DE19621818A1 - Kurzzeit-Heißverdichtung anodisierter Metalloberflächen mit tensidhaltigen Lösungen - Google Patents
Kurzzeit-Heißverdichtung anodisierter Metalloberflächen mit tensidhaltigen LösungenInfo
- Publication number
- DE19621818A1 DE19621818A1 DE19621818A DE19621818A DE19621818A1 DE 19621818 A1 DE19621818 A1 DE 19621818A1 DE 19621818 A DE19621818 A DE 19621818A DE 19621818 A DE19621818 A DE 19621818A DE 19621818 A1 DE19621818 A1 DE 19621818A1
- Authority
- DE
- Germany
- Prior art keywords
- acid
- acids
- aqueous solution
- group
- total
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 229910052751 metal Inorganic materials 0.000 title claims abstract description 22
- 239000002184 metal Substances 0.000 title claims abstract description 22
- 239000004094 surface-active agent Substances 0.000 title claims abstract description 4
- 238000007906 compression Methods 0.000 title description 32
- 230000006835 compression Effects 0.000 title description 25
- 238000000034 method Methods 0.000 claims abstract description 35
- 239000002253 acid Substances 0.000 claims abstract description 28
- 239000007864 aqueous solution Substances 0.000 claims abstract description 18
- 150000007513 acids Chemical class 0.000 claims abstract description 16
- 150000001340 alkali metals Chemical class 0.000 claims abstract description 12
- 150000003009 phosphonic acids Chemical class 0.000 claims abstract description 11
- 239000002736 nonionic surfactant Substances 0.000 claims abstract description 10
- 150000007524 organic acids Chemical class 0.000 claims abstract description 9
- 235000005985 organic acids Nutrition 0.000 claims abstract description 8
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 claims abstract description 7
- 239000003945 anionic surfactant Substances 0.000 claims abstract description 6
- -1 alkaline-earth metal cations Chemical class 0.000 claims abstract description 5
- 238000009835 boiling Methods 0.000 claims abstract description 5
- 239000003093 cationic surfactant Substances 0.000 claims abstract description 5
- 125000004122 cyclic group Chemical group 0.000 claims abstract description 5
- 125000000129 anionic group Chemical group 0.000 claims abstract description 3
- 125000002091 cationic group Chemical group 0.000 claims abstract description 3
- 238000007743 anodising Methods 0.000 claims description 24
- 239000000243 solution Substances 0.000 claims description 24
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 17
- 229910001413 alkali metal ion Inorganic materials 0.000 claims description 11
- 229910001420 alkaline earth metal ion Inorganic materials 0.000 claims description 11
- 238000011282 treatment Methods 0.000 claims description 11
- 239000012141 concentrate Substances 0.000 claims description 7
- 150000001412 amines Chemical class 0.000 claims description 6
- 150000001735 carboxylic acids Chemical class 0.000 claims description 6
- WLWKIJKUDWYINL-UHFFFAOYSA-N cyclohexane-1,1,2,2,3,3-hexacarboxylic acid Chemical compound OC(=O)C1(C(O)=O)CCCC(C(O)=O)(C(O)=O)C1(C(O)=O)C(O)=O WLWKIJKUDWYINL-UHFFFAOYSA-N 0.000 claims description 5
- 229910052744 lithium Inorganic materials 0.000 claims description 5
- 229910052749 magnesium Inorganic materials 0.000 claims description 5
- COKIOUWMXONTKQ-UHFFFAOYSA-N 1-phosphonopropane-1,2,3-tricarboxylic acid Chemical compound OC(=O)CC(C(O)=O)C(C(O)=O)P(O)(O)=O COKIOUWMXONTKQ-UHFFFAOYSA-N 0.000 claims description 4
- YDONNITUKPKTIG-UHFFFAOYSA-N [Nitrilotris(methylene)]trisphosphonic acid Chemical compound OP(O)(=O)CN(CP(O)(O)=O)CP(O)(O)=O YDONNITUKPKTIG-UHFFFAOYSA-N 0.000 claims description 4
- QMKYBPDZANOJGF-UHFFFAOYSA-N benzene-1,3,5-tricarboxylic acid Chemical compound OC(=O)C1=CC(C(O)=O)=CC(C(O)=O)=C1 QMKYBPDZANOJGF-UHFFFAOYSA-N 0.000 claims description 4
- 125000004432 carbon atom Chemical group C* 0.000 claims description 4
- YDSWCNNOKPMOTP-UHFFFAOYSA-N mellitic acid Chemical compound OC(=O)C1=C(C(O)=O)C(C(O)=O)=C(C(O)=O)C(C(O)=O)=C1C(O)=O YDSWCNNOKPMOTP-UHFFFAOYSA-N 0.000 claims description 4
