CA2257253A1 - Short time hot sealing of anodized metal surfaces with surfactant-containing solutions - Google Patents
Short time hot sealing of anodized metal surfaces with surfactant-containing solutions Download PDFInfo
- Publication number
- CA2257253A1 CA2257253A1 CA002257253A CA2257253A CA2257253A1 CA 2257253 A1 CA2257253 A1 CA 2257253A1 CA 002257253 A CA002257253 A CA 002257253A CA 2257253 A CA2257253 A CA 2257253A CA 2257253 A1 CA2257253 A1 CA 2257253A1
- Authority
- CA
- Canada
- Prior art keywords
- acid
- acids
- sealing
- anodized
- post
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
- 239000002184 metal Substances 0.000 title claims abstract description 25
- 229910052751 metal Inorganic materials 0.000 title claims abstract description 24
- 239000004094 surface-active agent Substances 0.000 title claims abstract description 4
- 238000007789 sealing Methods 0.000 title abstract description 61
- 238000000034 method Methods 0.000 claims abstract description 40
- 238000000576 coating method Methods 0.000 claims abstract description 38
- 239000002253 acid Substances 0.000 claims abstract description 31
- 239000000243 solution Substances 0.000 claims abstract description 27
- 150000007513 acids Chemical class 0.000 claims abstract description 18
- 239000007864 aqueous solution Substances 0.000 claims abstract description 15
- 239000011248 coating agent Substances 0.000 claims abstract description 15
- 239000002736 nonionic surfactant Substances 0.000 claims abstract description 10
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 claims abstract description 8
- 150000007524 organic acids Chemical class 0.000 claims abstract description 8
- 150000003009 phosphonic acids Chemical class 0.000 claims abstract description 8
- 235000005985 organic acids Nutrition 0.000 claims abstract description 7
- 239000003945 anionic surfactant Substances 0.000 claims abstract description 6
- 238000009835 boiling Methods 0.000 claims abstract description 5
- 239000003093 cationic surfactant Substances 0.000 claims abstract description 5
- 125000000129 anionic group Chemical group 0.000 claims abstract description 3
- 125000002091 cationic group Chemical group 0.000 claims abstract description 3
- 125000004122 cyclic group Chemical group 0.000 claims abstract description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 17
- 150000001412 amines Chemical class 0.000 claims description 15
- 150000001340 alkali metals Chemical class 0.000 claims description 11
- 229910001420 alkaline earth metal ion Inorganic materials 0.000 claims description 11
- 229910001413 alkali metal ion Inorganic materials 0.000 claims description 10
- 125000000217 alkyl group Chemical group 0.000 claims description 9
- 125000004432 carbon atom Chemical group C* 0.000 claims description 6
- 150000001735 carboxylic acids Chemical class 0.000 claims description 6
- 239000008367 deionised water Substances 0.000 claims description 5
- 229910021641 deionized water Inorganic materials 0.000 claims description 5
- 229910052744 lithium Inorganic materials 0.000 claims description 5
- 229910052749 magnesium Inorganic materials 0.000 claims description 5
- YDONNITUKPKTIG-UHFFFAOYSA-N [Nitrilotris(methylene)]trisphosphonic acid Chemical compound OP(O)(=O)CN(CP(O)(O)=O)CP(O)(O)=O YDONNITUKPKTIG-UHFFFAOYSA-N 0.000 claims description 4
