DE4397599C2 - Verfahren zur Herstellung von hochreinen Isomeren der Benzoldicarbonsäure - Google Patents

Verfahren zur Herstellung von hochreinen Isomeren der Benzoldicarbonsäure

Info

Publication number
DE4397599C2
DE4397599C2 DE4397599A DE4397599A DE4397599C2 DE 4397599 C2 DE4397599 C2 DE 4397599C2 DE 4397599 A DE4397599 A DE 4397599A DE 4397599 A DE4397599 A DE 4397599A DE 4397599 C2 DE4397599 C2 DE 4397599C2
Authority
DE
Germany
Prior art keywords
oxidation
post
ppm
oxidation step
concentration
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE4397599A
Other languages
German (de)
English (en)
Other versions
DE4397599T1 (de
Inventor
Vladimir Filippovich Nazimok
Nadezhda Nikolaevna Goncharova
Valerij Petrovich Yurjev
Vladimir Dmitrievich Manzurov
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
JOINT-STOCK Co OF RESEARCH AND DESIGN INSTITU
Hanwha TotalEnergies Petrochemical Co Ltd
Original Assignee
Samsung General Chemicals Co Ltd
NIPIM AO
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from RU93046190/04A external-priority patent/RU2047594C1/ru
Priority claimed from RU93046191/04A external-priority patent/RU2047595C1/ru
Application filed by Samsung General Chemicals Co Ltd, NIPIM AO filed Critical Samsung General Chemicals Co Ltd
Application granted granted Critical
Publication of DE4397599C2 publication Critical patent/DE4397599C2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/48—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C63/00—Compounds having carboxyl groups bound to a carbon atoms of six-membered aromatic rings
    • C07C63/14—Monocyclic dicarboxylic acids
    • C07C63/15—Monocyclic dicarboxylic acids all carboxyl groups bound to carbon atoms of the six-membered aromatic ring
    • C07C63/26—1,4 - Benzenedicarboxylic acid

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
DE4397599A 1993-09-28 1993-11-30 Verfahren zur Herstellung von hochreinen Isomeren der Benzoldicarbonsäure Expired - Lifetime DE4397599C2 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
RU93046190/04A RU2047594C1 (ru) 1993-09-28 1993-09-28 Способ получения изомеров бензолдикарбоновых кислот с высокой степенью очистки
RU93046191/04A RU2047595C1 (ru) 1993-09-28 1993-09-28 Способ получения изомеров фталевых кислот с высокой степенью чистоты
PCT/KR1993/000106 WO1995009143A1 (en) 1993-09-28 1993-11-30 Production method of high purity isomers of benzenedicarboxylic acids

Publications (1)

Publication Number Publication Date
DE4397599C2 true DE4397599C2 (de) 1998-02-19

Family

ID=26653761

Family Applications (2)

Application Number Title Priority Date Filing Date
DE4397599A Expired - Lifetime DE4397599C2 (de) 1993-09-28 1993-11-30 Verfahren zur Herstellung von hochreinen Isomeren der Benzoldicarbonsäure
DE4397599T Pending DE4397599T1 (de) 1993-09-28 1993-11-30 Verfahren zur Herstellung von hochreinen Isomeren von Benzoldikarbonsäure

Family Applications After (1)

Application Number Title Priority Date Filing Date
DE4397599T Pending DE4397599T1 (de) 1993-09-28 1993-11-30 Verfahren zur Herstellung von hochreinen Isomeren von Benzoldikarbonsäure

Country Status (21)

Country Link
US (1) US5359133A (enExample)
JP (1) JP3009223B2 (enExample)
KR (1) KR970000136B1 (enExample)
CN (1) CN1050118C (enExample)
AU (1) AU5576394A (enExample)
BE (1) BE1008546A4 (enExample)
BG (1) BG62324B1 (enExample)
BR (1) BR9305996A (enExample)
CA (1) CA2128719C (enExample)
DE (2) DE4397599C2 (enExample)
ES (1) ES2081265B1 (enExample)
FR (1) FR2710638B1 (enExample)
GB (1) GB2286588B (enExample)
IT (1) IT1271011B (enExample)
MY (1) MY108978A (enExample)
PL (1) PL175685B1 (enExample)
RO (1) RO113850B1 (enExample)
SA (1) SA94140587B1 (enExample)
SK (1) SK280582B6 (enExample)
TW (1) TW307753B (enExample)
WO (1) WO1995009143A1 (enExample)