- CYIDZMCFTVVTJO-UHFFFAOYSA-N pyromellitic acid Chemical compound OC(=O)C1=CC(C(O)=O)=C(C(O)=O)C=C1C(O)=O CYIDZMCFTVVTJO-UHFFFAOYSA-N 0.000 claims description 4
- ARCGXLSVLAOJQL-UHFFFAOYSA-N trimellitic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C(C(O)=O)=C1 ARCGXLSVLAOJQL-UHFFFAOYSA-N 0.000 claims description 4
- ZCOMURCDMLBWOR-UHFFFAOYSA-N (hydroxy-phenyl-phosphonomethyl)phosphonic acid Chemical compound OP(=O)(O)C(P(O)(O)=O)(O)C1=CC=CC=C1 ZCOMURCDMLBWOR-UHFFFAOYSA-N 0.000 claims description 3
- KMDMOMDSEVTJTI-UHFFFAOYSA-N 2-phosphonobutanedioic acid Chemical compound OC(=O)CC(C(O)=O)P(O)(O)=O KMDMOMDSEVTJTI-UHFFFAOYSA-N 0.000 claims description 3
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical group C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 claims description 3
- DBVJJBKOTRCVKF-UHFFFAOYSA-N Etidronic acid Chemical compound OP(=O)(O)C(O)(C)P(O)(O)=O DBVJJBKOTRCVKF-UHFFFAOYSA-N 0.000 claims description 3
- LDTZSTJLVYBEKB-UHFFFAOYSA-N butedronic acid Chemical compound OC(=O)CC(C(O)=O)C(P(O)(O)=O)P(O)(O)=O LDTZSTJLVYBEKB-UHFFFAOYSA-N 0.000 claims description 3
- GPCTYPSWRBUGFH-UHFFFAOYSA-N (1-amino-1-phosphonoethyl)phosphonic acid Chemical compound OP(=O)(O)C(N)(C)P(O)(O)=O GPCTYPSWRBUGFH-UHFFFAOYSA-N 0.000 claims description 2
- RUPZRJCPTQGQRU-UHFFFAOYSA-N (1-hydroxy-1-phosphonobutyl)phosphonic acid Chemical compound CCCC(O)(P(O)(O)=O)P(O)(O)=O RUPZRJCPTQGQRU-UHFFFAOYSA-N 0.000 claims description 2
- IDYCJOKDHJLCGO-UHFFFAOYSA-N (amino-phenyl-phosphonomethyl)phosphonic acid Chemical compound OP(=O)(O)C(P(O)(O)=O)(N)C1=CC=CC=C1 IDYCJOKDHJLCGO-UHFFFAOYSA-N 0.000 claims description 2
- GPXCJKUXBIGASD-UHFFFAOYSA-N 1-phosphonobutane-1,2,4-tricarboxylic acid Chemical compound OC(=O)CCC(C(O)=O)C(C(O)=O)P(O)(O)=O GPXCJKUXBIGASD-UHFFFAOYSA-N 0.000 claims description 2
- SCOXZKRXKMRCCY-UHFFFAOYSA-N [1-(dimethylamino)-1-phosphonoethyl]phosphonic acid Chemical compound CN(C)C(C)(P(O)(O)=O)P(O)(O)=O SCOXZKRXKMRCCY-UHFFFAOYSA-N 0.000 claims description 2
- 125000004836 hexamethylene group Chemical group [H]C([H])([*:2])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[*:1] 0.000 claims description 2
- DKPHLYCEFBDQKM-UHFFFAOYSA-H hexapotassium;1-phosphonato-n,n-bis(phosphonatomethyl)methanamine Chemical compound [K+].[K+].[K+].[K+].[K+].[K+].[O-]P([O-])(=O)CN(CP([O-])([O-])=O)CP([O-])([O-])=O DKPHLYCEFBDQKM-UHFFFAOYSA-H 0.000 claims description 2
- WXUAQHNMJWJLTG-UHFFFAOYSA-N monomethylpersuccinic acid Natural products OC(=O)C(C)CC(O)=O WXUAQHNMJWJLTG-UHFFFAOYSA-N 0.000 claims description 2
- 238000006386 neutralization reaction Methods 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 claims description 2
- 229920006395 saturated elastomer Polymers 0.000 claims description 2
- XHAZMZWXAOBLQG-UHFFFAOYSA-N (1-hydroxy-1-phosphonopropyl)phosphonic acid Chemical compound CCC(O)(P(O)(O)=O)P(O)(O)=O XHAZMZWXAOBLQG-UHFFFAOYSA-N 0.000 claims 1
- QJSFUOBKBXVTMN-UHFFFAOYSA-N C=C.P(O)(O)=O Chemical compound C=C.P(O)(O)=O QJSFUOBKBXVTMN-UHFFFAOYSA-N 0.000 claims 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims 1
- 239000005977 Ethylene Substances 0.000 claims 1
- SBRJRPNSSOSLRR-UHFFFAOYSA-N [1-phosphono-1-(propylamino)ethyl]phosphonic acid Chemical compound CCCNC(C)(P(O)(O)=O)P(O)(O)=O SBRJRPNSSOSLRR-UHFFFAOYSA-N 0.000 claims 1
- 238000010790 dilution Methods 0.000 claims 1
- 239000012895 dilution Substances 0.000 claims 1
- QHCCDDQKNUYGNC-UHFFFAOYSA-N n-ethylbutan-1-amine Chemical compound CCCCNCC QHCCDDQKNUYGNC-UHFFFAOYSA-N 0.000 claims 1
- 238000007789 sealing Methods 0.000 abstract description 10
- 229910001416 lithium ion Inorganic materials 0.000 abstract description 2
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 abstract 1
- 229910001425 magnesium ion Inorganic materials 0.000 abstract 1
- 239000010410 layer Substances 0.000 description 33
- 238000005056 compaction Methods 0.000 description 13