- YDSWCNNOKPMOTP-UHFFFAOYSA-N mellitic acid Chemical compound OC(=O)C1=C(C(O)=O)C(C(O)=O)=C(C(O)=O)C(C(O)=O)=C1C(O)=O YDSWCNNOKPMOTP-UHFFFAOYSA-N 0.000 claims description 4
- CYIDZMCFTVVTJO-UHFFFAOYSA-N pyromellitic acid Chemical compound OC(=O)C1=CC(C(O)=O)=C(C(O)=O)C=C1C(O)=O CYIDZMCFTVVTJO-UHFFFAOYSA-N 0.000 claims description 4
- ARCGXLSVLAOJQL-UHFFFAOYSA-N trimellitic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C(C(O)=O)=C1 ARCGXLSVLAOJQL-UHFFFAOYSA-N 0.000 claims description 4
- ZCOMURCDMLBWOR-UHFFFAOYSA-N (hydroxy-phenyl-phosphonomethyl)phosphonic acid Chemical compound OP(=O)(O)C(P(O)(O)=O)(O)C1=CC=CC=C1 ZCOMURCDMLBWOR-UHFFFAOYSA-N 0.000 claims description 3
- KMDMOMDSEVTJTI-UHFFFAOYSA-N 2-phosphonobutanedioic acid Chemical compound OC(=O)CC(C(O)=O)P(O)(O)=O KMDMOMDSEVTJTI-UHFFFAOYSA-N 0.000 claims description 3
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical group C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 claims description 3
- DBVJJBKOTRCVKF-UHFFFAOYSA-N Etidronic acid Chemical compound OP(=O)(O)C(O)(C)P(O)(O)=O DBVJJBKOTRCVKF-UHFFFAOYSA-N 0.000 claims description 3
- LDTZSTJLVYBEKB-UHFFFAOYSA-N butedronic acid Chemical compound OC(=O)CC(C(O)=O)C(P(O)(O)=O)P(O)(O)=O LDTZSTJLVYBEKB-UHFFFAOYSA-N 0.000 claims description 3
- 150000002191 fatty alcohols Chemical class 0.000 claims description 3
- 229920006395 saturated elastomer Polymers 0.000 claims description 3
- GPCTYPSWRBUGFH-UHFFFAOYSA-N (1-amino-1-phosphonoethyl)phosphonic acid Chemical compound OP(=O)(O)C(N)(C)P(O)(O)=O GPCTYPSWRBUGFH-UHFFFAOYSA-N 0.000 claims description 2
- RUPZRJCPTQGQRU-UHFFFAOYSA-N (1-hydroxy-1-phosphonobutyl)phosphonic acid Chemical compound CCCC(O)(P(O)(O)=O)P(O)(O)=O RUPZRJCPTQGQRU-UHFFFAOYSA-N 0.000 claims description 2
- XHAZMZWXAOBLQG-UHFFFAOYSA-N (1-hydroxy-1-phosphonopropyl)phosphonic acid Chemical compound CCC(O)(P(O)(O)=O)P(O)(O)=O XHAZMZWXAOBLQG-UHFFFAOYSA-N 0.000 claims description 2
- IDYCJOKDHJLCGO-UHFFFAOYSA-N (amino-phenyl-phosphonomethyl)phosphonic acid Chemical compound OP(=O)(O)C(P(O)(O)=O)(N)C1=CC=CC=C1 IDYCJOKDHJLCGO-UHFFFAOYSA-N 0.000 claims description 2
- GPXCJKUXBIGASD-UHFFFAOYSA-N 1-phosphonobutane-1,2,4-tricarboxylic acid Chemical compound OC(=O)CCC(C(O)=O)C(C(O)=O)P(O)(O)=O GPXCJKUXBIGASD-UHFFFAOYSA-N 0.000 claims description 2
- SCOXZKRXKMRCCY-UHFFFAOYSA-N [1-(dimethylamino)-1-phosphonoethyl]phosphonic acid Chemical compound CN(C)C(C)(P(O)(O)=O)P(O)(O)=O SCOXZKRXKMRCCY-UHFFFAOYSA-N 0.000 claims description 2
- SBRJRPNSSOSLRR-UHFFFAOYSA-N [1-phosphono-1-(propylamino)ethyl]phosphonic acid Chemical compound CCCNC(C)(P(O)(O)=O)P(O)(O)=O SBRJRPNSSOSLRR-UHFFFAOYSA-N 0.000 claims description 2
- -1 alkylaryl sulfates Chemical class 0.000 claims description 2
- WLWKIJKUDWYINL-UHFFFAOYSA-N cyclohexane-1,1,2,2,3,3-hexacarboxylic acid Chemical compound OC(=O)C1(C(O)=O)CCCC(C(O)=O)(C(O)=O)C1(C(O)=O)C(O)=O WLWKIJKUDWYINL-UHFFFAOYSA-N 0.000 claims description 2
- 238000006386 neutralization reaction Methods 0.000 claims description 2
- 150000003871 sulfonates Chemical class 0.000 claims description 2
- QMKYBPDZANOJGF-UHFFFAOYSA-N benzene-1,3,5-tricarboxylic acid Chemical compound OC(=O)C1=CC(C(O)=O)=CC(C(O)=O)=C1 QMKYBPDZANOJGF-UHFFFAOYSA-N 0.000 claims 2
- QLGZQPQQPUMNBD-UHFFFAOYSA-N [1-(butylamino)-1-phosphonoethyl]phosphonic acid Chemical compound CCCCNC(C)(P(O)(O)=O)P(O)(O)=O QLGZQPQQPUMNBD-UHFFFAOYSA-N 0.000 claims 1
- 125000003710 aryl alkyl group Chemical group 0.000 claims 1
- 229910021645 metal ion Inorganic materials 0.000 claims 1
