DE1445791A1 - Verfahren zur Herstellung chlorierter Stickstoffheterocyclen - Google Patents
Verfahren zur Herstellung chlorierter StickstoffheterocyclenInfo
- Publication number
- DE1445791A1 DE1445791A1 DE19641445791 DE1445791A DE1445791A1 DE 1445791 A1 DE1445791 A1 DE 1445791A1 DE 19641445791 DE19641445791 DE 19641445791 DE 1445791 A DE1445791 A DE 1445791A DE 1445791 A1 DE1445791 A1 DE 1445791A1
- Authority
- DE
- Germany
- Prior art keywords
- chlorine
- nitrogen heterocycles
- preparation
- heated
- chlorinated
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 8
- 238000002360 preparation method Methods 0.000 title description 2
- 238000006243 chemical reaction Methods 0.000 claims description 4
- 238000000197 pyrolysis Methods 0.000 claims description 4
- 239000011261 inert gas Substances 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 239000003960 organic solvent Substances 0.000 claims description 2
- 239000000460 chlorine Substances 0.000 description 60
- 229910052801 chlorine Inorganic materials 0.000 description 22
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 20
- IJGRMHOSHXDMSA-UHFFFAOYSA-N nitrogen Substances N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 12
- 229910052757 nitrogen Inorganic materials 0.000 description 7
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 6
- 239000001257 hydrogen Substances 0.000 description 6
- 229910052739 hydrogen Inorganic materials 0.000 description 6
- -1 aromatic isocyanide dichlorides Chemical class 0.000 description 5
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 3
- 125000001309 chloro group Chemical group Cl* 0.000 description 3
- 150000002431 hydrogen Chemical group 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 239000007858 starting material Substances 0.000 description 3
- 125000006414 CCl Chemical group ClC* 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- RLAROPIDCNCRNR-UHFFFAOYSA-N Cl.Cl.[C-]#N Chemical compound Cl.Cl.[C-]#N RLAROPIDCNCRNR-UHFFFAOYSA-N 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 230000008030 elimination Effects 0.000 description 2
- 238000003379 elimination reaction Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- TTWWZVGVBRPHLE-UHFFFAOYSA-N 1,1-dichloro-n-phenylmethanimine Chemical compound ClC(Cl)=NC1=CC=CC=C1 TTWWZVGVBRPHLE-UHFFFAOYSA-N 0.000 description 1
- RELMFMZEBKVZJC-UHFFFAOYSA-N 1,2,3-trichlorobenzene Chemical compound ClC1=CC=CC(Cl)=C1Cl RELMFMZEBKVZJC-UHFFFAOYSA-N 0.000 description 1
- OCJBOOLMMGQPQU-UHFFFAOYSA-N 1,4-dichlorobenzene Chemical compound ClC1=CC=C(Cl)C=C1 OCJBOOLMMGQPQU-UHFFFAOYSA-N 0.000 description 1
- 238000006418 Brown reaction Methods 0.000 description 1
- 101100202924 Neurospora crassa (strain ATCC 24698 / 74-OR23-1A / CBS 708.71 / DSM 1257 / FGSC 987) tsp-2 gene Proteins 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 125000004965 chloroalkyl group Chemical group 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000006482 condensation reaction Methods 0.000 description 1
- 229940117389 dichlorobenzene Drugs 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 239000004009 herbicide Substances 0.000 description 1
- 150000003949 imides Chemical class 0.000 description 1
- 239000012442 inert solvent Substances 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- JCXJVPUVTGWSNB-UHFFFAOYSA-N nitrogen dioxide Inorganic materials O=[N]=O JCXJVPUVTGWSNB-UHFFFAOYSA-N 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 238000007363 ring formation reaction Methods 0.000 description 1
- 125000001424 substituent group Chemical group 0.000 description 1
- 238000005292 vacuum distillation Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D215/00—Heterocyclic compounds containing quinoline or hydrogenated quinoline ring systems
- C07D215/02—Heterocyclic compounds containing quinoline or hydrogenated quinoline ring systems having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen atoms or carbon atoms directly attached to the ring nitrogen atom