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 12
- 229910052782 aluminium Inorganic materials 0.000 description 11
- 238000012360 testing method Methods 0.000 description 11
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 8
- 239000003792 electrolyte Substances 0.000 description 7
- KBPLFHHGFOOTCA-UHFFFAOYSA-N 1-Octanol Chemical compound CCCCCCCCO KBPLFHHGFOOTCA-UHFFFAOYSA-N 0.000 description 6
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 6
- 239000000975 dye Substances 0.000 description 6
- 150000002739 metals Chemical class 0.000 description 6
- 239000000654 additive Substances 0.000 description 5
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 4
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 4
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 4
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 4
- 229910045601 alloy Inorganic materials 0.000 description 4
- 239000000956 alloy Substances 0.000 description 4
- 238000000576 coating method Methods 0.000 description 4
- 238000004040 coloring Methods 0.000 description 4
- 238000005260 corrosion Methods 0.000 description 4
- 239000008367 deionised water Substances 0.000 description 4
- 229910021641 deionized water Inorganic materials 0.000 description 4
- 239000011777 magnesium Substances 0.000 description 4
- 239000011148 porous material Substances 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 229910000838 Al alloy Inorganic materials 0.000 description 3
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 3
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 3
- 239000000853 adhesive Substances 0.000 description 3
- 239000010407 anodic oxide Substances 0.000 description 3
- 238000002048 anodisation reaction Methods 0.000 description 3
- 229910001424 calcium ion Inorganic materials 0.000 description 3
- KRVSOGSZCMJSLX-UHFFFAOYSA-L chromic acid Substances O[Cr](O)(=O)=O KRVSOGSZCMJSLX-UHFFFAOYSA-L 0.000 description 3
- 230000007797 corrosion Effects 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 150000002191 fatty alcohols Chemical class 0.000 description 3
- AWJWCTOOIBYHON-UHFFFAOYSA-N furo[3,4-b]pyrazine-5,7-dione Chemical compound C1=CN=C2C(=O)OC(=O)C2=N1 AWJWCTOOIBYHON-UHFFFAOYSA-N 0.000 description 3
- 239000000565 sealant Substances 0.000 description 3
- 238000010186 staining Methods 0.000 description 3
- 239000010936 titanium Substances 0.000 description 3
- 229910052719 titanium Inorganic materials 0.000 description 3
- HVBSAKJJOYLTQU-UHFFFAOYSA-N 4-aminobenzenesulfonic acid Chemical compound NC1=CC=C(S(O)(=O)=O)C=C1 HVBSAKJJOYLTQU-UHFFFAOYSA-N 0.000 description 2
- 235000013162 Cocos nucifera Nutrition 0.000 description 2
- 244000060011 Cocos nucifera Species 0.000 description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 2
- WGLPBDUCMAPZCE-UHFFFAOYSA-N Trioxochromium Chemical compound O=[Cr](=O)=O WGLPBDUCMAPZCE-UHFFFAOYSA-N 0.000 description 2
- 150000001242 acetic acid derivatives Chemical class 0.000 description 2
- 125000000217 alkyl group Chemical group 0.000 description 2
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 2
- 229910021529 ammonia Inorganic materials 0.000 description 2
- 125000003118 aryl group Chemical group 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 229920001577 copolymer Polymers 0.000 description 2
- MOTZDAYCYVMXPC-UHFFFAOYSA-N dodecyl hydrogen sulfate Chemical compound CCCCCCCCCCCCOS(O)(=O)=O MOTZDAYCYVMXPC-UHFFFAOYSA-N 0.000 description 2
- 229940043264 dodecyl sulfate Drugs 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 239000003925 fat Substances 0.000 description 2
- 150000002222 fluorine compounds Chemical class 0.000 description 2
- 239000003112 inhibitor Substances 0.000 description 2
- UEGPKNKPLBYCNK-UHFFFAOYSA-L magnesium acetate Chemical compound [Mg+2].CC([O-])=O.CC([O-])=O UEGPKNKPLBYCNK-UHFFFAOYSA-L 0.000 description 2
- 229940069446 magnesium acetate Drugs 0.000 description 2