- JUJWROOIHBZHMG-UHFFFAOYSA-O pyridinium Chemical class C1=CC=[NH+]C=C1 JUJWROOIHBZHMG-UHFFFAOYSA-O 0.000 claims 1
- 150000003242 quaternary ammonium salts Chemical class 0.000 claims 1
- 229910001416 lithium ion Inorganic materials 0.000 abstract description 2
- 239000003513 alkali Substances 0.000 abstract 1
- 229910001425 magnesium ion Inorganic materials 0.000 abstract 1
- 229910052782 aluminium Inorganic materials 0.000 description 14
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 14
- 238000012360 testing method Methods 0.000 description 12
- 235000013162 Cocos nucifera Nutrition 0.000 description 8
- 244000060011 Cocos nucifera Species 0.000 description 8
- 239000000975 dye Substances 0.000 description 8
- 150000002739 metals Chemical class 0.000 description 8
- 229940116254 phosphonic acid Drugs 0.000 description 8
- 238000004040 coloring Methods 0.000 description 7
- 230000007797 corrosion Effects 0.000 description 7
- 238000005260 corrosion Methods 0.000 description 7
- 239000003792 electrolyte Substances 0.000 description 7
- 238000005259 measurement Methods 0.000 description 7
- 150000003839 salts Chemical class 0.000 description 7
- 239000000126 substance Substances 0.000 description 7
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 6
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 5
- 239000000654 additive Substances 0.000 description 5
- 239000003112 inhibitor Substances 0.000 description 5
- KBPLFHHGFOOTCA-UHFFFAOYSA-N 1-Octanol Chemical compound CCCCCCCCO KBPLFHHGFOOTCA-UHFFFAOYSA-N 0.000 description 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 4
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 4
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 4
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 4
- 229910045601 alloy Inorganic materials 0.000 description 4
- 239000000956 alloy Substances 0.000 description 4
- 238000002048 anodisation reaction Methods 0.000 description 4
- 239000012141 concentrate Substances 0.000 description 4
- 239000011777 magnesium Substances 0.000 description 4
- COKIOUWMXONTKQ-UHFFFAOYSA-N 1-phosphonopropane-1,2,3-tricarboxylic acid Chemical compound OC(=O)CC(C(O)=O)C(C(O)=O)P(O)(O)=O COKIOUWMXONTKQ-UHFFFAOYSA-N 0.000 description 3
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 3
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 3
- 239000010407 anodic oxide Substances 0.000 description 3
- KRVSOGSZCMJSLX-UHFFFAOYSA-L chromic acid Substances O[Cr](O)(=O)=O KRVSOGSZCMJSLX-UHFFFAOYSA-L 0.000 description 3
- AWJWCTOOIBYHON-UHFFFAOYSA-N furo[3,4-b]pyrazine-5,7-dione Chemical compound C1=CN=C2C(=O)OC(=O)C2=N1 AWJWCTOOIBYHON-UHFFFAOYSA-N 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000011148 porous material Substances 0.000 description 3
- 239000010936 titanium Substances 0.000 description 3
- 229910052719 titanium Inorganic materials 0.000 description 3
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 2
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 2
- HVBSAKJJOYLTQU-UHFFFAOYSA-N 4-aminobenzenesulfonic acid Chemical compound NC1=CC=C(S(O)(=O)=O)C=C1 HVBSAKJJOYLTQU-UHFFFAOYSA-N 0.000 description 2
- 229910000838 Al alloy Inorganic materials 0.000 description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- WGLPBDUCMAPZCE-UHFFFAOYSA-N Trioxochromium Chemical compound O=[Cr](=O)=O WGLPBDUCMAPZCE-UHFFFAOYSA-N 0.000 description 2
