DE208637C - - Google Patents
Info
- Publication number
- DE208637C DE208637C DENDAT208637D DE208637DA DE208637C DE 208637 C DE208637 C DE 208637C DE NDAT208637 D DENDAT208637 D DE NDAT208637D DE 208637D A DE208637D A DE 208637DA DE 208637 C DE208637 C DE 208637C
- Authority
- DE
- Germany
- Prior art keywords
- acid
- esters
- santalol
- oil
- neutral
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000002253 acid Substances 0.000 claims description 15
- 239000001306 (7E,9E,11E,13E)-pentadeca-7,9,11,13-tetraen-1-ol Substances 0.000 claims description 9
- 150000002148 esters Chemical class 0.000 claims description 9
- 230000001264 neutralization Effects 0.000 claims description 9
- 150000007513 acids Chemical class 0.000 claims description 4
- 235000005985 organic acids Nutrition 0.000 claims description 4
- 230000002378 acidificating Effects 0.000 claims description 3
- 150000008050 dialkyl sulfates Chemical class 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 3
- 150000007524 organic acids Chemical class 0.000 claims description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 27
- 239000000243 solution Substances 0.000 description 14
- RTZKZFJDLAIYFH-UHFFFAOYSA-N diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 8
- 230000005484 gravity Effects 0.000 description 6
- JZMJDSHXVKJFKW-UHFFFAOYSA-M methyl sulfate(1-) Chemical compound COS([O-])(=O)=O JZMJDSHXVKJFKW-UHFFFAOYSA-M 0.000 description 4
- BVKZGUZCCUSVTD-UHFFFAOYSA-N Carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 3
- 125000000217 alkyl group Chemical group 0.000 description 3
- 238000009835 boiling Methods 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- -1 esters Organic acids Chemical class 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- 239000000344 soap Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 229960000846 Camphor Drugs 0.000 description 2
- 241000723346 Cinnamomum camphora Species 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N HCl Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- JDRMYOQETPMYQX-UHFFFAOYSA-N Succinic acid methyl ester Natural products COC(=O)CCC(O)=O JDRMYOQETPMYQX-UHFFFAOYSA-N 0.000 description 2
- RINCXYDBBGOEEQ-UHFFFAOYSA-N Succinic anhydride Chemical compound O=C1CCC(=O)O1 RINCXYDBBGOEEQ-UHFFFAOYSA-N 0.000 description 2
- 230000001476 alcoholic Effects 0.000 description 2
- UHOVQNZJYSORNB-UHFFFAOYSA-N benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 2
- 229930007890 camphor Natural products 0.000 description 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 229940014800 succinic anhydride Drugs 0.000 description 2
- 150000003459 sulfonic acid esters Chemical class 0.000 description 2
- CNHMFZIFLREWPF-HQJQHLMTSA-N (1S,3R)-3-methoxycarbonyl-2,2,3-trimethylcyclopentane-1-carboxylic acid Chemical compound COC(=O)[C@]1(C)CC[C@H](C(O)=O)C1(C)C CNHMFZIFLREWPF-HQJQHLMTSA-N 0.000 description 1
- XCCFSZODNJHPEF-UHFFFAOYSA-N 2-carboxybenzoate;hydron;potassium Chemical compound [K].OC(=O)C1=CC=CC=C1C(O)=O XCCFSZODNJHPEF-UHFFFAOYSA-N 0.000 description 1
- VFZDNKRDYPTSTP-UHFFFAOYSA-N 5,8,8-trimethyl-3-oxabicyclo[3.2.1]octane-2,4-dione Chemical compound O=C1OC(=O)C2(C)CCC1C2(C)C VFZDNKRDYPTSTP-UHFFFAOYSA-N 0.000 description 1
- DSSYKIVIOFKYAU-UHFFFAOYSA-N Camphor Chemical compound C1CC2(C)C(=O)CC1C2(C)C DSSYKIVIOFKYAU-UHFFFAOYSA-N 0.000 description 1
- RIFGWPKJUGCATF-UHFFFAOYSA-N Ethyl chloroformate Chemical compound CCOC(Cl)=O RIFGWPKJUGCATF-UHFFFAOYSA-N 0.000 description 1