- 235000011285 magnesium acetate Nutrition 0.000 description 2
- 239000011654 magnesium acetate Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 150000002815 nickel Chemical class 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 2
- DURPTKYDGMDSBL-UHFFFAOYSA-N 1-butoxybutane Chemical compound CCCCOCCCC DURPTKYDGMDSBL-UHFFFAOYSA-N 0.000 description 1
- GKQHIYSTBXDYNQ-UHFFFAOYSA-M 1-dodecylpyridin-1-ium;chloride Chemical compound [Cl-].CCCCCCCCCCCC[N+]1=CC=CC=C1 GKQHIYSTBXDYNQ-UHFFFAOYSA-M 0.000 description 1
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- SDGNNLQZAPXALR-UHFFFAOYSA-N 3-sulfophthalic acid Chemical compound OC(=O)C1=CC=CC(S(O)(=O)=O)=C1C(O)=O SDGNNLQZAPXALR-UHFFFAOYSA-N 0.000 description 1
- XLSZENRVQPEAHK-UHFFFAOYSA-N 4-amino-2,3-dimethylbenzoic acid Chemical class CC1=C(C)C(C(O)=O)=CC=C1N XLSZENRVQPEAHK-UHFFFAOYSA-N 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical class [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- USFZMSVCRYTOJT-UHFFFAOYSA-N Ammonium acetate Chemical compound N.CC(O)=O USFZMSVCRYTOJT-UHFFFAOYSA-N 0.000 description 1
- 239000005695 Ammonium acetate Substances 0.000 description 1
- JUXUSCGBXZCFPZ-UHFFFAOYSA-N CCCCCCO.OP(=O)OP(O)=O Chemical compound CCCCCCO.OP(=O)OP(O)=O JUXUSCGBXZCFPZ-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- 229940120146 EDTMP Drugs 0.000 description 1
- QUSNBJAOOMFDIB-UHFFFAOYSA-N Ethylamine Chemical compound CCN QUSNBJAOOMFDIB-UHFFFAOYSA-N 0.000 description 1
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 description 1
- DJEQZVQFEPKLOY-UHFFFAOYSA-N N,N-dimethylbutylamine Chemical compound CCCCN(C)C DJEQZVQFEPKLOY-UHFFFAOYSA-N 0.000 description 1
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 1
- AMQJEAYHLZJPGS-UHFFFAOYSA-N N-Pentanol Chemical compound CCCCCO AMQJEAYHLZJPGS-UHFFFAOYSA-N 0.000 description 1
- MXRIRQGCELJRSN-UHFFFAOYSA-N O.O.O.[Al] Chemical compound O.O.O.[Al] MXRIRQGCELJRSN-UHFFFAOYSA-N 0.000 description 1
- ABLZXFCXXLZCGV-UHFFFAOYSA-N Phosphorous acid Chemical compound OP(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 description 1
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical class C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 1
- YSMRWXYRXBRSND-UHFFFAOYSA-N TOTP Chemical compound CC1=CC=CC=C1OP(=O)(OC=1C(=CC=CC=1)C)OC1=CC=CC=C1C YSMRWXYRXBRSND-UHFFFAOYSA-N 0.000 description 1
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 1
- QLGZQPQQPUMNBD-UHFFFAOYSA-N [1-(butylamino)-1-phosphonoethyl]phosphonic acid Chemical compound CCCCNC(C)(P(O)(O)=O)P(O)(O)=O QLGZQPQQPUMNBD-UHFFFAOYSA-N 0.000 description 1
- USNWAMPROKAEIT-UHFFFAOYSA-N [Na].C(C=C)(=O)O Chemical compound [Na].C(C=C)(=O)O USNWAMPROKAEIT-UHFFFAOYSA-N 0.000 description 1
- AEDPOTDCAAOODK-UHFFFAOYSA-N [butylamino(phosphono)methyl]phosphonic acid Chemical compound CCCCNC(P(O)(O)=O)P(O)(O)=O AEDPOTDCAAOODK-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 150000003926 acrylamides Chemical class 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 238000007792 addition Methods 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 230000000274 adsorptive effect Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 150000001447 alkali salts Chemical class 0.000 description 1
- 150000008051 alkyl sulfates Chemical class 0.000 description 1
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical group [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 1
- 229940043376 ammonium acetate Drugs 0.000 description 1
- 235000019257 ammonium acetate Nutrition 0.000 description 1
- 150000003863 ammonium salts Chemical class 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- JBIROUFYLSSYDX-UHFFFAOYSA-M benzododecinium chloride Chemical compound [Cl-].CCCCCCCCCCCC[N+](C)(C)CC1=CC=CC=C1 JBIROUFYLSSYDX-UHFFFAOYSA-M 0.000 description 1
- WGQKYBSKWIADBV-UHFFFAOYSA-N benzylamine Chemical compound NCC1=CC=CC=C1 WGQKYBSKWIADBV-UHFFFAOYSA-N 0.000 description 1