- 150000001242 acetic acid derivatives Chemical class 0.000 description 2
- 239000000853 adhesive Substances 0.000 description 2
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 2
- 229910021529 ammonia Inorganic materials 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 229910001424 calcium ion Inorganic materials 0.000 description 2
- 235000019864 coconut oil Nutrition 0.000 description 2
- 239000003240 coconut oil Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 239000000470 constituent Substances 0.000 description 2
- 229920001577 copolymer Polymers 0.000 description 2
- 238000010790 dilution Methods 0.000 description 2
- 239000012895 dilution Substances 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 150000002222 fluorine compounds Chemical class 0.000 description 2
- 230000002401 inhibitory effect Effects 0.000 description 2
- UEGPKNKPLBYCNK-UHFFFAOYSA-L magnesium acetate Chemical compound [Mg+2].CC([O-])=O.CC([O-])=O UEGPKNKPLBYCNK-UHFFFAOYSA-L 0.000 description 2
- 229940069446 magnesium acetate Drugs 0.000 description 2
- 235000011285 magnesium acetate Nutrition 0.000 description 2
- 239000011654 magnesium acetate Substances 0.000 description 2
- 150000002815 nickel Chemical class 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 2
- 230000017105 transposition Effects 0.000 description 2
- LBPHBRVNBKGYTP-UHFFFAOYSA-N (1-hydroxy-1-phosphonohexyl)phosphonic acid Chemical compound CCCCCC(O)(P(O)(O)=O)P(O)(O)=O LBPHBRVNBKGYTP-UHFFFAOYSA-N 0.000 description 1
- GKQHIYSTBXDYNQ-UHFFFAOYSA-M 1-dodecylpyridin-1-ium;chloride Chemical compound [Cl-].CCCCCCCCCCCC[N+]1=CC=CC=C1 GKQHIYSTBXDYNQ-UHFFFAOYSA-M 0.000 description 1
- SDGNNLQZAPXALR-UHFFFAOYSA-N 3-sulfophthalic acid Chemical compound OC(=O)C1=CC=CC(S(O)(=O)=O)=C1C(O)=O SDGNNLQZAPXALR-UHFFFAOYSA-N 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical class [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- USFZMSVCRYTOJT-UHFFFAOYSA-N Ammonium acetate Chemical compound N.CC(O)=O USFZMSVCRYTOJT-UHFFFAOYSA-N 0.000 description 1
- 239000005695 Ammonium acetate Substances 0.000 description 1
- 229940120146 EDTMP Drugs 0.000 description 1
- QUSNBJAOOMFDIB-UHFFFAOYSA-N Ethylamine Chemical compound CCN QUSNBJAOOMFDIB-UHFFFAOYSA-N 0.000 description 1
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 description 1
- DJEQZVQFEPKLOY-UHFFFAOYSA-N N,N-dimethylbutylamine Chemical compound CCCCN(C)C DJEQZVQFEPKLOY-UHFFFAOYSA-N 0.000 description 1
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 1
- AMQJEAYHLZJPGS-UHFFFAOYSA-N N-Pentanol Chemical compound CCCCCO AMQJEAYHLZJPGS-UHFFFAOYSA-N 0.000 description 1
- YFONKFDEZLYQDH-OPQQBVKSSA-N N-[(1R,2S)-2,6-dimethyindan-1-yl]-6-[(1R)-1-fluoroethyl]-1,3,5-triazine-2,4-diamine Chemical compound C[C@@H](F)C1=NC(N)=NC(N[C@H]2C3=CC(C)=CC=C3C[C@@H]2C)=N1 YFONKFDEZLYQDH-OPQQBVKSSA-N 0.000 description 1
- ABLZXFCXXLZCGV-UHFFFAOYSA-N Phosphorous acid Chemical compound OP(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- YSMRWXYRXBRSND-UHFFFAOYSA-N TOTP Chemical compound CC1=CC=CC=C1OP(=O)(OC=1C(=CC=CC=1)C)OC1=CC=CC=C1C YSMRWXYRXBRSND-UHFFFAOYSA-N 0.000 description 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 1
- XTMZDPMXSRLXCC-UHFFFAOYSA-N [(1r)-1-[hydroxy(dioxido)phosphaniumyl]-1-phosphonopentyl]azanium Chemical compound CCCCC(N)(P(O)(O)=O)P(O)(O)=O XTMZDPMXSRLXCC-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 150000003926 acrylamides Chemical class 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 238000007792 addition Methods 0.000 description 1