Families Citing this family (91)

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WO1996041790A1 (en) * 1995-06-08 1996-12-27 Mogilev Order Of Lenin Proizvodstvennoe Obiedinenie 'khimvolokno' Named After V.I. Lenin Method of obtaining isophthalic acid of monomeric purity
JP3757995B2 (ja) * 1996-07-12 2006-03-22 三菱瓦斯化学株式会社 高純度イソフタル酸の製造方法
JP3341620B2 (ja) * 1997-03-19 2002-11-05 株式会社日立製作所 芳香族ポリカルボン酸の製造方法および装置
KR100549107B1 (ko) * 1999-04-28 2006-02-06 삼성토탈 주식회사 아로마틱 폴리카본산의 제조방법
KR20000041506A (ko) 1998-12-22 2000-07-15 유현식 아로마틱폴리카본산의 제조방법
US6180822B1 (en) 1998-12-22 2001-01-30 Samsung General Chemical Co., Ltd. Method of producing aromatic carboxylic acids by oxidizing alkyl aromatic compounds or partially oxidized intermediates thereof with carbon dioxide containing gas
US6194607B1 (en) † 1998-12-22 2001-02-27 Samsung General Chemicals Co., Ltd. Method of producing aromatic carboxylic acids by oxidizing alkyl aromatic hydrocarbons or partially oxidized intermediates thereof
US6399790B1 (en) 1999-11-24 2002-06-04 General Electric Company Method for oxidation of xylene derivatives
US6465685B1 (en) 1999-11-24 2002-10-15 General Electric Company Method for oxidation of xylene derivatives
ATE311355T1 (de) 2000-01-18 2005-12-15 Inca Internat S P A Oxidation von alkylaromaten zu aromatischen säuren in wässrigem medium
US6649773B2 (en) 2002-03-22 2003-11-18 General Electric Company Method for the manufacture of halophthalic acids and anhydrides
US6657068B2 (en) 2002-03-22 2003-12-02 General Electric Company Liquid phase oxidation of halogenated ortho-xylenes
US6657067B2 (en) 2002-03-22 2003-12-02 General Electric Company Method for the manufacture of chlorophthalic anhydride
AU2003293252A1 (en) * 2002-12-09 2004-06-30 Eastman Chemical Company Process for the oxidative purification of terephthalic acid
BR0316462A (pt) * 2002-12-09 2005-10-11 Eastman Chem Co Processos para reduzir uma suspensão de ácido carboxìlico purificado, para purificar um produto de oxidação em estágios, para produzir um produto de ácido carboxìlico purificado, e, suspensão de ácido carboxìlico purificado
US7161027B2 (en) * 2002-12-09 2007-01-09 Eastman Chemical Company Process for the oxidative purification of terephthalic acid
JP2006509044A (ja) * 2002-12-09 2006-03-16 イーストマン ケミカル カンパニー 粗製カルボン酸スラリーの精製方法
RU2341512C2 (ru) * 2002-12-09 2008-12-20 Истман Кемикал Компани Способ очистки суспензии сырой карбоновой кислоты
US7074954B2 (en) * 2002-12-09 2006-07-11 Eastman Chemical Company Process for the oxidative purification of terephthalic acid
US7132566B2 (en) * 2003-09-22 2006-11-07 Eastman Chemical Company Process for the purification of a crude carboxylic acid slurry
US7546747B2 (en) * 2004-01-15 2009-06-16 Eastman Chemical Company Process for production of a dried carboxylic acid cake suitable for use in polyester production
US7348452B2 (en) * 2004-04-22 2008-03-25 Eastman Chemical Company Liquid phase oxidation of P-xylene to terephthalic acid in the presence of a catalyst system containing nickel, manganese, and bromine atoms
US20050283022A1 (en) * 2004-06-18 2005-12-22 Sheppard Ronald B Filtrate preparation process for terephthalic acid filtrate treatment
US7541489B2 (en) 2004-06-30 2009-06-02 Sabic Innovative Plastics Ip B.V. Method of making halophthalic acids and halophthalic anhydrides
US7371894B2 (en) * 2004-09-02 2008-05-13 Eastman Chemical Company Optimized liquid-phase oxidation
US7741515B2 (en) 2004-09-02 2010-06-22 Eastman Chemical Company Optimized liquid-phase oxidation
