DE2924072C2 - - Google Patents

Info

Publication number
DE2924072C2
DE2924072C2 DE2924072A DE2924072A DE2924072C2 DE 2924072 C2 DE2924072 C2 DE 2924072C2 DE 2924072 A DE2924072 A DE 2924072A DE 2924072 A DE2924072 A DE 2924072A DE 2924072 C2 DE2924072 C2 DE 2924072C2
Authority
DE
Germany
Prior art keywords
titanium
compound
temperature
aerosol
liquid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE2924072A
Other languages
German (de)
English (en)
Other versions
DE2924072A1 (de
Inventor
Egon Potsdam N.Y. Us Matijevic
Mario Alessandria It Visca
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Montedison SpA
Original Assignee
Montedison SpA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Montedison SpA filed Critical Montedison SpA
Publication of DE2924072A1 publication Critical patent/DE2924072A1/de
Application granted granted Critical
Publication of DE2924072C2 publication Critical patent/DE2924072C2/de
Granted legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/04—Oxides; Hydroxides
    • C01G23/047—Titanium dioxide
    • C01G23/053—Producing by wet processes, e.g. hydrolysing titanium salts
    • C01G23/0536—Producing by wet processes, e.g. hydrolysing titanium salts by hydrolysing chloride-containing salts
    • C01G23/0538—Producing by wet processes, e.g. hydrolysing titanium salts by hydrolysing chloride-containing salts in the presence of seeds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/04—Oxides; Hydroxides
    • C01G23/047—Titanium dioxide
    • C01G23/053—Producing by wet processes, e.g. hydrolysing titanium salts
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/04—Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/30—Particle morphology extending in three dimensions
    • C01P2004/32—Spheres
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/51—Particles with a specific particle size distribution
    • C01P2004/52—Particles with a specific particle size distribution highly monodisperse size distribution
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Geology (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Environmental & Geological Engineering (AREA)
  • Nanotechnology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Composite Materials (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Materials Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
DE19792924072 1978-06-19 1979-06-15 Verfahren zur herstellung von titandioxid und nach diesem verfahren hergestelltes titandioxid Granted DE2924072A1 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US05/916,883 US4241042A (en) 1978-06-19 1978-06-19 Spherical titanium dioxide particles and process of manufacture

Publications (2)

Publication Number Publication Date
DE2924072A1 DE2924072A1 (de) 1979-12-20
DE2924072C2 true DE2924072C2 (enExample) 1990-10-04

Family

ID=25437991

Family Applications (1)

Application Number Title Priority Date Filing Date
DE19792924072 Granted DE2924072A1 (de) 1978-06-19 1979-06-15 Verfahren zur herstellung von titandioxid und nach diesem verfahren hergestelltes titandioxid

Country Status (6)

Country Link
US (1) US4241042A (enExample)
JP (2) JPS5523090A (enExample)
DE (1) DE2924072A1 (enExample)
FR (1) FR2429184A1 (enExample)
GB (2) GB2023115B (enExample)
IT (1) IT1165096B (enExample)

Families Citing this family (44)