- 230000000274 adsorptive effect Effects 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 150000008051 alkyl sulfates Chemical class 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- 229940043376 ammonium acetate Drugs 0.000 description 1
- 235000019257 ammonium acetate Nutrition 0.000 description 1
- 150000003863 ammonium salts Chemical class 0.000 description 1
- 238000007743 anodising Methods 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- JBIROUFYLSSYDX-UHFFFAOYSA-M benzododecinium chloride Chemical compound [Cl-].CCCCCCCCCCCC[N+](C)(C)CC1=CC=CC=C1 JBIROUFYLSSYDX-UHFFFAOYSA-M 0.000 description 1
- WGQKYBSKWIADBV-UHFFFAOYSA-N benzylamine Chemical compound NCC1=CC=CC=C1 WGQKYBSKWIADBV-UHFFFAOYSA-N 0.000 description 1
- 230000000740 bleeding effect Effects 0.000 description 1
- 239000000872 buffer Substances 0.000 description 1
- ZCDOYSPFYFSLEW-UHFFFAOYSA-N chromate(2-) Chemical class [O-][Cr]([O-])(=O)=O ZCDOYSPFYFSLEW-UHFFFAOYSA-N 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- MOTZDAYCYVMXPC-UHFFFAOYSA-N dodecyl hydrogen sulfate Chemical compound CCCCCCCCCCCCOS(O)(=O)=O MOTZDAYCYVMXPC-UHFFFAOYSA-N 0.000 description 1
- 229940043264 dodecyl sulfate Drugs 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- NFDRPXJGHKJRLJ-UHFFFAOYSA-N edtmp Chemical compound OP(O)(=O)CN(CP(O)(O)=O)CCN(CP(O)(O)=O)CP(O)(O)=O NFDRPXJGHKJRLJ-UHFFFAOYSA-N 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 239000003925 fat Substances 0.000 description 1
- 235000019197 fats Nutrition 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 150000002395 hexacarboxylic acids Chemical class 0.000 description 1
- MNWFXJYAOYHMED-UHFFFAOYSA-N hexane carboxylic acid Natural products CCCCCCC(O)=O MNWFXJYAOYHMED-UHFFFAOYSA-N 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 150000003893 lactate salts Chemical class 0.000 description 1
- XIXADJRWDQXREU-UHFFFAOYSA-M lithium acetate Chemical compound [Li+].CC([O-])=O XIXADJRWDQXREU-UHFFFAOYSA-M 0.000 description 1
- 229910003002 lithium salt Inorganic materials 0.000 description 1
- 159000000002 lithium salts Chemical class 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- GNVRJGIVDSQCOP-UHFFFAOYSA-N n-ethyl-n-methylethanamine Chemical compound CCN(C)CC GNVRJGIVDSQCOP-UHFFFAOYSA-N 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 150000002816 nickel compounds Chemical class 0.000 description 1
- DBJLJFTWODWSOF-UHFFFAOYSA-L nickel(ii) fluoride Chemical compound F[Ni]F DBJLJFTWODWSOF-UHFFFAOYSA-L 0.000 description 1
- 150000002823 nitrates Chemical class 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 150000003891 oxalate salts Chemical class 0.000 description 1
- 235000006408 oxalic acid Nutrition 0.000 description 1
- ACVYVLVWPXVTIT-UHFFFAOYSA-N phosphinic acid Chemical class O[PH2]=O ACVYVLVWPXVTIT-UHFFFAOYSA-N 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical compound [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 description 1
- 229910052939 potassium sulfate Inorganic materials 0.000 description 1
- 235000011151 potassium sulphates Nutrition 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 1
- 239000011253 protective coating Substances 0.000 description 1
- 230000009183 running Effects 0.000 description 1
