DE1907361A1 - Verfahren zur Herstellung von granuliertem Kalkammonsalpeter - Google Patents
Verfahren zur Herstellung von granuliertem KalkammonsalpeterInfo
- Publication number
- DE1907361A1 DE1907361A1 DE19691907361 DE1907361A DE1907361A1 DE 1907361 A1 DE1907361 A1 DE 1907361A1 DE 19691907361 DE19691907361 DE 19691907361 DE 1907361 A DE1907361 A DE 1907361A DE 1907361 A1 DE1907361 A1 DE 1907361A1
- Authority
- DE
- Germany
- Prior art keywords
- ammonia
- ammonium nitrate
- carbon dioxide
- reaction mixture
- nitrate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000000034 method Methods 0.000 title claims description 18
- NGLMYMJASOJOJY-UHFFFAOYSA-O azanium;calcium;nitrate Chemical compound [NH4+].[Ca].[O-][N+]([O-])=O NGLMYMJASOJOJY-UHFFFAOYSA-O 0.000 title claims description 7
- 238000004519 manufacturing process Methods 0.000 title claims description 7
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 36
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 26
- ZCCIPPOKBCJFDN-UHFFFAOYSA-N calcium nitrate Chemical compound [Ca+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O ZCCIPPOKBCJFDN-UHFFFAOYSA-N 0.000 claims description 26
- 229910021529 ammonia Inorganic materials 0.000 claims description 18
- 239000003337 fertilizer Substances 0.000 claims description 14
- 239000001569 carbon dioxide Substances 0.000 claims description 13
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 13
- PAWQVTBBRAZDMG-UHFFFAOYSA-N 2-(3-bromo-2-fluorophenyl)acetic acid Chemical compound OC(=O)CC1=CC=CC(Br)=C1F PAWQVTBBRAZDMG-UHFFFAOYSA-N 0.000 claims description 10
- 239000007789 gas Substances 0.000 claims description 9
- 239000008187 granular material Substances 0.000 claims description 8
- 235000008733 Citrus aurantifolia Nutrition 0.000 claims description 7
- 235000011941 Tilia x europaea Nutrition 0.000 claims description 7
- 239000004571 lime Substances 0.000 claims description 7
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 6
- 239000000725 suspension Substances 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- 229910001868 water Inorganic materials 0.000 claims description 6
- 229910052757 nitrogen Inorganic materials 0.000 claims description 5
- 239000011541 reaction mixture Substances 0.000 claims description 5
- 239000007791 liquid phase Substances 0.000 claims description 3
- 239000007787 solid Substances 0.000 claims description 3
- 239000000470 constituent Substances 0.000 claims description 2
- 230000029087 digestion Effects 0.000 claims description 2
- 238000000926 separation method Methods 0.000 claims description 2
- -1 nitric acid Calcium nitrate tetrahydrate Chemical compound 0.000 claims 1
- 239000002367 phosphate rock Substances 0.000 claims 1
- 238000000746 purification Methods 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 description 9
- 239000000203 mixture Substances 0.000 description 5
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 4
- 239000007795 chemical reaction product Substances 0.000 description 4
- ZHJGWYRLJUCMRT-UHFFFAOYSA-N 5-[6-[(4-methylpiperazin-1-yl)methyl]benzimidazol-1-yl]-3-[1-[2-(trifluoromethyl)phenyl]ethoxy]thiophene-2-carboxamide Chemical compound C=1C=CC=C(C(F)(F)F)C=1C(C)OC(=C(S1)C(N)=O)C=C1N(C1=C2)C=NC1=CC=C2CN1CCN(C)CC1 ZHJGWYRLJUCMRT-UHFFFAOYSA-N 0.000 description 3
- 229910019142 PO4 Inorganic materials 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 235000021317 phosphate Nutrition 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 2
- 229910000019 calcium carbonate Inorganic materials 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 238000000354 decomposition reaction Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 235000015097 nutrients Nutrition 0.000 description 2
- 150000003013 phosphoric acid derivatives Chemical class 0.000 description 2
- 229910052698 phosphorus Inorganic materials 0.000 description 2
- 229910052700 potassium Inorganic materials 0.000 description 2
- 239000011435 rock Substances 0.000 description 2
- 238000007493 shaping process Methods 0.000 description 2
- 102100023760 Cytosolic iron-sulfur assembly component 2B Human genes 0.000 description 1
- 241000272184 Falconiformes Species 0.000 description 1
- 101100167258 Homo sapiens CIAO2B gene Proteins 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 229910002651 NO3 Inorganic materials 0.000 description 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000000184 acid digestion Methods 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 description 1
- 229910052921 ammonium sulfate Inorganic materials 0.000 description 1
