DE2714749A1 - Verfahren zum wiedergewinnen von zink aus rueckstandsloesungen - Google Patents
Verfahren zum wiedergewinnen von zink aus rueckstandsloesungenInfo
- Publication number
- DE2714749A1 DE2714749A1 DE19772714749 DE2714749A DE2714749A1 DE 2714749 A1 DE2714749 A1 DE 2714749A1 DE 19772714749 DE19772714749 DE 19772714749 DE 2714749 A DE2714749 A DE 2714749A DE 2714749 A1 DE2714749 A1 DE 2714749A1
- Authority
- DE
- Germany
- Prior art keywords
- zinc
- solution
- anion
- sulfuric acid
- exchanger
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 239000011701 zinc Substances 0.000 title claims description 48
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 title claims description 46
- 229910052725 zinc Inorganic materials 0.000 title claims description 45
- 238000000034 method Methods 0.000 title claims description 28
- 239000000243 solution Substances 0.000 claims description 56
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 42
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 18
- 150000001450 anions Chemical class 0.000 claims description 13
- 239000007788 liquid Substances 0.000 claims description 9
- 239000011780 sodium chloride Substances 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 238000000502 dialysis Methods 0.000 claims description 8
- 150000001768 cations Chemical class 0.000 claims description 7
- 230000000717 retained effect Effects 0.000 claims description 6
- 239000002253 acid Substances 0.000 claims description 5
- 150000004820 halides Chemical class 0.000 claims description 5
- 229920003002 synthetic resin Polymers 0.000 claims description 5
- 239000000057 synthetic resin Substances 0.000 claims description 5
- 230000009918 complex formation Effects 0.000 claims description 4
- 229910052751 metal Inorganic materials 0.000 claims description 4
- 239000002184 metal Substances 0.000 claims description 4
- 150000003751 zinc Chemical class 0.000 claims description 4
- 239000003513 alkali Substances 0.000 claims description 2
- 239000012266 salt solution Substances 0.000 claims description 2
- -1 zinc halide Chemical class 0.000 claims description 2
- PTFCDOFLOPIGGS-UHFFFAOYSA-N Zinc dication Chemical compound [Zn+2] PTFCDOFLOPIGGS-UHFFFAOYSA-N 0.000 claims 1
- 229940006486 zinc cation Drugs 0.000 claims 1
- 239000011777 magnesium Substances 0.000 description 13
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 9
- 229910052749 magnesium Inorganic materials 0.000 description 9
- 229920005989 resin Polymers 0.000 description 7
- 239000011347 resin Substances 0.000 description 7
- 238000005868 electrolysis reaction Methods 0.000 description 6
- 239000012535 impurity Substances 0.000 description 6
- 238000006386 neutralization reaction Methods 0.000 description 5
- 238000011084 recovery Methods 0.000 description 5
- 239000012528 membrane Substances 0.000 description 4
- 239000002351 wastewater Substances 0.000 description 4
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 3
- 235000011941 Tilia x europaea Nutrition 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 230000008021 deposition Effects 0.000 description 3
- 239000004571 lime Substances 0.000 description 3
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 description 3
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 2
- 229920002125 Sokalan® Polymers 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 2
- 125000000129 anionic group Chemical group 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 241001233037 catfish Species 0.000 description 2
- 238000005342 ion exchange Methods 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 229910052717 sulfur Inorganic materials 0.000 description 2
- 229960001763 zinc sulfate Drugs 0.000 description 2
- 229910000368 zinc sulfate Inorganic materials 0.000 description 2
- 101100127285 Drosophila melanogaster unc-104 gene Proteins 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 239000003929 acidic solution Substances 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 229920001429 chelating resin Polymers 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000008139 complexing agent Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 239000008151 electrolyte solution Substances 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 159000000003 magnesium salts Chemical class 0.000 description 1
- 229910052943 magnesium sulfate Inorganic materials 0.000 description 1
- 235000019341 magnesium sulphate Nutrition 0.000 description 1
- 229910052748 manganese Inorganic materials 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 229920001467 poly(styrenesulfonates) Polymers 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 229910052711 selenium Inorganic materials 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- WQSRXNAKUYIVET-UHFFFAOYSA-N sulfuric acid;zinc Chemical compound [Zn].OS(O)(=O)=O WQSRXNAKUYIVET-UHFFFAOYSA-N 0.000 description 1
- 229910021653 sulphate ion Inorganic materials 0.000 description 1
- 235000009529 zinc sulphate Nutrition 0.000 description 1
- 239000011686 zinc sulphate Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G9/00—Compounds of zinc
- C01G9/06—Sulfates
