DE3605634A1 - Verfahren zur behandlung kristalliner sprengstoffe fuer hochleistungssprengladungen - Google Patents
Verfahren zur behandlung kristalliner sprengstoffe fuer hochleistungssprengladungenInfo
- Publication number
- DE3605634A1 DE3605634A1 DE19863605634 DE3605634A DE3605634A1 DE 3605634 A1 DE3605634 A1 DE 3605634A1 DE 19863605634 DE19863605634 DE 19863605634 DE 3605634 A DE3605634 A DE 3605634A DE 3605634 A1 DE3605634 A1 DE 3605634A1
- Authority
- DE
- Germany
- Prior art keywords
- explosive
- solvent
- explosives
- octogen
- treated
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000002360 explosive Substances 0.000 title claims abstract description 51
- 238000000034 method Methods 0.000 title claims description 21
- 239000002904 solvent Substances 0.000 claims abstract description 22
- 239000002245 particle Substances 0.000 claims abstract description 19
- UZGLIIJVICEWHF-UHFFFAOYSA-N octogen Chemical compound [O-][N+](=O)N1CN([N+]([O-])=O)CN([N+]([O-])=O)CN([N+]([O-])=O)C1 UZGLIIJVICEWHF-UHFFFAOYSA-N 0.000 claims description 27
- 239000000028 HMX Substances 0.000 claims description 26
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 22
- 239000000203 mixture Substances 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 claims description 8
- XTFIVUDBNACUBN-UHFFFAOYSA-N 1,3,5-trinitro-1,3,5-triazinane Chemical compound [O-][N+](=O)N1CN([N+]([O-])=O)CN([N+]([O-])=O)C1 XTFIVUDBNACUBN-UHFFFAOYSA-N 0.000 claims description 5
- TZRXHJWUDPFEEY-UHFFFAOYSA-N Pentaerythritol Tetranitrate Chemical compound [O-][N+](=O)OCC(CO[N+]([O-])=O)(CO[N+]([O-])=O)CO[N+]([O-])=O TZRXHJWUDPFEEY-UHFFFAOYSA-N 0.000 claims 1
- 238000009835 boiling Methods 0.000 claims 1
- 238000005266 casting Methods 0.000 description 4
- 238000001878 scanning electron micrograph Methods 0.000 description 4
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 3
- 239000011230 binding agent Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- SPSSULHKWOKEEL-UHFFFAOYSA-N 2,4,6-trinitrotoluene Chemical compound CC1=C([N+]([O-])=O)C=C([N+]([O-])=O)C=C1[N+]([O-])=O SPSSULHKWOKEEL-UHFFFAOYSA-N 0.000 description 2
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 description 2
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 2
- 239000000539 dimer Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 239000000015 trinitrotoluene Substances 0.000 description 2
- 238000004438 BET method Methods 0.000 description 1
- 239000000020 Nitrocellulose Substances 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 230000002902 bimodal effect Effects 0.000 description 1
- 238000009750 centrifugal casting Methods 0.000 description 1
- 239000000084 colloidal system Substances 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000012067 mathematical method Methods 0.000 description 1
- 229920001220 nitrocellulos Polymers 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000002798 polar solvent Substances 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 239000003380 propellant Substances 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000012798 spherical particle Substances 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
- 239000003799 water insoluble solvent Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B21/00—Apparatus or methods for working-up explosives, e.g. forming, cutting, drying
- C06B21/0033—Shaping the mixture
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19863605634 DE3605634A1 (de) | 1986-02-21 | 1986-02-21 | Verfahren zur behandlung kristalliner sprengstoffe fuer hochleistungssprengladungen |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19863605634 DE3605634A1 (de) | 1986-02-21 | 1986-02-21 | Verfahren zur behandlung kristalliner sprengstoffe fuer hochleistungssprengladungen |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE3605634A1 true DE3605634A1 (de) | 1987-08-27 |
| DE3605634C2 DE3605634C2 (enExample) | 1990-09-13 |
Family
ID=6294651
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19863605634 Granted DE3605634A1 (de) | 1986-02-21 | 1986-02-21 | Verfahren zur behandlung kristalliner sprengstoffe fuer hochleistungssprengladungen |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE3605634A1 (enExample) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4336049C1 (de) * | 1993-10-22 | 1995-03-09 | Fraunhofer Ges Forschung | Verfahren zur Herstellung von sphärolithischem Nitroguanidin |
| FR2886641A1 (fr) * | 2005-06-02 | 2006-12-08 | Saint Louis Inst | Particules d'explosif peu sensibles aux chocs et procede de traitement associe |
| FR2887544A1 (fr) * | 2005-06-02 | 2006-12-29 | Saint Louis Inst | Particules d'explosif peu sensibles aux chocs et procede de traitement associe |