- 230000000740 bleeding effect Effects 0.000 description 1
- ZCDOYSPFYFSLEW-UHFFFAOYSA-N chromate(2-) Chemical class [O-][Cr]([O-])(=O)=O ZCDOYSPFYFSLEW-UHFFFAOYSA-N 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 229940090960 diethylenetriamine pentamethylene phosphonic acid Drugs 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- DUYCTCQXNHFCSJ-UHFFFAOYSA-N dtpmp Chemical compound OP(=O)(O)CN(CP(O)(O)=O)CCN(CP(O)(=O)O)CCN(CP(O)(O)=O)CP(O)(O)=O DUYCTCQXNHFCSJ-UHFFFAOYSA-N 0.000 description 1
- NFDRPXJGHKJRLJ-UHFFFAOYSA-N edtmp Chemical compound OP(O)(=O)CN(CP(O)(O)=O)CCN(CP(O)(O)=O)CP(O)(O)=O NFDRPXJGHKJRLJ-UHFFFAOYSA-N 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 150000003893 lactate salts Chemical class 0.000 description 1
- XIXADJRWDQXREU-UHFFFAOYSA-M lithium acetate Chemical compound [Li+].CC([O-])=O XIXADJRWDQXREU-UHFFFAOYSA-M 0.000 description 1
- 229910003002 lithium salt Inorganic materials 0.000 description 1
- 159000000002 lithium salts Chemical class 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- DAZXVJBJRMWXJP-UHFFFAOYSA-N n,n-dimethylethylamine Chemical compound CCN(C)C DAZXVJBJRMWXJP-UHFFFAOYSA-N 0.000 description 1
- GNVRJGIVDSQCOP-UHFFFAOYSA-N n-ethyl-n-methylethanamine Chemical compound CCN(C)CC GNVRJGIVDSQCOP-UHFFFAOYSA-N 0.000 description 1
- XCVNDBIXFPGMIW-UHFFFAOYSA-N n-ethylpropan-1-amine Chemical compound CCCNCC XCVNDBIXFPGMIW-UHFFFAOYSA-N 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 150000002816 nickel compounds Chemical class 0.000 description 1
- DBJLJFTWODWSOF-UHFFFAOYSA-L nickel(ii) fluoride Chemical compound F[Ni]F DBJLJFTWODWSOF-UHFFFAOYSA-L 0.000 description 1
- 150000002823 nitrates Chemical class 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 150000003891 oxalate salts Chemical class 0.000 description 1
- 235000006408 oxalic acid Nutrition 0.000 description 1
- ACVYVLVWPXVTIT-UHFFFAOYSA-N phosphinic acid Chemical class O[PH2]=O ACVYVLVWPXVTIT-UHFFFAOYSA-N 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical compound [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 description 1
- 229910052939 potassium sulfate Inorganic materials 0.000 description 1
- 235000011151 potassium sulphates Nutrition 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 239000011241 protective layer Substances 0.000 description 1
- 150000003242 quaternary ammonium salts Chemical class 0.000 description 1
- 229910001379 sodium hypophosphite Inorganic materials 0.000 description 1
- 229950000244 sulfanilic acid Drugs 0.000 description 1
- 150000003871 sulfonates Chemical class 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 238000004381 surface treatment Methods 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 231100000563 toxic property Toxicity 0.000 description 1
- 238000012549 training Methods 0.000 description 1
- 238000004065 wastewater treatment Methods 0.000 description 1
- 238000004018 waxing Methods 0.000 description 1
- 230000004580 weight loss Effects 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D11/00—Electrolytic coating by surface reaction, i.e. forming conversion layers
- C25D11/02—Anodisation
- C25D11/04—Anodisation of aluminium or alloys based thereon
- C25D11/18—After-treatment, e.g. pore-sealing
- C25D11/24—Chemical after-treatment
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D11/00—Electrolytic coating by surface reaction, i.e. forming conversion layers
- C25D11/02—Anodisation
- C25D11/04—Anodisation of aluminium or alloys based thereon
- C25D11/18—After-treatment, e.g. pore-sealing
- C25D11/24—Chemical after-treatment
- C25D11/246—Chemical after-treatment for sealing layers
Landscapes
- Chemical & Material Sciences (AREA)
- Metallurgy (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Treatment Of Metals (AREA)
- Preventing Corrosion Or Incrustation Of Metals (AREA)
- Gasket Seals (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
- Paints Or Removers (AREA)
