DE1592467C3 - Verfahren zur Herstellung eines sehr reinen roten Bleimonoxids - Google Patents
Verfahren zur Herstellung eines sehr reinen roten BleimonoxidsInfo
- Publication number
- DE1592467C3 DE1592467C3 DE1592467A DE1592467A DE1592467C3 DE 1592467 C3 DE1592467 C3 DE 1592467C3 DE 1592467 A DE1592467 A DE 1592467A DE 1592467 A DE1592467 A DE 1592467A DE 1592467 C3 DE1592467 C3 DE 1592467C3
- Authority
- DE
- Germany
- Prior art keywords
- lead
- silicon
- lead monoxide
- monoxide
- ammonia
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- YEXPOXQUZXUXJW-UHFFFAOYSA-N oxolead Chemical compound [Pb]=O YEXPOXQUZXUXJW-UHFFFAOYSA-N 0.000 title claims description 64
- 238000000034 method Methods 0.000 title claims description 6
- 238000004519 manufacturing process Methods 0.000 title claims description 5
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 26
- 229910021529 ammonia Inorganic materials 0.000 claims description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
- 239000002244 precipitate Substances 0.000 claims description 10
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 9
- 238000006243 chemical reaction Methods 0.000 claims description 9
- 229910052710 silicon Inorganic materials 0.000 claims description 9
- 239000010703 silicon Substances 0.000 claims description 9
- 229940046892 lead acetate Drugs 0.000 claims description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 5
- 229910052799 carbon Inorganic materials 0.000 claims description 5
- 238000001556 precipitation Methods 0.000 claims description 5
- RKTYLMNFRDHKIL-UHFFFAOYSA-N copper;5,10,15,20-tetraphenylporphyrin-22,24-diide Chemical compound [Cu+2].C1=CC(C(=C2C=CC([N-]2)=C(C=2C=CC=CC=2)C=2C=CC(N=2)=C(C=2C=CC=CC=2)C2=CC=C3[N-]2)C=2C=CC=CC=2)=NC1=C3C1=CC=CC=C1 RKTYLMNFRDHKIL-UHFFFAOYSA-N 0.000 claims description 4
- 239000000463 material Substances 0.000 claims description 4
- 238000002441 X-ray diffraction Methods 0.000 claims description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 2
- 239000008367 deionised water Substances 0.000 claims description 2
- 229910021641 deionized water Inorganic materials 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- 239000001301 oxygen Substances 0.000 claims description 2
- 229910052760 oxygen Inorganic materials 0.000 claims description 2
- 238000003756 stirring Methods 0.000 claims description 2
- 230000007704 transition Effects 0.000 claims description 2
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims 6
- 239000012535 impurity Substances 0.000 claims 3
- 239000000047 product Substances 0.000 claims 3
- 239000013078 crystal Substances 0.000 claims 2
- 150000002611 lead compounds Chemical class 0.000 claims 2
- 235000011121 sodium hydroxide Nutrition 0.000 claims 2
- 239000000243 solution Substances 0.000 claims 2
- 239000007858 starting material Substances 0.000 claims 2
- 239000000126 substance Substances 0.000 claims 2
- 230000009466 transformation Effects 0.000 claims 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical group CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims 1
- 241000282414 Homo sapiens Species 0.000 claims 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 239000007864 aqueous solution Substances 0.000 claims 1
- 239000007795 chemical reaction product Substances 0.000 claims 1
- 238000000354 decomposition reaction Methods 0.000 claims 1
- 239000004744 fabric Substances 0.000 claims 1
- 239000000446 fuel Substances 0.000 claims 1
- RLJMLMKIBZAXJO-UHFFFAOYSA-N lead nitrate Chemical compound [O-][N+](=O)O[Pb]O[N+]([O-])=O RLJMLMKIBZAXJO-UHFFFAOYSA-N 0.000 claims 1
- 229910021514 lead(II) hydroxide Inorganic materials 0.000 claims 1
- 229910052751 metal Inorganic materials 0.000 claims 1
- 239000002184 metal Substances 0.000 claims 1
- 229910001092 metal group alloy Inorganic materials 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- 239000011734 sodium Substances 0.000 claims 1
- 238000005406 washing Methods 0.000 claims 1
- 238000001035 drying Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 241001072332 Monia Species 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000003760 magnetic stirring Methods 0.000 description 1
