DE2647950A1 - Verfahren zur herstellung eines alpha-primaerphasen-vanadinbronze-traegerkatalysators - Google Patents
Verfahren zur herstellung eines alpha-primaerphasen-vanadinbronze-traegerkatalysatorsInfo
- Publication number
- DE2647950A1 DE2647950A1 DE19762647950 DE2647950A DE2647950A1 DE 2647950 A1 DE2647950 A1 DE 2647950A1 DE 19762647950 DE19762647950 DE 19762647950 DE 2647950 A DE2647950 A DE 2647950A DE 2647950 A1 DE2647950 A1 DE 2647950A1
- Authority
- DE
- Germany
- Prior art keywords
- primary phase
- catalyst
- mixture
- bronze
- vanadine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 239000003054 catalyst Substances 0.000 title claims description 27
- 238000004519 manufacturing process Methods 0.000 title claims description 7
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 14
- 239000000203 mixture Substances 0.000 claims description 14
- 238000000034 method Methods 0.000 claims description 13
- 229910052720 vanadium Inorganic materials 0.000 claims description 9
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 claims description 8
- 229910000906 Bronze Inorganic materials 0.000 claims description 7
- 239000010974 bronze Substances 0.000 claims description 7
- KUNSUQLRTQLHQQ-UHFFFAOYSA-N copper tin Chemical compound [Cu].[Sn] KUNSUQLRTQLHQQ-UHFFFAOYSA-N 0.000 claims description 7
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 4
- 239000007787 solid Substances 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 3
- 239000011261 inert gas Substances 0.000 claims description 3
- 229910021529 ammonia Inorganic materials 0.000 claims description 2
- 238000002156 mixing Methods 0.000 claims description 2
- 230000003647 oxidation Effects 0.000 claims description 2
- 238000007254 oxidation reaction Methods 0.000 claims description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 10
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 6
- 238000002441 X-ray diffraction Methods 0.000 description 5
- 229910052757 nitrogen Inorganic materials 0.000 description 5
- 239000011734 sodium Substances 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
- 150000001339 alkali metal compounds Chemical class 0.000 description 3
- 229910052708 sodium Inorganic materials 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 2
- URLKBWYHVLBVBO-UHFFFAOYSA-N Para-Xylene Chemical group CC1=CC=C(C)C=C1 URLKBWYHVLBVBO-UHFFFAOYSA-N 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 244000309464 bull Species 0.000 description 2
- 238000001354 calcination Methods 0.000 description 2
- 239000000470 constituent Substances 0.000 description 2
- GNTDGMZSJNCJKK-UHFFFAOYSA-N divanadium pentaoxide Chemical compound O=[V](=O)O[V](=O)=O GNTDGMZSJNCJKK-UHFFFAOYSA-N 0.000 description 2
- 229910052744 lithium Inorganic materials 0.000 description 2
- -1 m- and p-xylene Chemical class 0.000 description 2
- IVSZLXZYQVIEFR-UHFFFAOYSA-N m-xylene Chemical compound CC1=CC=CC(C)=C1 IVSZLXZYQVIEFR-UHFFFAOYSA-N 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 241000158147 Sator Species 0.000 description 1
- LXASOGUHMSNFCR-UHFFFAOYSA-D [V+5].[V+5].[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O Chemical compound [V+5].[V+5].[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O LXASOGUHMSNFCR-UHFFFAOYSA-D 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 229910000272 alkali metal oxide Inorganic materials 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000002547 anomalous effect Effects 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 150000001491 aromatic compounds Chemical class 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000011365 complex material Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 229910052593 corundum Inorganic materials 0.000 description 1
- 239000010431 corundum Substances 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000000976 ink Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 150000004706 metal oxides Chemical class 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000008188 pellet Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 150000003388 sodium compounds Chemical class 0.000 description 1