- 210000002784 Stomach Anatomy 0.000 description 1
- 125000003158 alcohol group Chemical group 0.000 description 1
- 125000005907 alkyl ester group Chemical group 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005886 esterification reaction Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000005457 ice water Substances 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 150000004702 methyl esters Chemical class 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L na2so4 Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- 210000000056 organs Anatomy 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 230000003595 spectral Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000001225 therapeutic Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
- C07C69/013—Esters of alcohols having the esterified hydroxy group bound to a carbon atom of a ring other than a six-membered aromatic ring
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE208637C true DE208637C (fr) |
Family
ID=470658
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT208637D Active DE208637C (fr) |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE208637C (fr) |
-
0
- DE DENDAT208637D patent/DE208637C/de active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE2544595A1 (de) | Verfahren zur gewinnung von monocarbonsaeureestern und dicarbonsaeuren oder deren estern aus den abfallsalzloesungen der cyclohexanonherstellung | |
| DE1951299A1 (de) | Veresterungs- und Extraktionsverfahren | |
| DE208637C (fr) | ||
| DE1142858B (de) | Verfahren zur Gewinnung von Diphenylpolycarbonsaeuremethylestern | |
| DE902496C (de) | Verfahren zur Gewinnung von hoehermolekularen organischen Hydroxylverbindungen aus solche enthaltenden Gemischen | |
| DE325639C (de) | Verfahren zur Gewinnung von Estern aus rohem Holzessig | |
| DE964594C (de) | Verfahren zur Herstellung von y-Dihydrojonon | |
| DE360274C (de) | Verfahren zur Raffination von Mineraloelen | |
| DE414190C (de) | Verfahren zur Darstellung von Zitronensaeuretribenzylester | |
| DE529947C (de) | Verfahren zur Darstellung von inaktivem Menthol | |
| DE838642C (de) | Verfahren zur Gewinnung von Sterinen aus Fettsaeuren, Fetten, OElen und Fettgemischen | |
| DE870100C (de) | Verfahren zur Aufarbeitung von Sulfatseifen unter Gewinnung von Sterinen | |
| DE610502C (de) | Verfahren zur Darstellung von C, C-disubstituierten Abkoemmlingen der Barbitursaeure | |
| DE591105C (de) | Verfahren zur Raffination von Mineraloelen und fetten OElen | |
| DE148207C (fr) | ||
| AT144513B (de) | Verfahren zur Abscheidung des Follikelhormons aus Harn schwangerer Individuen. | |
| DE630393C (de) | Verfahren zur Darstellung von Acylderivaten der Octahydrofollikelhormone | |
| DE871751C (de) | Verfahren zur Gewinnung des Pentaerythrit-dichlorhydrinmonoschwefligsaeureesters | |
| DE1002339C2 (de) | Verfahren zur Aufarbeitung des bei der Oxydation von technischem trans-Dekahydronaphthalin gebildeten Reaktionsgemisches | |
| DE875515C (de) | Verfahren zur Aufarbeitung von Fettpechen und Sterinkonzentraten unter Gewinnung vonSterinen | |
| DE674517C (de) | Verfahren zur Darstellung von Ketonen | |
| DE746578C (de) | Verfahren zur Herstellung von basischen 1, 3-Dialkoxypropanlen | |
| DE701956C (de) | Verfahren zur Gewinnung hormonartig wirkender Stoffe | |
| DE587450C (de) | Verfahren zur Gewinnung wertvoller Produkte aus Montanwachs | |
| DE681730C (de) | Verfahren zur Herstellung von vitamin-A-haltigen Extrakten aus Fischoelen, insbesondere Fischleberoelen |