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EP0107700B1 (en) * 1982-05-03 1991-08-14 Western Electric Company, Incorporated Method for fabricating ceramic materials
IT1161200B (it) * 1983-02-25 1987-03-18 Montedison Spa Processo e apparecchio per la preparazione di particelle di ossidi metallici monodisperse, sferiche, non aggregate e di dimensione inferiore al micron
DE3417438A1 (de) * 1984-05-11 1985-11-14 Licentia Patent-Verwaltungs-Gmbh, 6000 Frankfurt Verfahren und vorrichtung zur herstellung eines aerosolstromes
GB2166126B (en) * 1984-10-25 1989-08-23 Mitsubishi Mining & Cement Co Production of ceramic powder
JPS61168528A (ja) * 1985-01-23 1986-07-30 Shokubai Kasei Kogyo Kk 酸化チタンからなる真球状微粒子粉末
IT1183382B (it) * 1985-02-20 1987-10-22 Montedison Spa Partecelle sferiche a distribuzione granulometrica ristretta di biossi do di titanio ricoperto da uno strato uniforme di ossidi di ferro e processo per la loro preparazione
EP0214308B1 (en) * 1985-03-05 1993-07-28 Idemitsu Kosan Company Limited Method for preparing super-fine spherical particles of metal oxide
US4755369A (en) * 1985-05-22 1988-07-05 Research Development Corporation Of Japan Production of ultrafine particles
JPS61275108A (ja) * 1985-05-30 1986-12-05 Mitsubishi Mining & Cement Co Ltd 誘電体粉末の製造方法
US4678657A (en) * 1985-06-10 1987-07-07 Aluminum Company Of America Production of high purity substantially spherical metal hydroxide/oxide particles from the hydrolysis of a metal alkoxide aerosol using metal hydroxide/oxide seed nuclei
US4724134A (en) * 1985-06-10 1988-02-09 Aluminum Company Of America Production of tailor-made particle size distributions of substantially spherical metal hydroxide/oxide particles comprising single or multiple hydroxides by hydrolysis of one or more metal alkoxide aerosols
JPH0648388B2 (ja) * 1985-07-31 1994-06-22 出光興産株式会社 乾式現像剤
GB8527716D0 (en) * 1985-11-09 1985-12-11 Tioxide Group Plc Finely divided oxide
IT1197814B (it) * 1986-09-16 1988-12-06 Montedison Spa Processo per la preparazione di biossido di titanio sotto forma di particelle sferiche per idrolisi di ti (iv)
US4917830A (en) * 1988-09-19 1990-04-17 The United States Of America As Represented By The United States Department Of Energy Monodisperse aerosol generator
DE3840196C1 (enExample) * 1988-11-29 1990-04-12 Bayer Ag, 5090 Leverkusen, De
DE4206913A1 (de) * 1992-03-05 1993-09-09 Kronos Titan Gmbh Katalysator fuer die carbonylsulfid-hydrolyse
TW288044B (enExample) * 1993-05-12 1996-10-11 Sumitomo Chemical Co
US5508015A (en) * 1994-07-15 1996-04-16 E. I. Du Pont De Nemours And Company Process for controlling agglomeration in the manufacture of TiO2
US5626786A (en) * 1995-04-17 1997-05-06 Huntington; John H. Labile bromine fire suppressants
US5656175A (en) * 1995-07-05 1997-08-12 Cytec Technology Corp. Recovery of metal oxides from a slurry
US6338809B1 (en) 1997-02-24 2002-01-15 Superior Micropowders Llc Aerosol method and apparatus, particulate products, and electronic devices made therefrom
US5871872A (en) * 1997-05-30 1999-02-16 Shipley Company, Ll.C. Dye incorporated pigments and products made from same
US5885343A (en) * 1997-05-30 1999-03-23 Shipley Company, L.L.C. Dyed silica pigments and products made from same
US6387531B1 (en) 1998-07-27 2002-05-14 Nanogram Corporation Metal (silicon) oxide/carbon composite particles
US6099798A (en) * 1997-10-31 2000-08-08 Nanogram Corp. Ultraviolet light block and photocatalytic materials
US7384680B2 (en) * 1997-07-21 2008-06-10 Nanogram Corporation Nanoparticle-based power coatings and corresponding structures
