DE2155927A1 - Verfahren zur Herstellung von Alkydharz en - Google Patents
Verfahren zur Herstellung von Alkydharz enInfo
- Publication number
- DE2155927A1 DE2155927A1 DE19712155927 DE2155927A DE2155927A1 DE 2155927 A1 DE2155927 A1 DE 2155927A1 DE 19712155927 DE19712155927 DE 19712155927 DE 2155927 A DE2155927 A DE 2155927A DE 2155927 A1 DE2155927 A1 DE 2155927A1
- Authority
- DE
- Germany
- Prior art keywords
- stage
- mol
- alkyd resin
- amount
- anhydride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 229920000180 alkyd Polymers 0.000 title claims description 46
- 238000000034 method Methods 0.000 title claims description 20
- 238000004519 manufacturing process Methods 0.000 title claims description 5
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 28
- 239000000203 mixture Substances 0.000 claims description 13
- 235000011187 glycerol Nutrition 0.000 claims description 12
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 12
- 229920005862 polyol Polymers 0.000 claims description 12
- 150000003077 polyols Chemical class 0.000 claims description 12
- LGRFSURHDFAFJT-UHFFFAOYSA-N Phthalic anhydride Natural products C1=CC=C2C(=O)OC(=O)C2=C1 LGRFSURHDFAFJT-UHFFFAOYSA-N 0.000 claims description 11
- JHIWVOJDXOSYLW-UHFFFAOYSA-N butyl 2,2-difluorocyclopropane-1-carboxylate Chemical compound CCCCOC(=O)C1CC1(F)F JHIWVOJDXOSYLW-UHFFFAOYSA-N 0.000 claims description 11
- 239000003999 initiator Substances 0.000 claims description 11
- 150000008064 anhydrides Chemical class 0.000 claims description 10
- 150000002148 esters Chemical class 0.000 claims description 9
- 239000004593 Epoxy Substances 0.000 claims description 8
- -1 carboxy compound Chemical class 0.000 claims description 6
- 125000004432 carbon atom Chemical group C* 0.000 claims description 4
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 claims description 4
- 230000001588 bifunctional effect Effects 0.000 claims description 3
- 229910052799 carbon Inorganic materials 0.000 claims description 3
- 125000005907 alkyl ester group Chemical group 0.000 claims description 2
- 150000002762 monocarboxylic acid derivatives Chemical class 0.000 claims description 2
- 150000008065 acid anhydrides Chemical class 0.000 claims 3
- 210000003298 dental enamel Anatomy 0.000 claims 1
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 18
- 239000008096 xylene Substances 0.000 description 18
- 239000002253 acid Substances 0.000 description 16
- 239000011541 reaction mixture Substances 0.000 description 15
- 238000000576 coating method Methods 0.000 description 9
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 8
- 238000006243 chemical reaction Methods 0.000 description 8
- 239000012299 nitrogen atmosphere Substances 0.000 description 8
- 238000003756 stirring Methods 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 6
- 238000010533 azeotropic distillation Methods 0.000 description 6
- 229940072282 cardura Drugs 0.000 description 5
- 239000011248 coating agent Substances 0.000 description 5
- RUZYUOTYCVRMRZ-UHFFFAOYSA-N doxazosin Chemical compound C1OC2=CC=CC=C2OC1C(=O)N(CC1)CCN1C1=NC(N)=C(C=C(C(OC)=C2)OC)C2=N1 RUZYUOTYCVRMRZ-UHFFFAOYSA-N 0.000 description 5
- 229920005989 resin Polymers 0.000 description 5
- 239000011347 resin Substances 0.000 description 5
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 4
- 229910000831 Steel Inorganic materials 0.000 description 4
- 235000011037 adipic acid Nutrition 0.000 description 4
- 239000001361 adipic acid Substances 0.000 description 4
- 239000003960 organic solvent Substances 0.000 description 4
- 239000010959 steel Substances 0.000 description 4
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
- 125000002843 carboxylic acid group Chemical group 0.000 description 3
- 239000008199 coating composition Substances 0.000 description 3
- WERYXYBDKMZEQL-UHFFFAOYSA-N butane-1,4-diol Chemical compound OCCCCO WERYXYBDKMZEQL-UHFFFAOYSA-N 0.000 description 2
- 239000004359 castor oil Substances 0.000 description 2
- 235000019438 castor oil Nutrition 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 235000014113 dietary fatty acids Nutrition 0.000 description 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 2
- 229930195729 fatty acid Natural products 0.000 description 2
- 239000000194 fatty acid Substances 0.000 description 2
- 150000004665 fatty acids Chemical class 0.000 description 2