- 229920002120 photoresistant polymer Polymers 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J9/00—Apparatus or processes specially adapted for the manufacture, installation, removal, maintenance of electric discharge tubes, discharge lamps, or parts thereof; Recovery of material from discharge tubes or lamps
- H01J9/20—Manufacture of screens on or from which an image or pattern is formed, picked up, converted or stored; Applying coatings to the vessel
- H01J9/233—Manufacture of photoelectric screens or charge-storage screens
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G21/00—Compounds of lead
- C01G21/02—Oxides
- C01G21/06—Lead monoxide [PbO]
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
- C01P2002/76—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by a space-group or by other symmetry indications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/10—Solid density
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Computer Hardware Design (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Physics & Mathematics (AREA)
- Inorganic Chemistry (AREA)
- Microelectronics & Electronic Packaging (AREA)
- Power Engineering (AREA)
- Silicon Compounds (AREA)
- Image-Pickup Tubes, Image-Amplification Tubes, And Storage Tubes (AREA)
- Investigating Or Analysing Materials By The Use Of Chemical Reactions (AREA)
- Photoreceptors In Electrophotography (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL6500458A NL6500458A (fi) | 1965-01-15 | 1965-01-15 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE1592467A1 DE1592467A1 (de) | 1970-12-17 |
| DE1592467B2 DE1592467B2 (de) | 1974-08-08 |
| DE1592467C3 true DE1592467C3 (de) | 1975-03-27 |
Family
ID=19792119
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE1592467A Expired DE1592467C3 (de) | 1965-01-15 | 1966-01-12 | Verfahren zur Herstellung eines sehr reinen roten Bleimonoxids |
Country Status (6)
| Country | Link |
|---|---|
| US (2) | US3450496A (fi) |
| JP (2) | JPS4528055B1 (fi) |
| DE (1) | DE1592467C3 (fi) |
| FR (1) | FR1463628A (fi) |
| GB (1) | GB1080208A (fi) |
| NL (1) | NL6500458A (fi) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS518758B2 (fi) * | 1972-03-27 | 1976-03-19 | ||
| GB1509103A (en) * | 1976-05-13 | 1978-04-26 | Mizusawa Industrial Chem | Lead monoxide and process for preparation thereof |
| DE2641018C3 (de) * | 1976-09-11 | 1980-02-14 | Philips Patentverwaltung Gmbh, 2000 Hamburg | Verfahren zur Herstellung eines elektroradiographischen Aufzeichnungsmaterials |
| JPS5539603U (fi) * | 1978-09-06 | 1980-03-14 | ||
| US4220628A (en) * | 1978-10-10 | 1980-09-02 | N L Industries, Inc. | Production of lead monoxide from lead sulfate with acidic ammonium acetate |
| NZ212810A (en) * | 1984-07-27 | 1988-01-08 | Gasohol Energy Pty Ltd | Methods for producing hydrated lead oxides in the bivalent state and tri- and tetra-basic lead sulphates |
| US5252311A (en) * | 1990-04-20 | 1993-10-12 | Riman Richard E | Phase stable lead monoxide and process for the production thereof |
| EP1851807A1 (en) * | 2005-02-08 | 2007-11-07 | Koninklijke Philips Electronics N.V. | Lead oxide based photosensitive device and its manufacturing method |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL111327C (fi) * | 1957-02-26 | |||
| DE1153735B (de) * | 1960-12-31 | 1963-09-05 | Varta Ag | Verfahren zur Herstellung von Bleihydroxidoxid 5 PbOíñ2HO |
| NL290119A (fi) * | 1963-03-12 | |||
| NL290120A (fi) * | 1963-03-12 |
-
1965
- 1965-01-15 NL NL6500458A patent/NL6500458A/xx unknown
-
1966
- 1966-01-07 US US518482A patent/US3450496A/en not_active Expired - Lifetime
- 1966-01-12 GB GB1456/66A patent/GB1080208A/en not_active Expired
- 1966-01-12 DE DE1592467A patent/DE1592467C3/de not_active Expired
- 1966-01-13 JP JP1527770A patent/JPS4528055B1/ja active Pending
- 1966-01-13 JP JP41001622A patent/JPS4843559B1/ja active Pending
- 1966-01-14 FR FR45953A patent/FR1463628A/fr not_active Expired
- 1966-03-08 US US532578A patent/US3497382A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| JPS4528055B1 (fi) | 1970-09-12 |
| JPS4843559B1 (fi) | 1973-12-19 |
| US3450496A (en) | 1969-06-17 |
| DE1592467A1 (de) | 1970-12-17 |
| NL6500458A (fi) | 1966-07-18 |
| GB1080208A (en) | 1967-08-23 |
| US3497382A (en) | 1970-02-24 |
| DE1592467B2 (de) | 1974-08-08 |
| FR1463628A (fr) | 1966-12-23 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| E77 | Valid patent as to the heymanns-index 1977 | ||
| EHJ | Ceased/non-payment of the annual fee |