earth halide, and a radiation detection system including the scintillation crystal
CN102230215B (zh) * 2011-06-28 2015-05-13 中国计量学院 一种掺铈氯溴化镧闪烁晶体的制备方法
FR2978251B1 (fr) 2011-07-19 2014-04-18 Saint Gobain Cristaux Et Detecteurs Detecteur a scintillateur conique
EP4234659B1 (en) * 2011-09-22 2025-07-02 Luxium Solutions Apparatus comprising a scintillator
WO2014066900A1 (en) * 2012-10-28 2014-05-01 Stichting Voor De Technische Wetenschappen Scintillation crystal including a rare earth halide, and a radiation detection apparatus including the scintillation crystal
FR3004467B1 (fr) 2013-04-12 2016-05-27 Saint-Gobain Cristaux Et Detecteurs Fabrication d'une elpasolite stoechiometrique
RU2016105053A (ru) * 2013-07-17 2017-08-21 Конинклейке Филипс Н.В. АКТИВИРОВАННЫЕ ЛЮМИНЕСЦЕНТНЫЕ СОСТАВЫ НА ОСНОВЕ Ce3+ ДЛЯ ПРИМЕНЕНИЯ В СИСТЕМАХ ФОРМИРОВАНИЯ ИЗОБРАЖЕНИЯ
CN103409769B (zh) * 2013-07-31 2017-05-03 有研稀土新材料股份有限公司 提纯稀土卤化物的装置及其方法
CN104418378B (zh) * 2013-08-26 2016-09-14 中国科学院过程工程研究所 XNH4Br·LaBr3·YH2O、其制备方法以及无水溴化镧的制备方法
US9334444B1 (en) 2014-02-11 2016-05-10 Sandia Corporation Sorohalide scintillators, phosphors, and uses thereof
FR3022555B1 (fr) 2014-06-23 2017-12-22 Saint-Gobain Cristaux Et Detecteurs Materiau luminescent a couche photonique texturee
CN104326502B (zh) * 2014-11-06 2015-11-18 赣州有色冶金研究所 气相法制备无水氯化稀土的方法和装置
US10379230B2 (en) 2015-06-03 2019-08-13 Northwestern University Chalco-phosphate-based hard radiation detectors
CN106753378A (zh) * 2015-11-24 2017-05-31 有研稀土新材料股份有限公司 高纯无水复合稀土卤化物及其制备方法
EP3423327B1 (en) 2016-03-04 2022-05-11 Continental Teves AG & Co. OHG Method to determine the roll angle of a motorcycle
CN108264079B (zh) * 2016-12-30 2020-03-27 有研稀土新材料股份有限公司 含氢稀土卤化物、其制备方法及应用
CN107215887B (zh) * 2017-06-09 2018-05-04 厦门中烁光电科技有限公司 无水溴化铈的制备方法
CN109988577B (zh) * 2017-12-27 2020-12-25 有研稀土新材料股份有限公司 稀土卤化物闪烁材料及其应用
WO2019137962A1 (fr) 2018-01-11 2019-07-18 Stichting Voor De Technische Wetenschappen Matériau scintillateur comprenant un halogénure de cation cristallin dopé par eu2+ et co-dopé par sm2+
CN109576789A (zh) * 2018-12-29 2019-04-05 厦门中烁光电科技有限公司 铈掺杂稀土卤化物单晶的处理方法
CN110219046B (zh) * 2019-05-31 2021-08-06 山东大学 一种用于大尺寸溴铅铯单晶体的可视化定向生长装置及生长方法
CN110982527B (zh) * 2019-11-01 2021-12-14 有研稀土新材料股份有限公司 稀土卤化物闪烁材料
KR102595966B1 (ko) 2020-04-14 2023-11-01 세인트-고바인 세라믹스 앤드 플라스틱스, 인크. 이온 전도성 재료, 이온 전도성 재료를 포함하는 전해질 및 형성 방법
EP4101021B1 (en) 2020-04-14 2025-09-03 Saint-Gobain Ceramics & Plastics Inc. Electrolyte material and methods of forming
KR20230079480A (ko) 2020-04-23 2023-06-07 세인트-고바인 세라믹스 앤드 플라스틱스, 인크. 이온 전도층 및 형성 방법
FI4104232T3 (fi) 2020-04-23 2025-12-12 Saint Gobain Ceramics Ioneja johtava kerros ja muodostamismenetelmiä
CN120727955A (zh) 2020-08-07 2025-09-30 圣戈本陶瓷及塑料股份有限公司 电解质材料及其形成方法
FR3114104A1 (fr) 2020-09-15 2022-03-18 Saint-Gobain Cristaux Et Detecteurs Matériau scintillateur comprenant une pérovskite d’halogénure dopée
CN115216840B (zh) * 2021-04-14 2023-10-13 中国科学院上海硅酸盐研究所 离子补偿法制备锂铊共掺杂碘化钠闪烁晶体的方法
KR102637203B1 (ko) 2021-05-17 2024-02-19 세인트-고바인 세라믹스 앤드 플라스틱스, 인크. 전해질 물질 및 형성 방법
CN113336255B (zh) * 2021-08-05 2021-10-29 天津包钢稀土研究院有限责任公司 一种稀土卤化物熔盐的提纯方法
CN114959894B (zh) * 2022-05-09 2023-06-09 中国科学院福建物质结构研究所 一种多孔卤氧化镧单晶材料及其制备方法和应用