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 2
- QQVIHTHCMHWDBS-UHFFFAOYSA-N isophthalic acid Chemical compound OC(=O)C1=CC=CC(C(O)=O)=C1 QQVIHTHCMHWDBS-UHFFFAOYSA-N 0.000 description 2
- BDJRBEYXGGNYIS-UHFFFAOYSA-N nonanedioic acid Chemical compound OC(=O)CCCCCCCC(O)=O BDJRBEYXGGNYIS-UHFFFAOYSA-N 0.000 description 2
- 239000003208 petroleum Substances 0.000 description 2
- XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical compound OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 description 2
- YPFDHNVEDLHUCE-UHFFFAOYSA-N propane-1,3-diol Chemical compound OCCCO YPFDHNVEDLHUCE-UHFFFAOYSA-N 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- SFRDXVJWXWOTEW-UHFFFAOYSA-N 2-(hydroxymethyl)propane-1,3-diol Chemical compound OCC(CO)CO SFRDXVJWXWOTEW-UHFFFAOYSA-N 0.000 description 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
- 229920000877 Melamine resin Polymers 0.000 description 1
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 235000019486 Sunflower oil Nutrition 0.000 description 1
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 1
- 229920001807 Urea-formaldehyde Polymers 0.000 description 1
- 230000001464 adherent effect Effects 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 150000001735 carboxylic acids Chemical class 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000003240 coconut oil Substances 0.000 description 1
- 235000019864 coconut oil Nutrition 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- IFDVQVHZEKPUSC-UHFFFAOYSA-N cyclohex-3-ene-1,2-dicarboxylic acid Chemical compound OC(=O)C1CCC=CC1C(O)=O IFDVQVHZEKPUSC-UHFFFAOYSA-N 0.000 description 1
- QSAWQNUELGIYBC-UHFFFAOYSA-N cyclohexane-1,2-dicarboxylic acid Chemical compound OC(=O)C1CCCCC1C(O)=O QSAWQNUELGIYBC-UHFFFAOYSA-N 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000032050 esterification Effects 0.000 description 1
- 238000005886 esterification reaction Methods 0.000 description 1
- 235000013312 flour Nutrition 0.000 description 1
- 125000003055 glycidyl group Chemical group C(C1CO1)* 0.000 description 1
- 239000000944 linseed oil Substances 0.000 description 1
- 235000021388 linseed oil Nutrition 0.000 description 1
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 description 1
- 239000011976 maleic acid Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000002763 monocarboxylic acids Chemical class 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 description 1
- ODGAOXROABLFNM-UHFFFAOYSA-N polynoxylin Chemical compound O=C.NC(N)=O ODGAOXROABLFNM-UHFFFAOYSA-N 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000005201 scrubbing Methods 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- 239000002600 sunflower oil Substances 0.000 description 1
- UFDHBDMSHIXOKF-UHFFFAOYSA-N tetrahydrophthalic acid Natural products OC(=O)C1=C(C(O)=O)CCCC1 UFDHBDMSHIXOKF-UHFFFAOYSA-N 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
- QXJQHYBHAIHNGG-UHFFFAOYSA-N trimethylolethane Chemical compound OCC(C)(CO)CO QXJQHYBHAIHNGG-UHFFFAOYSA-N 0.000 description 1
- 239000012463 white pigment Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/02—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
- C08G63/12—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from polycarboxylic acids and polyhydroxy compounds
- C08G63/40—Polyesters derived from ester-forming derivatives of polycarboxylic acids or of polyhydroxy compounds, other than from esters thereof
- C08G63/42—Cyclic ethers; Cyclic carbonates; Cyclic sulfites; Cyclic orthoesters
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D167/00—Coating compositions based on polyesters obtained by reactions forming a carboxylic ester link in the main chain; Coating compositions based on derivatives of such polymers
- C09D167/08—Polyesters modified with higher fatty oils or their acids, or with natural resins or resin acids
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Wood Science & Technology (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Polyesters Or Polycarbonates (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Paints Or Removers (AREA)
- Epoxy Resins (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB5384470 | 1970-11-12 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2155927A1 true DE2155927A1 (de) | 1972-05-18 |
Family
ID=10469160
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19712155927 Withdrawn DE2155927A1 (de) | 1970-11-12 | 1971-11-10 | Verfahren zur Herstellung von Alkydharz en |