US7361784B2 (en) 2004-09-02 2008-04-22 Eastman Chemical Company Optimized liquid-phase oxidation
US7608732B2 (en) 2005-03-08 2009-10-27 Eastman Chemical Company Optimized liquid-phase oxidation
US7563926B2 (en) 2004-09-02 2009-07-21 Eastman Chemical Company Optimized liquid-phase oxidation
US7572936B2 (en) 2004-09-02 2009-08-11 Eastman Chemical Company Optimized liquid-phase oxidation
US7582793B2 (en) 2004-09-02 2009-09-01 Eastman Chemical Company Optimized liquid-phase oxidation
US7507857B2 (en) 2004-09-02 2009-03-24 Eastman Chemical Company Optimized liquid-phase oxidation
US7615663B2 (en) * 2004-09-02 2009-11-10 Eastman Chemical Company Optimized production of aromatic dicarboxylic acids
US7910769B2 (en) 2004-09-02 2011-03-22 Eastman Chemical Company Optimized liquid-phase oxidation
US7399882B2 (en) 2004-09-02 2008-07-15 Eastman Chemical Company Optimized liquid-phase oxidation
US7390921B2 (en) 2004-09-02 2008-06-24 Eastman Chemical Company Optimized liquid-phase oxidation
US7572932B2 (en) 2004-09-02 2009-08-11 Eastman Chemical Company Optimized liquid-phase oxidation
US7692037B2 (en) 2004-09-02 2010-04-06 Eastman Chemical Company Optimized liquid-phase oxidation
US7568361B2 (en) 2004-09-02 2009-08-04 Eastman Chemical Company Optimized liquid-phase oxidation
US7482482B2 (en) 2004-09-02 2009-01-27 Eastman Chemical Company Optimized liquid-phase oxidation
US7504535B2 (en) 2004-09-02 2009-03-17 Eastman Chemical Company Optimized liquid-phase oxidation
US7692036B2 (en) 2004-11-29 2010-04-06 Eastman Chemical Company Optimized liquid-phase oxidation
WO2006028817A2 (en) * 2004-09-02 2006-03-16 Eastman Chemical Company Optimized liquid-phase oxidation
US7608733B2 (en) 2004-09-02 2009-10-27 Eastman Chemical Company Optimized liquid-phase oxidation
US7381836B2 (en) 2004-09-02 2008-06-03 Eastman Chemical Company Optimized liquid-phase oxidation
US7495125B2 (en) 2004-09-02 2009-02-24 Eastman Chemical Company Optimized liquid-phase oxidation
US7683210B2 (en) 2004-09-02 2010-03-23 Eastman Chemical Company Optimized liquid-phase oxidation
US7589231B2 (en) 2004-09-02 2009-09-15 Eastman Chemical Company Optimized liquid-phase oxidation
US7586000B2 (en) 2004-09-02 2009-09-08 Eastman Chemical Company Optimized liquid-phase oxidation
US20060205974A1 (en) * 2005-03-08 2006-09-14 Lavoie Gino G Processes for producing aromatic dicarboxylic acids
US7550627B2 (en) * 2005-03-08 2009-06-23 Eastman Chemical Company Processes for producing aromatic dicarboxylic acids
US7834208B2 (en) * 2005-05-19 2010-11-16 Eastman Chemical Company Process to produce a post catalyst removal composition
US7919652B2 (en) * 2005-05-19 2011-04-05 Eastman Chemical Company Process to produce an enriched composition through the use of a catalyst removal zone and an enrichment zone
US7741516B2 (en) * 2005-05-19 2010-06-22 Eastman Chemical Company Process to enrich a carboxylic acid composition
US7557243B2 (en) * 2005-05-19 2009-07-07 Eastman Chemical Company Enriched terephthalic acid composition
US7897809B2 (en) * 2005-05-19 2011-03-01 Eastman Chemical Company Process to produce an enrichment feed
US20060264656A1 (en) * 2005-05-19 2006-11-23 Fujitsu Limited Enrichment process using compounds useful in a polyester process
US7432395B2 (en) * 2005-05-19 2008-10-07 Eastman Chemical Company Enriched carboxylic acid composition
US7884231B2 (en) * 2005-05-19 2011-02-08 Eastman Chemical Company Process to produce an enriched composition
US7880031B2 (en) * 2005-05-19 2011-02-01 Eastman Chemical Company Process to produce an enrichment feed