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J41/00—Anion exchange; Use of material as anion exchangers; Treatment of material for improving the anion exchange properties
- B01J41/04—Processes using organic exchangers
- B01J41/07—Processes using organic exchangers in the weakly basic form
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G9/00—Compounds of zinc
- C01G9/003—Preparation involving a liquid-liquid extraction, an adsorption or an ion-exchange
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G9/00—Compounds of zinc
- C01G9/006—Compounds containing zinc, with or without oxygen or hydrogen, and containing two or more other elements
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G9/00—Compounds of zinc
- C01G9/04—Halides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrolytic Production Of Metals (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Treatment Of Water By Ion Exchange (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7609587A FR2346457A1 (fr) | 1976-04-02 | 1976-04-02 | Recuperation du zinc des solutions residuelles de l'electrodeposition |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2714749A1 true DE2714749A1 (de) | 1977-10-06 |
Family
ID=9171297
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19772714749 Withdrawn DE2714749A1 (de) | 1976-04-02 | 1977-04-01 | Verfahren zum wiedergewinnen von zink aus rueckstandsloesungen |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US4108744A (enExample) |
| JP (1) | JPS52138015A (enExample) |
| BE (1) | BE853150A (enExample) |
| CA (1) | CA1075636A (enExample) |
| DE (1) | DE2714749A1 (enExample) |
| FR (1) | FR2346457A1 (enExample) |
| GB (1) | GB1553641A (enExample) |
| IN (1) | IN147278B (enExample) |
| IT (1) | IT1075369B (enExample) |
| NL (1) | NL7703614A (enExample) |
| NO (1) | NO149068C (enExample) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1981000728A1 (en) * | 1979-09-13 | 1981-03-19 | L Rennerfelt | Purification process for spent pickling baths |
| DE102008056776A1 (de) * | 2008-11-11 | 2010-05-12 | Enthone Inc., West Haven | Galvanisches Bad und Verfahren zur Abscheidung von zinkhaltigen Schichten |
| RU2468545C1 (ru) * | 2011-10-12 | 2012-11-27 | Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Национальный исследовательский Томский политехнический университет" | Источник тормозного излучения |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2544750B1 (fr) * | 1983-04-25 | 1988-09-16 | Minemet Rech Sa | Procede de traitement d'une solution de purge notamment destinee a un procede d'extraction de zinc par voie electrolytique |
| JPS60243236A (ja) * | 1984-05-16 | 1985-12-03 | Mitsui Mining & Smelting Co Ltd | 亜鉛製錬におけるマグネシウム除去方法 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3537845A (en) * | 1967-04-24 | 1970-11-03 | Dow Chemical Co | Separation and recovery of cobalt and zinc |
| US3488185A (en) * | 1967-06-02 | 1970-01-06 | Nalco Chemical Co | Separation and recovery of zinc from solutions containing zinc ions and other metal ions |
| US3488184A (en) * | 1968-02-19 | 1970-01-06 | Nalco Chemical Co | Separation and recovery of cobalt from waste streams containing cobalt and zinc |
| US3929598A (en) * | 1972-08-14 | 1975-12-30 | Anaconda Co | Recovery of copper and zinc from low-grade non-ferrous materials |
-
1976
- 1976-04-02 FR FR7609587A patent/FR2346457A1/fr active Granted
-
1977
- 1977-03-30 GB GB13408/77A patent/GB1553641A/en not_active Expired
- 1977-03-31 IT IT21866/77A patent/IT1075369B/it active
- 1977-04-01 CA CA275,350A patent/CA1075636A/fr not_active Expired
- 1977-04-01 US US05/783,699 patent/US4108744A/en not_active Expired - Lifetime
- 1977-04-01 NO NO771157A patent/NO149068C/no unknown
- 1977-04-01 DE DE19772714749 patent/DE2714749A1/de not_active Withdrawn
- 1977-04-01 BE BE176341A patent/BE853150A/xx not_active IP Right Cessation
- 1977-04-01 NL NL7703614A patent/NL7703614A/xx not_active Application Discontinuation
- 1977-04-02 JP JP3697877A patent/JPS52138015A/ja active Pending
- 1977-04-13 IN IN569/CAL/77A patent/IN147278B/en unknown
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1981000728A1 (en) * | 1979-09-13 | 1981-03-19 | L Rennerfelt | Purification process for spent pickling baths |
| DE102008056776A1 (de) * | 2008-11-11 | 2010-05-12 | Enthone Inc., West Haven | Galvanisches Bad und Verfahren zur Abscheidung von zinkhaltigen Schichten |
| RU2468545C1 (ru) * | 2011-10-12 | 2012-11-27 | Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Национальный исследовательский Томский политехнический университет" | Источник тормозного излучения |
Also Published As
| Publication number | Publication date |
|---|---|
| FR2346457B1 (enExample) | 1978-08-25 |
| IN147278B (enExample) | 1980-01-12 |
| FR2346457A1 (fr) | 1977-10-28 |
| NO771157L (no) | 1977-10-04 |
| NO149068B (no) | 1983-10-31 |
| NL7703614A (nl) | 1977-10-04 |
| JPS52138015A (en) | 1977-11-17 |
| BE853150A (fr) | 1977-08-01 |
| NO149068C (no) | 1984-02-08 |
| GB1553641A (en) | 1979-09-26 |
| US4108744A (en) | 1978-08-22 |
| IT1075369B (it) | 1985-04-22 |
| CA1075636A (fr) | 1980-04-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8141 | Disposal/no request for examination |