- 229910001379 sodium hypophosphite Inorganic materials 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000007655 standard test method Methods 0.000 description 1
- 229950000244 sulfanilic acid Drugs 0.000 description 1
- 239000001117 sulphuric acid Substances 0.000 description 1
- 235000011149 sulphuric acid Nutrition 0.000 description 1
- 238000004381 surface treatment Methods 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 231100000563 toxic property Toxicity 0.000 description 1
- 238000004065 wastewater treatment Methods 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
- 230000004580 weight loss Effects 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D11/00—Electrolytic coating by surface reaction, i.e. forming conversion layers
- C25D11/02—Anodisation
- C25D11/04—Anodisation of aluminium or alloys based thereon
- C25D11/18—After-treatment, e.g. pore-sealing
- C25D11/24—Chemical after-treatment
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D11/00—Electrolytic coating by surface reaction, i.e. forming conversion layers
- C25D11/02—Anodisation
- C25D11/04—Anodisation of aluminium or alloys based thereon
- C25D11/18—After-treatment, e.g. pore-sealing
- C25D11/24—Chemical after-treatment
- C25D11/246—Chemical after-treatment for sealing layers
Landscapes
- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Chemical Treatment Of Metals (AREA)
- Preventing Corrosion Or Incrustation Of Metals (AREA)
- Gasket Seals (AREA)
- Paints Or Removers (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19621818.7 | 1996-05-31 | ||
| DE19621818A DE19621818A1 (de) | 1996-05-31 | 1996-05-31 | Kurzzeit-Heißverdichtung anodisierter Metalloberflächen mit tensidhaltigen Lösungen |
| PCT/EP1997/002620 WO1997046738A1 (de) | 1996-05-31 | 1997-05-22 | Kurzzeit-heissverdichtung anodisierter metalloberflächen mit tensidhaltigen lösungen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA2257253A1 true CA2257253A1 (en) | 1997-12-11 |
Family
ID=7795743
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA002257253A Abandoned CA2257253A1 (en) | 1996-05-31 | 1997-05-22 | Short time hot sealing of anodized metal surfaces with surfactant-containing solutions |
Country Status (15)
| Country | Link |
|---|---|
| US (1) | US6059897A (enExample) |
| EP (1) | EP0902849B1 (enExample) |
| JP (1) | JP2000511972A (enExample) |
| KR (1) | KR20000016130A (enExample) |
| CN (1) | CN1219984A (enExample) |
| AR (1) | AR007357A1 (enExample) |
| AT (1) | ATE195356T1 (enExample) |
| AU (1) | AU719630B2 (enExample) |
| CA (1) | CA2257253A1 (enExample) |
| DE (2) | DE19621818A1 (enExample) |
| ES (1) | ES2150250T3 (enExample) |
| PL (1) | PL330016A1 (enExample) |
| TR (1) | TR199802338T2 (enExample) |
| WO (1) | WO1997046738A1 (enExample) |
| ZA (1) | ZA974742B (enExample) |
Families Citing this family (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19858034A1 (de) * | 1998-12-16 | 2000-06-21 | Henkel Kgaa | Verbessertes Verdichtungsverfahren für anodisierte Metalloberflächen |
| DE10022074A1 (de) * | 2000-05-06 | 2001-11-08 | Henkel Kgaa | Elektrochemisch erzeugte Schichten zum Korrosionsschutz oder als Haftgrund |
| AU2002345320A1 (en) * | 2001-06-28 | 2003-03-03 | Algat Sherutey Gimur Teufati | Treatment for improved magnesium surface corrosion-resistance |
| US7578921B2 (en) * | 2001-10-02 | 2009-08-25 | Henkel Kgaa | Process for anodically coating aluminum and/or titanium with ceramic oxides |