Priority Applications (16)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19621818A DE19621818A1 (de) | 1996-05-31 | 1996-05-31 | Kurzzeit-Heißverdichtung anodisierter Metalloberflächen mit tensidhaltigen Lösungen |
| AU29598/97A AU719630B2 (en) | 1996-05-31 | 1997-05-22 | Short-term heat-sealing of anodized metal surfaces with surfactant-containing solutions |
| DE59702148T DE59702148D1 (de) | 1996-05-31 | 1997-05-22 | Kurzzeit-heissverdichtung anodisierter metalloberflächen mit tensidhaltigen lösungen |
| AT97923978T ATE195356T1 (de) | 1996-05-31 | 1997-05-22 | Kurzzeit-heissverdichtung anodisierter metalloberflächen mit tensidhaltigen lösungen |
| CA002257253A CA2257253A1 (en) | 1996-05-31 | 1997-05-22 | Short time hot sealing of anodized metal surfaces with surfactant-containing solutions |
| PL97330016A PL330016A1 (en) | 1996-05-31 | 1997-05-22 | Transitory hot-desification of anodised metal surfaces by means of solutions containing surfactants |
| PCT/EP1997/002620 WO1997046738A1 (de) | 1996-05-31 | 1997-05-22 | Kurzzeit-heissverdichtung anodisierter metalloberflächen mit tensidhaltigen lösungen |
| TR1998/02338T TR199802338T2 (xx) | 1996-05-31 | 1997-05-22 | Anotlanm�� metal y�zeylerin y�zeyaktif maddeler i�eren ��zeltilerle h�zland�r�lm�� s�cak son-kaplamalar� |
| JP10500155A JP2000511972A (ja) | 1996-05-31 | 1997-05-22 | 界面活性剤含有溶液を用いる陽極酸化金属面の短期間の加熱による封孔処理 |
| ES97923978T ES2150250T3 (es) | 1996-05-31 | 1997-05-22 | Termosellado rapido de superficies metalicas anodizadas con soluciones que contienen tensioactivos |
| KR1019980709697A KR20000016130A (ko) | 1996-05-31 | 1997-05-22 | 계면활성제를 함유한 용액을 이용한 양극산화된 금속 표면의 단기간 열밀봉 |
| CN97195000A CN1219984A (zh) | 1996-05-31 | 1997-05-22 | 使用含表面活性剂溶液快速热封阳极化金属表面的方法 |
| EP97923978A EP0902849B1 (de) | 1996-05-31 | 1997-05-22 | Kurzzeit-heissverdichtung anodisierter metalloberflächen mit tensidhaltigen lösungen |
| US09/194,391 US6059897A (en) | 1996-05-31 | 1997-05-22 | Short-term heat-sealing of anodized metal surfaces with surfactant-containing solutions |
| ZA9704742A ZA974742B (en) | 1996-05-31 | 1997-05-29 | Accelerated hot post-sealing of anodised metal surfaces using solutions containing surfactants. |
| ARP970102350A AR007357A1 (es) | 1996-05-31 | 1997-05-30 | Procedimiento para el sellado de superficies metalicas anodizadas con soluciones acuosas que contienen por lo menos un tensioactivo y por lo menosun acido organico y en los cuales pueden estar presentes metales alcalinos o alcalinoterreos, procedimiento para el tratamiento posterior de las superficies |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19621818A DE19621818A1 (de) | 1996-05-31 | 1996-05-31 | Kurzzeit-Heißverdichtung anodisierter Metalloberflächen mit tensidhaltigen Lösungen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE19621818A1 true DE19621818A1 (de) | 1997-12-04 |
Family
ID=7795743
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19621818A Withdrawn DE19621818A1 (de) | 1996-05-31 | 1996-05-31 | Kurzzeit-Heißverdichtung anodisierter Metalloberflächen mit tensidhaltigen Lösungen |
| DE59702148T Expired - Fee Related DE59702148D1 (de) | 1996-05-31 | 1997-05-22 | Kurzzeit-heissverdichtung anodisierter metalloberflächen mit tensidhaltigen lösungen |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE59702148T Expired - Fee Related DE59702148D1 (de) | 1996-05-31 | 1997-05-22 | Kurzzeit-heissverdichtung anodisierter metalloberflächen mit tensidhaltigen lösungen |
Country Status (15)
| Country | Link |
|---|---|
| US (1) | US6059897A (enExample) |
| EP (1) | EP0902849B1 (enExample) |
| JP (1) | JP2000511972A (enExample) |
| KR (1) | KR20000016130A (enExample) |
| CN (1) | CN1219984A (enExample) |
| AR (1) | AR007357A1 (enExample) |
| AT (1) | ATE195356T1 (enExample) |
| AU (1) | AU719630B2 (enExample) |
| CA (1) | CA2257253A1 (enExample) |
| DE (2) | DE19621818A1 (enExample) |
| ES (1) | ES2150250T3 (enExample) |
| PL (1) | PL330016A1 (enExample) |
| TR (1) | TR199802338T2 (enExample) |