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4179492A (en) * 1977-07-08 1979-12-18 Cato Research Corp. Process for making rare earth metal chlorides
US5309452B1 (en) * 1992-01-31 1998-01-20 Univ Rutgers Praseodymium laser system
JPH06135715A (ja) * 1992-10-28 1994-05-17 Mitsubishi Materials Corp 高純度希土類ハロゲン化物の製造方法
JPH07157395A (ja) * 1993-12-03 1995-06-20 Tosoh Corp 光化学ホールバーニング結晶及びその製造法
DE4443001A1 (de) * 1993-12-03 1995-06-08 Tosoh Corp Sm·2·+ als aktive Ionen enthaltender Kristall vom fehlgeordneten Fluorit-Typ zum photochemischen Lochbrennen
FR2799194B1 (fr) * 1999-10-05 2001-12-14 Corning Sa Billes d'un fluorure d'alcalin ou d'alcalino-terreux polycristallin, leur preparation et leur utilisation pour preparer des monocristaux
NL1014401C2 (nl) * 2000-02-17 2001-09-04 Stichting Tech Wetenschapp Ceriumhoudend anorganisch scintillatormateriaal.
FR2840926B1 (fr) * 2002-06-12 2005-03-04 Saint Gobain Cristaux Detecteu Utilisation d'un creuset comprenant du carbone pour la croissance de cristaux comprenant un halogenure de terre rare
US7084403B2 (en) * 2003-10-17 2006-08-01 General Electric Company Scintillator compositions, and related processes and articles of manufacture
FR2869115B1 (fr) 2004-04-14 2006-05-26 Saint Gobain Cristaux Detecteu Materiau scintillateur a base de terre rare a bruit de fond nucleaire reduit

Also Published As

Publication number Publication date
JP2006508227A (ja) 2006-03-09
DE60320135D1 (de) 2008-05-15
EP1567611A1 (fr) 2005-08-31
EP1567611B1 (fr) 2008-04-02
EA200500877A1 (ru) 2005-10-27
CN103122483A (zh) 2013-05-29
WO2004050792A1 (fr) 2004-06-17
FR2847594A1 (fr) 2004-05-28
US20100098613A1 (en) 2010-04-22
PL375231A1 (en) 2005-11-28
US7670578B2 (en) 2010-03-02
CA2507283A1 (fr) 2004-06-17
JP4594100B2 (ja) 2010-12-08
US8021636B2 (en) 2011-09-20
US20060104880A1 (en) 2006-05-18
SI1567611T1 (sl) 2008-08-31
FR2847594B1 (fr) 2004-12-24
KR20050086814A (ko) 2005-08-30
PL206055B1 (pl) 2010-06-30
AU2003290186B2 (en) 2009-07-30
US8252260B2 (en) 2012-08-28
EA009230B1 (ru) 2007-12-28
AU2003290186A1 (en) 2004-06-23
US20110293499A1 (en) 2011-12-01
CN1717466A (zh) 2006-01-04
ATE391158T1 (de) 2008-04-15
CN1717466B (zh) 2013-02-06
UA87656C2 (ru) 2009-08-10