- C07D215/16—Heterocyclic compounds containing quinoline or hydrogenated quinoline ring systems having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen atoms or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D215/18—Halogen atoms or nitro radicals
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D209/00—Heterocyclic compounds containing five-membered rings, condensed with other rings, with one nitrogen atom as the only ring hetero atom
- C07D209/02—Heterocyclic compounds containing five-membered rings, condensed with other rings, with one nitrogen atom as the only ring hetero atom condensed with one carbocyclic ring
- C07D209/04—Indoles; Hydrogenated indoles
- C07D209/30—Indoles; Hydrogenated indoles with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, directly attached to carbon atoms of the hetero ring
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH OR ROCK DRILLING; MINING
- E21B—EARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B33/00—Sealing or packing boreholes or wells
- E21B33/10—Sealing or packing boreholes or wells in the borehole
- E21B33/13—Methods or devices for cementing, for plugging holes, crevices or the like
- E21B33/14—Methods or devices for cementing, for plugging holes, crevices or the like for cementing casings into boreholes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Mining & Mineral Resources (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Geology (AREA)
- Fluid Mechanics (AREA)
- Environmental & Geological Engineering (AREA)
- Physics & Mathematics (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Indole Compounds (AREA)
- Pyrrole Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEF0044727 | 1964-12-16 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1445791A1 true DE1445791A1 (de) | 1969-03-13 |
Family
ID=7100156
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19641445791 Pending DE1445791A1 (de) | 1964-12-16 | 1964-12-16 | Verfahren zur Herstellung chlorierter Stickstoffheterocyclen |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US3335151A (enExample) |
| AT (1) | AT256121B (enExample) |
| BE (2) | BE673779A (enExample) |
| CH (1) | CH470386A (enExample) |
| DE (1) | DE1445791A1 (enExample) |
| DK (1) | DK123774B (enExample) |
| FR (1) | FR1481058A (enExample) |
| GB (1) | GB1135216A (enExample) |
| IL (1) | IL24545A (enExample) |
| NL (1) | NL6516261A (enExample) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3108873A1 (de) * | 1981-03-09 | 1982-09-16 | Basf Ag, 6700 Ludwigshafen | Dichlorchinolinderivate, ihre herstellung, ihre verwendung als herbizide und mittel dafuer |
| US4497651A (en) * | 1982-02-17 | 1985-02-05 | Basf Aktiengesellschaft | Dichloroquinoline derivatives for use as herbicides |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2661276A (en) * | 1951-01-25 | 1953-12-01 | Monsanto Chemicals | Herbicides |
| US2886568A (en) * | 1956-10-16 | 1959-05-12 | Union Carbide Corp | Preparation of quinolines |
-
0
- BE BE673999D patent/BE673999A/xx unknown
-
1964
- 1964-12-16 DE DE19641445791 patent/DE1445791A1/de active Pending
-
1965
- 1965-10-28 CH CH1486565A patent/CH470386A/de not_active IP Right Cessation
- 1965-10-31 IL IL24545A patent/IL24545A/xx unknown
- 1965-11-01 US US505963A patent/US3335151A/en not_active Expired - Lifetime
- 1965-11-12 DK DK584665AA patent/DK123774B/da unknown
- 1965-12-14 AT AT1123165A patent/AT256121B/de active
- 1965-12-14 NL NL6516261A patent/NL6516261A/xx unknown
- 1965-12-14 GB GB53060/65A patent/GB1135216A/en not_active Expired
- 1965-12-15 BE BE673779D patent/BE673779A/xx unknown
- 1965-12-16 FR FR42643A patent/FR1481058A/fr not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| AT256121B (de) | 1967-08-10 |
| GB1135216A (en) | 1968-12-04 |
| IL24545A (en) | 1969-05-28 |
| NL6516261A (enExample) | 1966-06-17 |
| FR1481058A (fr) | 1967-05-19 |
| CH470386A (de) | 1969-03-31 |
| DK123774B (da) | 1972-07-31 |
| BE673779A (enExample) | 1966-06-15 |
| US3335151A (en) | 1967-08-08 |
| BE673999A (enExample) |
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