US20060264662A1 (en) * 2005-05-19 2006-11-23 Gibson Philip E Esterification of an enriched composition
US20060264664A1 (en) * 2005-05-19 2006-11-23 Parker Kenny R Esterification of an exchange solvent enriched composition
US7884232B2 (en) 2005-06-16 2011-02-08 Eastman Chemical Company Optimized liquid-phase oxidation
US20070155987A1 (en) * 2006-01-04 2007-07-05 O'meadhra Ruairi S Oxidative digestion with optimized agitation
US7358389B2 (en) 2006-01-04 2008-04-15 Eastman Chemical Company Oxidation system employing internal structure for enhanced hydrodynamics
US7355068B2 (en) 2006-01-04 2008-04-08 Eastman Chemical Company Oxidation system with internal secondary reactor
US20070179312A1 (en) * 2006-02-02 2007-08-02 O'meadhra Ruairi Seosamh Process for the purification of a crude carboxylic axid slurry
US7326807B2 (en) * 2006-03-01 2008-02-05 Eastman Chemical Company Polycarboxylic acid production system with enhanced heating for oxidative digestion
US7772424B2 (en) * 2006-03-01 2010-08-10 Eastman Chemical Company Polycarboxylic acid production system employing enhanced evaporative concentration downstream of oxidative digestion
US7326808B2 (en) * 2006-03-01 2008-02-05 Eastman Chemical Company Polycarboxylic acid production system employing cooled mother liquor from oxidative digestion as feed to impurity purge system
US20070208194A1 (en) 2006-03-01 2007-09-06 Woodruff Thomas E Oxidation system with sidedraw secondary reactor
US7501537B2 (en) * 2006-03-01 2009-03-10 Eastman Chemical Company Polycarboxylic acid production system employing oxidative digestion with reduced or eliminated upstream liquor exchange
US7393973B2 (en) * 2006-03-01 2008-07-01 Eastman Chemical Company Polycarboxylic acid production system with enhanced residence time distribution for oxidative digestion
US7816556B2 (en) * 2006-03-01 2010-10-19 Eastman Chemical Company Polycarboxylic acid production system employing enhanced multistage oxidative digestion
US7420082B2 (en) * 2006-03-01 2008-09-02 Eastman Chemical Company Polycarboxylic acid production system employing hot liquor removal downstream of oxidative digestion
US7888529B2 (en) * 2006-03-01 2011-02-15 Eastman Chemical Company Process to produce a post catalyst removal composition
CN101636374A (zh) * 2006-12-21 2010-01-27 纳幕尔杜邦公司 用于制备卤代芳香二酸的方法
US8455680B2 (en) 2008-01-15 2013-06-04 Eastman Chemical Company Carboxylic acid production process employing solvent from esterification of lignocellulosic material
US8614350B2 (en) 2008-01-15 2013-12-24 Eastman Chemical Company Carboxylic acid production process employing solvent from esterification of lignocellulosic material
RU2014131232A (ru) * 2011-12-29 2016-02-20 Юоп Ллк Способ получения терефталевой кислоты
US8927764B2 (en) 2011-12-29 2015-01-06 Uop Llc Process for producing terephthalic acid
US9085522B2 (en) 2011-12-29 2015-07-21 Uop Llc Process for producing terephthalic acid
US9024059B2 (en) 2011-12-29 2015-05-05 Uop Llc Process for producing terephthalic acid
US9045408B2 (en) 2011-12-29 2015-06-02 Uop Llc Process for oxidizing alkyl-aromatic compounds
US9156765B2 (en) 2011-12-29 2015-10-13 Uop Llc Process for oxidizing alkyl-aromatic compounds
US9212121B2 (en) 2013-09-24 2015-12-15 Eastman Chemical Company Processes for producing terephthalic acid
US9199906B2 (en) 2013-09-24 2015-12-01 Eastman Chemical Company Processes for producing isophthalic acid
CN105688988B (zh) 2014-12-16 2018-11-27 财团法人工业技术研究院 糠醛化合物的氧化反应催化剂及糠醛化合物的氧化方法
CN107954850A (zh) * 2017-11-02 2018-04-24 华东理工大学 间苯二甲酸的制备方法
CN107963964A (zh) * 2017-11-02 2018-04-27 华东理工大学 间苯二甲酸的制备方法