US6106798A (en) * 1997-07-21 2000-08-22 Nanogram Corporation Vanadium oxide nanoparticles
JP4184487B2 (ja) * 1997-08-15 2008-11-19 昭和電工株式会社 二酸化チタン微粒子の製造方法
US6683023B2 (en) * 2000-04-21 2004-01-27 Showa Denko K.K. Photocatalytic powder and polymer composition
JP2003252627A (ja) * 2002-02-27 2003-09-10 Toshiba Corp 微粒子の製造方法および微粒子製造装置
AU2003297639A1 (en) * 2002-12-02 2004-06-23 University Of Florida Treatments for benign tumors, cancers, neoplasias, and/or other inflammatory disorders or diseases
CN100532274C (zh) * 2003-12-31 2009-08-26 科学与工业研究委员会 超细金红石型二氧化钛颗粒的低温合成
US7413726B2 (en) * 2004-03-26 2008-08-19 Council Of Scientific And Industrial Research Synthesis of ultrafine rutile phase titanium dioxide particles
EP1807352A1 (en) * 2004-11-11 2007-07-18 Basell Poliolefine Italia S.r.l. Preparation of tio2 powders from a waste liquid containing titanium compounds
JP2008519750A (ja) * 2004-11-11 2008-06-12 バーゼル・ポリオレフィン・イタリア・ソチエタ・ア・レスポンサビリタ・リミタータ チタン化合物を含有する廃液からＴｉＯ２粉末の製造
KR101502161B1 (ko) * 2005-01-12 2015-03-12 이클립스 에어로스페이스, 인크. 화재 진압 시스템
KR100800129B1 (ko) 2006-06-28 2008-01-31 카운슬 오브 사이언티픽 앤드 인더스트리얼 리서치 저온에서 극미세 루타일 상 이산화티타늄 입자의 합성 방법
US7803711B2 (en) * 2007-09-18 2010-09-28 Cabot Microelectronics Corporation Low pH barrier slurry based on titanium dioxide
US20090298617A1 (en) * 2008-05-28 2009-12-03 Bridgestone Sports Co., Ltd. Golf ball material and golf ball
DE102009009780A1 (de) * 2009-02-20 2010-08-26 Kronos International, Inc. Mehrstufiges Verfahren zur Herstellung von Titandioxid
TWI615446B (zh) * 2017-04-21 2018-02-21 國立清華大學 阻隔紅外線的材料與使用所述材料的塗料
CN111362287B (zh) * 2020-03-20 2022-04-01 辽宁瑞鸥新材料科技有限公司 用于制备镁合金半固态浆料的MgOHCl气溶胶及其用法
CN117303439A (zh) * 2023-09-21 2023-12-29 宜宾天原海丰和泰有限公司 一种利用氯化法钛白粉副产盐酸制备纳米二氧化钛的方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1842620A (en) * 1928-03-19 1932-01-26 Minerals Increment Company Method of manufacturing titanic hydroxide
US1819184A (en) * 1928-05-12 1931-08-18 Benjamin G Macintire Process for generating smoke clouds
US1931380A (en) * 1931-09-03 1933-10-17 Krebs Pigment And Color Corp Production of titanium dioxide from titanium tetrachloride
NL83582C (enExample) 1952-11-01
US2998391A (en) * 1957-05-24 1961-08-29 Aeroprojects Inc Aerosolization unit
US3062621A (en) * 1960-07-07 1962-11-06 American Cyanamid Co Titanium dioxide pigment and compositions containing the same
GB1047714A (en) * 1962-07-17 1966-11-09 Thann Fab Prod Chem Apparatus useful inter alia for the production of finely divided metal oxides
US3406012A (en) * 1965-06-16 1968-10-15 Pittsburgh Plate Glass Co Process for classifying pigmentary metal oxide
US3663283A (en) * 1969-10-02 1972-05-16 Richard A Hebert Process and apparatus for the production of finely-divided metal oxides
BE792503A (fr) * 1971-12-10 1973-06-08 Montedison Spa Procede de preparation d'un bioxyde de titane d'une taille de particules controlee

Also Published As

Publication number Publication date
GB2070579A (en) 1981-09-09
FR2429184A1 (fr) 1980-01-18
JPS623772B2 (enExample) 1987-01-27
GB2023115B (en) 1982-12-22
JPH0130767B2 (enExample) 1989-06-21
DE2924072A1 (de) 1979-12-20
JPS5523090A (en) 1980-02-19
FR2429184B1 (enExample) 1984-11-30
IT1165096B (it) 1987-04-22
IT7923623A0 (it) 1979-06-15
GB2070579B (en) 1983-01-19
GB2023115A (en) 1979-12-28
JPS62171922A (ja) 1987-07-28
US4241042A (en) 1980-12-23

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Legal Events

Date Code Title Description
8110 Request for examination paragraph 44
D2 Grant after examination
8364 No opposition during term of opposition
8339 Ceased/non-payment of the annual fee