- CMZUMMUJMWNLFH-UHFFFAOYSA-N sodium metavanadate Chemical compound [Na+].[O-][V](=O)=O CMZUMMUJMWNLFH-UHFFFAOYSA-N 0.000 description 1
- 229910052721 tungsten Inorganic materials 0.000 description 1
- 239000010937 tungsten Substances 0.000 description 1
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 1
- 229910000166 zirconium phosphate Inorganic materials 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
- B01J23/20—Vanadium, niobium or tantalum
- B01J23/22—Vanadium
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US05/624,699 US3990997A (en) | 1975-10-22 | 1975-10-22 | Method of preparing ammoxidation catalyst |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2647950A1 true DE2647950A1 (de) | 1977-05-05 |
Family
ID=24502987
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19762647950 Withdrawn DE2647950A1 (de) | 1975-10-22 | 1976-10-22 | Verfahren zur herstellung eines alpha-primaerphasen-vanadinbronze-traegerkatalysators |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US3990997A (enExample) |
| JP (1) | JPS605338B2 (enExample) |
| BE (1) | BE847493A (enExample) |
| CA (1) | CA1078807A (enExample) |
| DE (1) | DE2647950A1 (enExample) |
| FR (1) | FR2328511A1 (enExample) |
| GB (1) | GB1569142A (enExample) |
| IL (1) | IL50740A (enExample) |
| IT (1) | IT1077075B (enExample) |
| NL (1) | NL7611663A (enExample) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5354038A (en) * | 1989-09-29 | 1994-10-11 | Consolidated Engineering Company, Inc. | Heat treatment of metal castings and in-furnace sand reclamation |
| JPH04297684A (ja) * | 1991-03-27 | 1992-10-21 | Mitsui Mining & Smelting Co Ltd | ケーブル結合機構 |
| WO2011097461A1 (en) * | 2010-02-05 | 2011-08-11 | The Board Of Regents For Oklahoma State University | Colorimetric reagent for prevention of peroxide formation in solvents |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2247452A1 (en) * | 1973-10-10 | 1975-05-09 | Sun Ventures Inc | Ammonoxidation of aromatic hydrocarbons pref. xylenes to nitriles - using vanadium "bronze" catalyst on alpha alumina support |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3803205A (en) * | 1972-05-15 | 1974-04-09 | Sun Research Development | Production of aromatic nitriles by ammoxidation |
| US3839398A (en) * | 1972-11-29 | 1974-10-01 | Sun Research Development | Ammoxidation process |
-
1975
- 1975-10-22 US US05/624,699 patent/US3990997A/en not_active Expired - Lifetime
-
1976
- 1976-10-21 NL NL7611663A patent/NL7611663A/xx not_active Application Discontinuation
- 1976-10-21 JP JP51125561A patent/JPS605338B2/ja not_active Expired
- 1976-10-21 BE BE171675A patent/BE847493A/xx not_active IP Right Cessation
- 1976-10-21 CA CA263,847A patent/CA1078807A/en not_active Expired
- 1976-10-21 IL IL50740A patent/IL50740A/xx unknown
- 1976-10-21 IT IT28584/76A patent/IT1077075B/it active
- 1976-10-22 DE DE19762647950 patent/DE2647950A1/de not_active Withdrawn
- 1976-10-22 GB GB43929/76A patent/GB1569142A/en not_active Expired
- 1976-10-22 FR FR7631859A patent/FR2328511A1/fr active Granted
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2247452A1 (en) * | 1973-10-10 | 1975-05-09 | Sun Ventures Inc | Ammonoxidation of aromatic hydrocarbons pref. xylenes to nitriles - using vanadium "bronze" catalyst on alpha alumina support |
Also Published As
| Publication number | Publication date |
|---|---|
| CA1078807A (en) | 1980-06-03 |
| IL50740A0 (en) | 1976-12-31 |
| FR2328511A1 (fr) | 1977-05-20 |
| IL50740A (en) | 1979-11-30 |
| NL7611663A (nl) | 1977-04-26 |
| US3990997A (en) | 1976-11-09 |
| IT1077075B (it) | 1985-04-27 |
| FR2328511B1 (enExample) | 1980-03-28 |
| BE847493A (fr) | 1977-04-21 |
| JPS605338B2 (ja) | 1985-02-09 |
| JPS5274590A (en) | 1977-06-22 |
| GB1569142A (en) | 1980-06-11 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8128 | New person/name/address of the agent |
Representative=s name: STREHL, P., DIPL.-ING. DIPL.-WIRTSCH.-ING. SCHUEBE |
|
| 8110 | Request for examination paragraph 44 | ||
| 8130 | Withdrawal |