- 235000011130 ammonium sulphate Nutrition 0.000 description 1
- JCRBPEBDDUPYOF-UHFFFAOYSA-M azanium;calcium;carbonate;nitrate Chemical compound [NH4+].[Ca+2].[O-]C([O-])=O.[O-][N+]([O-])=O JCRBPEBDDUPYOF-UHFFFAOYSA-M 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000012084 conversion product Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 210000002969 egg yolk Anatomy 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 238000005469 granulation Methods 0.000 description 1
- 230000003179 granulation Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 229910052943 magnesium sulfate Inorganic materials 0.000 description 1
- 235000019341 magnesium sulphate Nutrition 0.000 description 1
- VUZPPFZMUPKLLV-UHFFFAOYSA-N methane;hydrate Chemical compound C.O VUZPPFZMUPKLLV-UHFFFAOYSA-N 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- 239000001103 potassium chloride Substances 0.000 description 1
- 235000011164 potassium chloride Nutrition 0.000 description 1
- 159000000001 potassium salts Chemical class 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C1/00—Ammonium nitrate fertilisers
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B11/00—Fertilisers produced by wet-treating or leaching raw materials either with acids in such amounts and concentrations as to yield solutions followed by neutralisation, or with alkaline lyes
- C05B11/04—Fertilisers produced by wet-treating or leaching raw materials either with acids in such amounts and concentrations as to yield solutions followed by neutralisation, or with alkaline lyes using mineral acid
- C05B11/06—Fertilisers produced by wet-treating or leaching raw materials either with acids in such amounts and concentrations as to yield solutions followed by neutralisation, or with alkaline lyes using mineral acid using nitric acid (nitrophosphates)
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C1/00—Ammonium nitrate fertilisers
- C05C1/02—Granulation; Pelletisation; Stabilisation; Colouring
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Fertilizers (AREA)
Priority Applications (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19691907361 DE1907361A1 (de) | 1969-02-14 | 1969-02-14 | Verfahren zur Herstellung von granuliertem Kalkammonsalpeter |
| SE99370A SE358630B (cs) | 1969-02-14 | 1970-01-27 | |
| CS74870A CS164854B2 (cs) | 1969-02-14 | 1970-02-03 | |
| DK52070A DK122808B (da) | 1969-02-14 | 1970-02-03 | Fremgangsmåde til fremstilling af granuleret kalkammonsalpater. |
| BE745561D BE745561A (fr) | 1969-02-14 | 1970-02-05 | Procede pour la preparation d'un melange granule de carbonate de calcium et de nitrate d'ammonium |
| FR7005011A FR2031424A1 (en) | 1969-02-14 | 1970-02-12 | Process for preparing granulated mixtures - of caco3 and nh4o3 |
| NO51670A NO122435B (cs) | 1969-02-14 | 1970-02-13 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19691907361 DE1907361A1 (de) | 1969-02-14 | 1969-02-14 | Verfahren zur Herstellung von granuliertem Kalkammonsalpeter |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1907361A1 true DE1907361A1 (de) | 1970-08-27 |
Family
ID=5725212
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19691907361 Withdrawn DE1907361A1 (de) | 1969-02-14 | 1969-02-14 | Verfahren zur Herstellung von granuliertem Kalkammonsalpeter |
Country Status (7)
| Country | Link |
|---|---|
| BE (1) | BE745561A (cs) |
| CS (1) | CS164854B2 (cs) |
| DE (1) | DE1907361A1 (cs) |
| DK (1) | DK122808B (cs) |
| FR (1) | FR2031424A1 (cs) |
| NO (1) | NO122435B (cs) |
| SE (1) | SE358630B (cs) |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE943775C (de) * | 1953-08-12 | 1956-06-01 | Chem Fab Kalk Ges Mit Beschrae | Verfahren zur Herstellung von Kalkammonsalpeter |
-
1969
- 1969-02-14 DE DE19691907361 patent/DE1907361A1/de not_active Withdrawn
-
1970
- 1970-01-27 SE SE99370A patent/SE358630B/xx unknown
- 1970-02-03 CS CS74870A patent/CS164854B2/cs unknown
- 1970-02-03 DK DK52070A patent/DK122808B/da unknown
- 1970-02-05 BE BE745561D patent/BE745561A/xx unknown
- 1970-02-12 FR FR7005011A patent/FR2031424A1/fr active Granted
- 1970-02-13 NO NO51670A patent/NO122435B/no unknown
Also Published As
| Publication number | Publication date |
|---|---|
| DK122808B (da) | 1972-04-17 |
| BE745561A (fr) | 1970-08-05 |
| CS164854B2 (cs) | 1975-11-28 |
| FR2031424B1 (cs) | 1974-06-21 |
| FR2031424A1 (en) | 1970-11-20 |
| SE358630B (cs) | 1973-08-06 |
| NO122435B (cs) | 1971-06-28 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| E77 | Valid patent as to the heymanns-index 1977 | ||
| 8339 | Ceased/non-payment of the annual fee |