| US7452454B2 (en) * | 2001-10-02 | 2008-11-18 | Henkel Kgaa | Anodized coating over aluminum and aluminum alloy coated substrates |
| US6916414B2 (en) | 2001-10-02 | 2005-07-12 | Henkel Kommanditgesellschaft Auf Aktien | Light metal anodization |
| US7820300B2 (en) * | 2001-10-02 | 2010-10-26 | Henkel Ag & Co. Kgaa | Article of manufacture and process for anodically coating an aluminum substrate with ceramic oxides prior to organic or inorganic coating |
| US7569132B2 (en) * | 2001-10-02 | 2009-08-04 | Henkel Kgaa | Process for anodically coating an aluminum substrate with ceramic oxides prior to polytetrafluoroethylene or silicone coating |
| DE10161847A1 (de) * | 2001-12-15 | 2003-06-26 | Henkel Kgaa | Verdichtung von anodisierten Metalloberflächen zur Verbesserung des Witterungsverhaltens |
| DE102006005765A1 (de) * | 2006-02-07 | 2007-08-09 | Henkel Kgaa | Verbesserung der Reinigung von Lackapplikationsgeräten |
| US20090056090A1 (en) * | 2007-09-05 | 2009-03-05 | Thomas Bunk | Memorial article and method thereof |
| RU2354759C1 (ru) * | 2007-09-24 | 2009-05-10 | Государственное образовательное учреждение высшего профессионального образования Пензенская государственная технологическая академия | Способ получения покрытий |
| JP5370014B2 (ja) * | 2008-09-01 | 2013-12-18 | スズキ株式会社 | 陽極酸化皮膜の封孔処理方法 |
| US9701177B2 (en) | 2009-04-02 | 2017-07-11 | Henkel Ag & Co. Kgaa | Ceramic coated automotive heat exchanger components |
| JP5408612B2 (ja) * | 2009-04-13 | 2014-02-05 | 奥野製薬工業株式会社 | アルミニウム合金の陽極酸化皮膜用封孔処理方法 |
| RU2424381C1 (ru) * | 2010-06-07 | 2011-07-20 | Государственное образовательное учреждение высшего профессионального образования "Тверской государственный технический университет" | Способ получения износостойкого покрытия на алюминии и его сплавах |
| DE102012204636A1 (de) * | 2012-03-22 | 2013-09-26 | Nanogate Ag | Behandlung einer anodisch oxidierten Oberfläche |
| MX2017003052A (es) * | 2014-09-08 | 2018-01-26 | Mct Res And Development | Recubrimientos de silicato. |
| RU2581956C1 (ru) * | 2014-12-30 | 2016-04-20 | Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Тверской государственный технический университет" | Способ нанесения керамического покрытия на алюминий и его сплавы |
| WO2016116949A1 (en) | 2015-01-19 | 2016-07-28 | Council Of Scientific & Industrial Research | A process for the preparation of corrosion resistant sealed anodized coatings on aluminum alloy |
| CN106191959A (zh) * | 2015-05-08 | 2016-12-07 | 广州市汉科建材科技有限公司 | 一种环保型铝合金封孔剂 |
| US20190112726A1 (en) * | 2016-03-28 | 2019-04-18 | Okuno Chemical Industries Co., Ltd. | Sealing liquid for anodic oxide coating films of aluminum alloy, concentrated liquid and sealing method |
| US10138566B2 (en) * | 2017-01-13 | 2018-11-27 | Macdermid Acumen, Inc. | Sealing anodized aluminum using a low-temperature nickel-free process |
| PL424520A1 (pl) * | 2018-02-06 | 2019-08-12 | Cim-Mes Projekt Spółka Z Ograniczoną Odpowiedzialnością | Sposób formowania warstwy powierzchniowej aluminium |
| DE102019101449A1 (de) | 2019-01-21 | 2020-07-23 | Carl Freudenberg Kg | Oberflächenbehandlung von eloxiertem Aluminium |
| KR102365724B1 (ko) * | 2020-10-16 | 2022-02-23 | 주식회사 영광와이케이엠씨 | 황산 아노다이징 처리된 알루미늄 합금용 봉공처리액 및 이를 이용한 황산 아노다이징 처리된 알루미늄 합금의 고내식성 봉공처리방법 |
| KR102467268B1 (ko) * | 2020-10-29 | 2022-11-17 | 주식회사 영광와이케이엠씨 | 옥살산 전해액에서 전류밀도 변화에 따른 아노다이징 처리 방법 |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH220502A (de) * | 1941-01-31 | 1942-04-15 | Chem Ind Basel | Verfahren zur Nachbehandlung von anoxydiertem Aluminium und dessen Legierungen. |