Citations (6)

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Publication number Priority date Publication date Assignee Title
DE1922775A1 (de) * 1968-05-09 1969-11-13 Atlantic Richfield Co Verfahren zur Herstellung von aromatischen Dicarbonsaeuren
US3683017A (en) * 1970-04-01 1972-08-08 Fmc Corp Oxidation of p-xylene and p-tolujc acid to terephthalic acid
DE2362295A1 (de) * 1972-12-14 1974-06-20 Halcon International Inc Verfahren zur herstellung von isooder terephthalsaeure
DE2703161A1 (de) * 1976-01-29 1977-08-11 Mitsubishi Chem Ind Verfahren zur herstellung von hochgradig reiner terephthalsaeure
US4772748A (en) * 1982-12-10 1988-09-20 Mitsubishi Chemical Industries Limited Process for producing highly pure terephthalic acid
US4877900A (en) * 1987-04-24 1989-10-31 Mitsubishi Chemical Industries Limited Process for preparing terephthalic acid of high quality

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US3595908A (en) * 1966-11-01 1971-07-27 Inst Francais Du Petrole Two-step oxidation of paraxylene for the production of terephthalic acid
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JPS5518698B1 (enExample) * 1971-04-03 1980-05-21
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JPS59104345A (ja) * 1982-12-03 1984-06-16 Kuraray Yuka Kk 直接重合用に適したテレフタル酸の製造方法
JPS60233032A (ja) * 1984-05-04 1985-11-19 Kuraray Yuka Kk 直接重合用に適したテレフタル酸の製造法
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JPH0662495B2 (ja) * 1986-05-16 1994-08-17 三菱化成株式会社 高純度テレフタル酸の製法
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Patent Citations (6)

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Publication number Priority date Publication date Assignee Title
DE1922775A1 (de) * 1968-05-09 1969-11-13 Atlantic Richfield Co Verfahren zur Herstellung von aromatischen Dicarbonsaeuren
US3683017A (en) * 1970-04-01 1972-08-08 Fmc Corp Oxidation of p-xylene and p-tolujc acid to terephthalic acid
DE2362295A1 (de) * 1972-12-14 1974-06-20 Halcon International Inc Verfahren zur herstellung von isooder terephthalsaeure
DE2703161A1 (de) * 1976-01-29 1977-08-11 Mitsubishi Chem Ind Verfahren zur herstellung von hochgradig reiner terephthalsaeure
US4772748A (en) * 1982-12-10 1988-09-20 Mitsubishi Chemical Industries Limited Process for producing highly pure terephthalic acid
US4877900A (en) * 1987-04-24 1989-10-31 Mitsubishi Chemical Industries Limited Process for preparing terephthalic acid of high quality

Also Published As

Publication number Publication date
ES2081265B1 (es) 1996-10-16
BG62324B1 (bg) 1999-08-31
TW307753B (enExample) 1997-06-11
BG98919A (bg) 1995-05-31
JPH08506571A (ja) 1996-07-16
BR9305996A (pt) 1997-10-21
SK280582B6 (sk) 2000-04-10
IT1271011B (it) 1997-05-26
SK87794A3 (en) 1995-05-10
KR950008467A (ko) 1995-04-17
CN1050118C (zh) 2000-03-08
US5359133A (en) 1994-10-25
PL308537A1 (en) 1995-08-21
RO113850B1 (ro) 1998-11-30
GB9415915D0 (en) 1995-05-24
KR970000136B1 (ko) 1997-01-04
CA2128719C (en) 1998-06-09
ITMI941879A1 (it) 1996-03-14
MY108978A (en) 1996-11-30
ITMI941879A0 (it) 1994-09-14
ES2081265A1 (es) 1996-02-16
GB2286588B (en) 1996-09-11
SA94140587B1 (ar) 2006-11-12
DE4397599T1 (de) 1997-07-24
JP3009223B2 (ja) 2000-02-14
FR2710638A1 (fr) 1995-04-07
BE1008546A4 (nl) 1996-06-04
PL175685B1 (pl) 1999-01-29
AU5576394A (en) 1995-04-18
CN1103860A (zh) 1995-06-21
CA2128719A1 (en) 1995-03-29
GB2286588A (en) 1995-08-23
WO1995009143A1 (en) 1995-04-06
FR2710638B1 (fr) 1996-04-26

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