| WO (1) | WO1997046738A1 (enExample) |
| ZA (1) | ZA974742B (enExample) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2000036190A3 (de) * | 1998-12-16 | 2000-11-09 | Henkel Kgaa | Verbessertes verdichtungsverfahren für anodisierte metalloberflächen |
| WO2003052171A3 (de) * | 2001-12-15 | 2003-07-24 | Henkel Kgaa | Verdichtung von anodisierten metalloberflächen zur verbessung des witterungsverhaltens |
Families Citing this family (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10022074A1 (de) * | 2000-05-06 | 2001-11-08 | Henkel Kgaa | Elektrochemisch erzeugte Schichten zum Korrosionsschutz oder als Haftgrund |
| DE60235927D1 (de) * | 2001-06-28 | 2010-05-20 | Alonim Holding Agricultural Co | Oberflächebehandlung zur Verbesserung der Korrosionsbeständigkeit von Magnesium |
| US6916414B2 (en) | 2001-10-02 | 2005-07-12 | Henkel Kommanditgesellschaft Auf Aktien | Light metal anodization |
| US7578921B2 (en) | 2001-10-02 | 2009-08-25 | Henkel Kgaa | Process for anodically coating aluminum and/or titanium with ceramic oxides |
| US7820300B2 (en) * | 2001-10-02 | 2010-10-26 | Henkel Ag & Co. Kgaa | Article of manufacture and process for anodically coating an aluminum substrate with ceramic oxides prior to organic or inorganic coating |
| US7569132B2 (en) * | 2001-10-02 | 2009-08-04 | Henkel Kgaa | Process for anodically coating an aluminum substrate with ceramic oxides prior to polytetrafluoroethylene or silicone coating |
| US7452454B2 (en) * | 2001-10-02 | 2008-11-18 | Henkel Kgaa | Anodized coating over aluminum and aluminum alloy coated substrates |
| DE102006005765A1 (de) * | 2006-02-07 | 2007-08-09 | Henkel Kgaa | Verbesserung der Reinigung von Lackapplikationsgeräten |
| US20090056090A1 (en) * | 2007-09-05 | 2009-03-05 | Thomas Bunk | Memorial article and method thereof |
| RU2354759C1 (ru) * | 2007-09-24 | 2009-05-10 | Государственное образовательное учреждение высшего профессионального образования Пензенская государственная технологическая академия | Способ получения покрытий |
| JP5370014B2 (ja) * | 2008-09-01 | 2013-12-18 | スズキ株式会社 | 陽極酸化皮膜の封孔処理方法 |
| US9701177B2 (en) | 2009-04-02 | 2017-07-11 | Henkel Ag & Co. Kgaa | Ceramic coated automotive heat exchanger components |
| JP5408612B2 (ja) * | 2009-04-13 | 2014-02-05 | 奥野製薬工業株式会社 | アルミニウム合金の陽極酸化皮膜用封孔処理方法 |
| RU2424381C1 (ru) * | 2010-06-07 | 2011-07-20 | Государственное образовательное учреждение высшего профессионального образования "Тверской государственный технический университет" | Способ получения износостойкого покрытия на алюминии и его сплавах |
| DE102012204636A1 (de) * | 2012-03-22 | 2013-09-26 | Nanogate Ag | Behandlung einer anodisch oxidierten Oberfläche |
| WO2016039809A1 (en) * | 2014-09-08 | 2016-03-17 | Mct Research And Development | Silicate coatings |
| RU2581956C1 (ru) * | 2014-12-30 | 2016-04-20 | Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Тверской государственный технический университет" | Способ нанесения керамического покрытия на алюминий и его сплавы |
| US10920332B2 (en) | 2015-01-19 | 2021-02-16 | Council Of Scientific And Industrial Research | Process for the preparation of corrosion resistance sealed anodized coatings on aluminum alloy |
| CN106191959A (zh) * | 2015-05-08 | 2016-12-07 | 广州市汉科建材科技有限公司 | 一种环保型铝合金封孔剂 |
| HK1258691A1 (zh) * | 2016-03-28 | 2019-11-15 | 奥野制药工业株式会社 | 铝合金的阳极氧化覆膜用封孔处理液、浓缩液和封孔处理方法 |
| US10138566B2 (en) * | 2017-01-13 | 2018-11-27 | Macdermid Acumen, Inc. | Sealing anodized aluminum using a low-temperature nickel-free process |
| PL424520A1 (pl) * | 2018-02-06 | 2019-08-12 | Cim-Mes Projekt Spółka Z Ograniczoną Odpowiedzialnością | Sposób formowania warstwy powierzchniowej aluminium |
| DE102019101449A1 (de) | 2019-01-21 | 2020-07-23 | Carl Freudenberg Kg | Oberflächenbehandlung von eloxiertem Aluminium |
| KR102365724B1 (ko) * | 2020-10-16 | 2022-02-23 | 주식회사 영광와이케이엠씨 | 황산 아노다이징 처리된 알루미늄 합금용 봉공처리액 및 이를 이용한 황산 아노다이징 처리된 알루미늄 합금의 고내식성 봉공처리방법 |