| US3257244A (en) * | 1964-10-14 | 1966-06-21 | Reynolds Metals Co | Sealing and inhibiting corrosion of anodized aluminum |
| GB1232693A (enExample) * | 1968-05-28 | 1971-05-19 | ||
| DE2211553C3 (de) * | 1972-03-10 | 1978-04-20 | Henkel Kgaa, 4000 Duesseldorf | Verfahren zum Verdichten von anodischen Oxidschichten auf Aluminium und Aluminiumlegierungen |
| DE2650989C2 (de) * | 1976-11-08 | 1985-01-24 | Henkel KGaA, 4000 Düsseldorf | Verfahren zur Behandlung von Aluminiumoberflächen durch Oxidation mit einer nachfolgenden Verdichtung |
| DE3233411A1 (de) * | 1982-09-09 | 1984-03-15 | Henkel KGaA, 4000 Düsseldorf | Verfahren zum verdichten von anodisch erzeugten oxidschichten auf aluminium oder aluminiumlegierungen |
| GB8309571D0 (en) * | 1983-04-08 | 1983-05-11 | Albright & Wilson | Accelerated sealing of anodised aluminium |
| US4647347A (en) * | 1984-08-16 | 1987-03-03 | Amchen Products, Inc. | Process and sealant compositions for sealing anodized aluminum |
| DE3820650A1 (de) * | 1988-06-18 | 1989-12-21 | Henkel Kgaa | Verfahren zum verdichten von anodisierten oxidschichten auf aluminium und aluminiumlegierungen |
| US5411607A (en) * | 1993-11-10 | 1995-05-02 | Novamax Technologies Holdings, Inc. | Process and composition for sealing anodized aluminum surfaces |
| DE19538777A1 (de) * | 1995-10-18 | 1997-04-24 | Henkel Kgaa | Kurzzeit-Heißverdichtung anodisierter Metalloberflächen |
-
1996
- 1996-05-31 DE DE19621818A patent/DE19621818A1/de not_active Withdrawn
-
1997
- 1997-05-22 PL PL97330016A patent/PL330016A1/xx unknown
- 1997-05-22 ES ES97923978T patent/ES2150250T3/es not_active Expired - Lifetime
- 1997-05-22 JP JP10500155A patent/JP2000511972A/ja not_active Ceased
- 1997-05-22 WO PCT/EP1997/002620 patent/WO1997046738A1/de not_active Ceased
- 1997-05-22 KR KR1019980709697A patent/KR20000016130A/ko not_active Withdrawn
- 1997-05-22 EP EP97923978A patent/EP0902849B1/de not_active Expired - Lifetime
- 1997-05-22 DE DE59702148T patent/DE59702148D1/de not_active Expired - Fee Related
- 1997-05-22 US US09/194,391 patent/US6059897A/en not_active Expired - Fee Related
- 1997-05-22 TR TR1998/02338T patent/TR199802338T2/xx unknown
- 1997-05-22 CA CA002257253A patent/CA2257253A1/en not_active Abandoned
- 1997-05-22 AU AU29598/97A patent/AU719630B2/en not_active Ceased
- 1997-05-22 CN CN97195000A patent/CN1219984A/zh active Pending
- 1997-05-22 AT AT97923978T patent/ATE195356T1/de not_active IP Right Cessation
- 1997-05-29 ZA ZA9704742A patent/ZA974742B/xx unknown
- 1997-05-30 AR ARP970102350A patent/AR007357A1/es not_active Application Discontinuation
Also Published As
| Publication number | Publication date |
|---|---|
| ES2150250T3 (es) | 2000-11-16 |
| WO1997046738A1 (de) | 1997-12-11 |
| DE59702148D1 (de) | 2000-09-14 |
| AR007357A1 (es) | 1999-10-27 |
| EP0902849A1 (de) | 1999-03-24 |
| EP0902849B1 (de) | 2000-08-09 |
| AU719630B2 (en) | 2000-05-11 |
| TR199802338T2 (xx) | 1999-02-22 |
| CN1219984A (zh) | 1999-06-16 |
| ATE195356T1 (de) | 2000-08-15 |
| US6059897A (en) | 2000-05-09 |
| KR20000016130A (ko) | 2000-03-25 |
| AU2959897A (en) | 1998-01-05 |
| JP2000511972A (ja) | 2000-09-12 |
| DE19621818A1 (de) | 1997-12-04 |
| ZA974742B (en) | 1997-12-01 |
| PL330016A1 (en) | 1999-04-26 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request | ||
| FZDE | Discontinued |