Similar Documents

Publication Publication Date Title
DE60320135T2 (de) Herstellung von blockformen aus einem seltenerdhalogenid, dadurch hergestellte blockformen, ihre verwendung zur herstellung von einkristallen und dadurch hergestellte einkristalle
CN113174635B (zh) 钾冰晶石类型闪烁体材料的制备
DE102012101199B4 (de) Iodid-Szintillatoren mit Europium-Dotierung
DE102011050767B4 (de) Züchtungsverfahren für einen Einkristall-Szintillator-Werkstoff auf der Basis von Oxysilikaten und nach dem Verfahren hergestellter Einkirstall-Szintillator-Werkstoff
JP6978157B2 (ja) 結晶シンチレータを製造する方法
DE112012004222T5 (de) Metallhalogenid-Szintillatoren mit verminderter Hygroskopizität und Verfahren zu ihrer Herstellung
DE10217946A1 (de) Quarzglastiegel und Verfahren zur Herstellung desselben
DE69508473T2 (de) Verfahren zur Herstellung von Silizium-Einkristall und Tiegel aus geschmolzenem Silika dafür
DE102011115149B4 (de) Verwendung einer Substanz umfassend ein Element der Gruppe 7 des Periodensystems zur Unterdrückung von Kristallwachstumsinstabilitäten während der Herstellung von Seltenerd-Oxyorthosilikat-Kristallen
DE102014118239A1 (de) Chlorid-, Bromid- und Iodid-Szintillatoren mit Europium-Dotierung
DE1259486B (de) Szintillationskristall und Verfahren zu seiner Herstellung
DE102009043003A1 (de) Herstellung von Seltenerd-Aluminium- oder -Gallium-Granat-Kristallen aus einer fluoridhaltigen Schmelze sowie ihre Verwendung als optisches Element für die Mirolithographie sowie als Szintillator
DE102009028842A1 (de) Szintillationsmaterial in einkristalliner, polykristalliner oder keramischer Form
DE1667604B1 (de) Verfahren zur herstellung von kristallinem cadmiumtellurid
EP2308949A1 (de) Szintillationsmaterial mit verbesserten Eigenschaften und Verfahren zur Herstellung derselben
DE102010044017A1 (de) Herstellung von strahlungsbeständigen Fluorid-Kristallen, insbesondere von Kalziumfluorid-Kristallen
DE102009043002A1 (de) Verwendung eines Fluoridflussmittels zur Kristallisation von Seltenerd-Aluminium-Granat aus einer Schmelze zur Herstellung optischer Elemente für die Mikrolithographie sowie von Szintillatoren
DE69612245T2 (de) Verfahren zur Herstellung eines Einkristalles aus seltenen Erden Silikate
DE102009045520A1 (de) Verfahren zur Herstellung von Szintillationsmaterialien mit geringer Spannungsdoppelbrechung und hoher Homogenität der Brechzahl
Yoshikawa et al. Scintillating bulk oxide crystals
DE2400911C3 (de) Verfahren zur Herstellung von Neodym-Ultraphosphaten
EP2308948A1 (de) Szintillatormaterialien mit geringem Sauerstoffgehalt und Verfahren zur Herstellung derselben

Legal Events

Date Code Title Description
8364 No opposition during term of opposition