| KR102467268B1 (ko) * | 2020-10-29 | 2022-11-17 | 주식회사 영광와이케이엠씨 | 옥살산 전해액에서 전류밀도 변화에 따른 아노다이징 처리 방법 |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH220502A (de) * | 1941-01-31 | 1942-04-15 | Chem Ind Basel | Verfahren zur Nachbehandlung von anoxydiertem Aluminium und dessen Legierungen. |
| US3257244A (en) * | 1964-10-14 | 1966-06-21 | Reynolds Metals Co | Sealing and inhibiting corrosion of anodized aluminum |
| GB1232693A (enExample) * | 1968-05-28 | 1971-05-19 | ||
| DE2211553C3 (de) * | 1972-03-10 | 1978-04-20 | Henkel Kgaa, 4000 Duesseldorf | Verfahren zum Verdichten von anodischen Oxidschichten auf Aluminium und Aluminiumlegierungen |
| DE2650989C2 (de) * | 1976-11-08 | 1985-01-24 | Henkel KGaA, 4000 Düsseldorf | Verfahren zur Behandlung von Aluminiumoberflächen durch Oxidation mit einer nachfolgenden Verdichtung |
| DE3233411A1 (de) * | 1982-09-09 | 1984-03-15 | Henkel KGaA, 4000 Düsseldorf | Verfahren zum verdichten von anodisch erzeugten oxidschichten auf aluminium oder aluminiumlegierungen |
| GB8309571D0 (en) * | 1983-04-08 | 1983-05-11 | Albright & Wilson | Accelerated sealing of anodised aluminium |
| US4647347A (en) * | 1984-08-16 | 1987-03-03 | Amchen Products, Inc. | Process and sealant compositions for sealing anodized aluminum |
| DE3820650A1 (de) * | 1988-06-18 | 1989-12-21 | Henkel Kgaa | Verfahren zum verdichten von anodisierten oxidschichten auf aluminium und aluminiumlegierungen |
| US5411607A (en) * | 1993-11-10 | 1995-05-02 | Novamax Technologies Holdings, Inc. | Process and composition for sealing anodized aluminum surfaces |
| DE19538777A1 (de) * | 1995-10-18 | 1997-04-24 | Henkel Kgaa | Kurzzeit-Heißverdichtung anodisierter Metalloberflächen |
-
1996
- 1996-05-31 DE DE19621818A patent/DE19621818A1/de not_active Withdrawn
-
1997
- 1997-05-22 US US09/194,391 patent/US6059897A/en not_active Expired - Fee Related
- 1997-05-22 CA CA002257253A patent/CA2257253A1/en not_active Abandoned
- 1997-05-22 AT AT97923978T patent/ATE195356T1/de not_active IP Right Cessation
- 1997-05-22 JP JP10500155A patent/JP2000511972A/ja not_active Ceased
- 1997-05-22 KR KR1019980709697A patent/KR20000016130A/ko not_active Withdrawn
- 1997-05-22 PL PL97330016A patent/PL330016A1/xx unknown
- 1997-05-22 TR TR1998/02338T patent/TR199802338T2/xx unknown
- 1997-05-22 WO PCT/EP1997/002620 patent/WO1997046738A1/de not_active Ceased
- 1997-05-22 AU AU29598/97A patent/AU719630B2/en not_active Ceased
- 1997-05-22 EP EP97923978A patent/EP0902849B1/de not_active Expired - Lifetime
- 1997-05-22 ES ES97923978T patent/ES2150250T3/es not_active Expired - Lifetime
- 1997-05-22 CN CN97195000A patent/CN1219984A/zh active Pending
- 1997-05-22 DE DE59702148T patent/DE59702148D1/de not_active Expired - Fee Related
- 1997-05-29 ZA ZA9704742A patent/ZA974742B/xx unknown
- 1997-05-30 AR ARP970102350A patent/AR007357A1/es not_active Application Discontinuation
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2000036190A3 (de) * | 1998-12-16 | 2000-11-09 | Henkel Kgaa | Verbessertes verdichtungsverfahren für anodisierte metalloberflächen |
| WO2003052171A3 (de) * | 2001-12-15 | 2003-07-24 | Henkel Kgaa | Verdichtung von anodisierten metalloberflächen zur verbessung des witterungsverhaltens |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1219984A (zh) | 1999-06-16 |
| WO1997046738A1 (de) | 1997-12-11 |
| AU2959897A (en) | 1998-01-05 |
| ES2150250T3 (es) | 2000-11-16 |
| KR20000016130A (ko) | 2000-03-25 |
| ZA974742B (en) | 1997-12-01 |
| EP0902849A1 (de) | 1999-03-24 |
| PL330016A1 (en) | 1999-04-26 |
| JP2000511972A (ja) | 2000-09-12 |
| AU719630B2 (en) | 2000-05-11 |
| EP0902849B1 (de) | 2000-08-09 |
| DE59702148D1 (de) | 2000-09-14 |
| ATE195356T1 (de) | 2000-08-15 |
| US6059897A (en) | 2000-05-09 |
| CA2257253A1 (en) | 1997-12-11 |
| TR199802338T2 (xx) | 1999-02-22 |
| AR007357A1 (es) | 1999-10-27 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8141 | Disposal/no request for examination |