| GB2426755B (en) * | 2005-06-02 | 2009-07-22 | Saint Louis Inst | Crystalline explosive form and preparation process thereof |
| FR2954308A1 (fr) * | 2009-12-23 | 2011-06-24 | Nexter Munitions | Composition explosive fusible/coulable et a vulnerabilite reduite |
| WO2012136933A1 (fr) * | 2011-04-08 | 2012-10-11 | Sme | Procede d'obtention d'une charge de cristaux d'hexanitrohexaazaisowurtzitane a morphologie arrondie; charge et materiau energetique correspondant. |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1067719B (de) * | 1958-04-30 | 1959-10-22 | Olin Mathieson | Verfahren zur Herstellung von Globularpulver auf der Basis von gelatinierbaren Polynitrostoffen |
| US4065529A (en) * | 1975-01-13 | 1977-12-27 | The United States Of America As Represented By The Secretary Of The Army | Process for spheroidization of RDX crystals |
| GB2156805A (en) * | 1984-04-04 | 1985-10-16 | Bofors Ab | Recrystallisation of the high explosives hmx and rdx |
-
1986
- 1986-02-21 DE DE19863605634 patent/DE3605634A1/de active Granted
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1067719B (de) * | 1958-04-30 | 1959-10-22 | Olin Mathieson | Verfahren zur Herstellung von Globularpulver auf der Basis von gelatinierbaren Polynitrostoffen |
| US4065529A (en) * | 1975-01-13 | 1977-12-27 | The United States Of America As Represented By The Secretary Of The Army | Process for spheroidization of RDX crystals |
| GB2156805A (en) * | 1984-04-04 | 1985-10-16 | Bofors Ab | Recrystallisation of the high explosives hmx and rdx |
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4336049C1 (de) * | 1993-10-22 | 1995-03-09 | Fraunhofer Ges Forschung | Verfahren zur Herstellung von sphärolithischem Nitroguanidin |
| FR2886641A1 (fr) * | 2005-06-02 | 2006-12-08 | Saint Louis Inst | Particules d'explosif peu sensibles aux chocs et procede de traitement associe |
| FR2887544A1 (fr) * | 2005-06-02 | 2006-12-29 | Saint Louis Inst | Particules d'explosif peu sensibles aux chocs et procede de traitement associe |
| GB2426755B (en) * | 2005-06-02 | 2009-07-22 | Saint Louis Inst | Crystalline explosive form and preparation process thereof |
| US8747581B2 (en) | 2005-06-02 | 2014-06-10 | Institut Franco-Allemand De Recherches De Saint-Louis | Particles of an explosive of low sensitivity to shock and associated treatment process |
| DE102006025187B4 (de) * | 2005-06-02 | 2017-04-06 | Deutsch Französisches Forschungsinstitut Saint Louis | Verfahren zur Herstellung von wenig stoßempfindlichen Sprengstoffpartikeln |
| FR2954308A1 (fr) * | 2009-12-23 | 2011-06-24 | Nexter Munitions | Composition explosive fusible/coulable et a vulnerabilite reduite |
| WO2011086246A1 (fr) * | 2009-12-23 | 2011-07-21 | Nexter Munitions | Composition explosive fusible/coulable et a vulnerabilite reduite |
| US9242906B2 (en) | 2009-12-23 | 2016-01-26 | Nexter Munitions | Melt-cast insensitive explosive composition |
| WO2012136933A1 (fr) * | 2011-04-08 | 2012-10-11 | Sme | Procede d'obtention d'une charge de cristaux d'hexanitrohexaazaisowurtzitane a morphologie arrondie; charge et materiau energetique correspondant. |
| FR2973799A1 (fr) * | 2011-04-08 | 2012-10-12 | Sme | Procede d'obtention d'une charge de cristaux d'hexanitrohexaazaisowurtzitane a morphologie arrondie ; charge et materiau energetique correspondant |
| US9353456B2 (en) | 2011-04-08 | 2016-05-31 | Herakles | Process for obtaining a charge of hexanitrohexaazaisowurtzitane crystals having a rounded morphology; charge and corresponding energetic material |
Also Published As
| Publication number | Publication date |
|---|---|
| DE3605634C2 (enExample) | 1990-09-13 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OP8 | Request for examination as to paragraph 44 patent law | ||
| D2 | Grant after examination | ||
| 8363 | Opposition against the patent | ||
| 8368 | Opposition refused due to inadmissibility | ||
| 8327 | Change in the person/name/address of the patent owner |
Owner name: DEUTSCHE AEROSPACE AG, 8000 MUENCHEN, DE |
|
| 8320 | Willingness to grant licences declared (paragraph 23) | ||
| 8327 | Change in the person/name/address of the patent owner |
Owner name: DAIMLER-BENZ AEROSPACE AKTIENGESELLSCHAFT, 80804 M |
|
| 8327 | Change in the person/name/address of the patent owner |
Owner name: DAIMLERCHRYSLER AEROSPACE AKTIENGESELLSCHAFT, 8099 |
|
| 8327 | Change in the person/name/address of the patent owner |
Owner name: DAIMLERCHRYSLER AEROSPACE AG, 85521 OTTOBRUNN, DE |
|
| 8327 | Change in the person/name/address of the patent owner |
Owner name: TDW GESELLSCHAFT FUER VERTEIDIGUNGSTECHNISCHE WIRKS |
|
| 8339 | Ceased/non-payment of the annual fee |