Country Status (9)
| Country | Link |
|---|---|
| JP (1) | JPS5512452B1 (enExample) |
| BE (1) | BE774805A (enExample) |
| CA (1) | CA941093A (enExample) |
| DE (1) | DE2155927A1 (enExample) |
| FR (1) | FR2113900B1 (enExample) |
| GB (1) | GB1317969A (enExample) |
| IT (1) | IT940520B (enExample) |
| NL (1) | NL166039C (enExample) |
| SE (1) | SE369913B (enExample) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2507985C2 (de) * | 1975-02-25 | 1982-05-06 | Deutsche Texaco Ag, 2000 Hamburg | Verfahren zur Herstellung von niedrigviskosen, fettsäuremodifizierten Polyestern für lösungsmittelarme Einbrennlacksysteme |
| US4314918A (en) | 1980-06-26 | 1982-02-09 | Ppg Industries, Inc. | Coating compositions containing organic alcoholic reactive diluents |
| US4403093A (en) | 1982-09-28 | 1983-09-06 | Ppg Industries, Inc. | Polyesters |
-
1970
- 1970-11-12 GB GB1317969D patent/GB1317969A/en not_active Expired
-
1971
- 1971-11-03 BE BE774805A patent/BE774805A/nl not_active IP Right Cessation
- 1971-11-10 NL NL7115422A patent/NL166039C/xx not_active IP Right Cessation
- 1971-11-10 CA CA127,388A patent/CA941093A/en not_active Expired
- 1971-11-10 DE DE19712155927 patent/DE2155927A1/de not_active Withdrawn
- 1971-11-10 JP JP8915471A patent/JPS5512452B1/ja active Pending
- 1971-11-10 FR FR7140333A patent/FR2113900B1/fr not_active Expired
- 1971-11-10 SE SE1438871A patent/SE369913B/xx unknown
- 1971-11-10 IT IT3093871A patent/IT940520B/it active
Also Published As
| Publication number | Publication date |
|---|---|
| NL166039B (nl) | 1981-01-15 |
| FR2113900B1 (enExample) | 1974-09-06 |
| IT940520B (it) | 1973-02-20 |
| SE369913B (enExample) | 1974-09-23 |
| NL166039C (nl) | 1981-06-15 |
| NL7115422A (enExample) | 1972-05-16 |
| JPS5512452B1 (enExample) | 1980-04-02 |
| GB1317969A (en) | 1973-05-23 |
| CA941093A (en) | 1974-01-29 |
| FR2113900A1 (enExample) | 1972-06-30 |
| BE774805A (nl) | 1972-05-03 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE2637167C2 (enExample) | ||
| DE2656462A1 (de) | Pigmente enthaltende beschichtungskomposition mit einem hohen feststoffgehalt | |
| DE2629930A1 (de) | Verfahren zur herstellung von polyestern und deren verwendung in ueberzugsmassen | |
| DE1520732C3 (de) | Verfahren zur Herstellung von Alkydharze« | |
| EP0032554B1 (de) | Bindemittelkombinationen für korrosionsfeste Lacke | |
| DE2933480A1 (de) | Modifiziertes alkydharz und seine verwendung zum ueberziehen von draht | |
| DE2436371A1 (de) | Verfahren zur herstellung von niedrigviskosen polyester-lackharzen | |
| DE2936686C2 (de) | Verfahren zur Herstellung von nach Neutralisation mit Basen wasserlöslichen Lackbindemitteln | |
| DE2506113C2 (de) | Wässriger Isolierlack | |
| DE3246618A1 (de) | Alkydharze, enthaltend ringoeffnungsprodukte epoxidierter fettalkohole oder fettsaeurederivate als hydroxylverbindungen | |
| DE2155927A1 (de) | Verfahren zur Herstellung von Alkydharz en | |
| DE4222012A1 (de) | Waessrige fuellerzusammensetzung | |
| DE2225646B2 (de) | Wasserverdünnbare Einbrennlacke | |
| DE1669132A1 (de) | Waessrige Lacke | |
| DE2525066A1 (de) | Warmhaertende beschichtungszusammensetzung mit hohem feststoffgehalt | |
| DE2138193A1 (de) | Schellackersatzmittel und Verfahren zur Herstellung eines Schellackersatzmittels | |
| DE1745052A1 (de) | Verfahren zur Herstellung von Kondensationsprodukten | |
| DE1570461C3 (de) | Verfahren zur Herstellung von mit Wasser verdünnbaren Bindemitteln | |
| EP0547502A1 (de) | Härtbares Bindemittel und Verfahren zu dessen Herstellung | |
| EP0008419B1 (de) | Verfahren zur Herstellung von Alkydharzen, die Epsilon-Caprolactamreste enthalten; die erhaltenen Harze und ihre Verwendung als wasserverdünnbare Bindemittel für Malerlacke | |
| DE2809840C3 (de) | Wasserdispergierbares epoxymodifiziertes Alkydharz und dessen Verwendung | |
| DE1520771C3 (de) | Verfahren zur Herstellung von Alkydharzen. Ausscheidung aus: 1520745 | |
| DE2204844C2 (de) | Verfahren zur Herstellung von Phosphor in chemischer Bindung enthaltenden Polykondensaten | |
| DE2314376A1 (de) | Haertbares wasserloesliches polyesteramid und verfahren zu dessen herstellung | |
| DE2119161C3 (de) | Verfahren zur Herstellung von Alkyd harzen und deren Verwendung |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OD | Request for examination | ||
| 8130 | Withdrawal |