DE1139478B - Verfahren zur Herstellung von Glykolestern der Phosphorsaeure und phosphorigen Saeure - Google Patents
Verfahren zur Herstellung von Glykolestern der Phosphorsaeure und phosphorigen SaeureInfo
- Publication number
- DE1139478B DE1139478B DEU7660A DEU0007660A DE1139478B DE 1139478 B DE1139478 B DE 1139478B DE U7660 A DEU7660 A DE U7660A DE U0007660 A DEU0007660 A DE U0007660A DE 1139478 B DE1139478 B DE 1139478B
- Authority
- DE
- Germany
- Prior art keywords
- chloro
- acid
- phosphoric acid
- mol
- reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 title claims description 32
- 229910000147 aluminium phosphate Inorganic materials 0.000 title claims description 13
- ISIJQEHRDSCQIU-UHFFFAOYSA-N tert-butyl 2,7-diazaspiro[4.5]decane-7-carboxylate Chemical compound C1N(C(=O)OC(C)(C)C)CCCC11CNCC1 ISIJQEHRDSCQIU-UHFFFAOYSA-N 0.000 title claims description 5
- 238000000034 method Methods 0.000 title claims description 4
- 150000002334 glycols Chemical class 0.000 title claims description 3
- 238000004519 manufacturing process Methods 0.000 title description 3
- 239000002253 acid Substances 0.000 claims description 10
- 229910052736 halogen Inorganic materials 0.000 claims description 9
- -1 aliphatic halogen epoxide Chemical class 0.000 claims description 7
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 5
- 125000004432 carbon atom Chemical group C* 0.000 claims description 4
- 125000001188 haloalkyl group Chemical group 0.000 claims description 4
- 125000003342 alkenyl group Chemical group 0.000 claims description 2
- 125000000217 alkyl group Chemical group 0.000 claims description 2
- 125000000262 haloalkenyl group Chemical group 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 claims description 2
- 239000000376 reactant Substances 0.000 claims description 2
- 239000000460 chlorine Substances 0.000 description 18
- 238000006243 chemical reaction Methods 0.000 description 15
- 239000011541 reaction mixture Substances 0.000 description 14
- 235000011007 phosphoric acid Nutrition 0.000 description 13
- 238000004821 distillation Methods 0.000 description 10
- BRLQWZUYTZBJKN-UHFFFAOYSA-N Epichlorohydrin Chemical compound ClCC1CO1 BRLQWZUYTZBJKN-UHFFFAOYSA-N 0.000 description 9
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 9
- 150000001875 compounds Chemical class 0.000 description 8
- 239000004593 Epoxy Substances 0.000 description 7
- 239000000243 solution Substances 0.000 description 7
- 229910052801 chlorine Inorganic materials 0.000 description 6
- 239000006260 foam Substances 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 229920000647 polyepoxide Polymers 0.000 description 4
- 229920005862 polyol Polymers 0.000 description 4
- 239000007858 starting material Substances 0.000 description 4
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 239000003063 flame retardant Substances 0.000 description 3
- 150000002367 halogens Chemical class 0.000 description 3
- 230000007935 neutral effect Effects 0.000 description 3
- 229910052698 phosphorus Inorganic materials 0.000 description 3
- 239000011574 phosphorus Substances 0.000 description 3
- 150000003077 polyols Chemical class 0.000 description 3
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 2
- SKCLYNFYASNQIL-UHFFFAOYSA-N 2-(chloromethyl)-2-ethyl-3-propyloxirane Chemical compound CCCC1OC1(CC)CCl SKCLYNFYASNQIL-UHFFFAOYSA-N 0.000 description 2
- IKNXPNNMKVOEMV-UHFFFAOYSA-N 2-butyl-3-propyloxirane Chemical compound CCCCC1OC1CCC IKNXPNNMKVOEMV-UHFFFAOYSA-N 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 125000005843 halogen group Chemical group 0.000 description 2
- 239000003999 initiator Substances 0.000 description 2
- 150000003017 phosphorus Chemical class 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 description 1
- LECYALNHBVILEC-UHFFFAOYSA-N 2,3-bis(1-chlorobutyl)oxirane Chemical compound CCCC(Cl)C1OC1C(Cl)CCC LECYALNHBVILEC-UHFFFAOYSA-N 0.000 description 1
- TTYOZMIKBYZEGL-UHFFFAOYSA-N 2,3-bis(1-chloroethyl)oxirane Chemical compound CC(Cl)C1OC1C(C)Cl TTYOZMIKBYZEGL-UHFFFAOYSA-N 0.000 description 1
- ORKJOULYBCJKFT-UHFFFAOYSA-N 2,3-bis(1-chloropropyl)oxirane Chemical compound ClC(CC)C1C(C(CC)Cl)O1 ORKJOULYBCJKFT-UHFFFAOYSA-N 0.000 description 1
- VUSYFNXNYLAECV-UHFFFAOYSA-N 2,3-bis(chloromethyl)oxirane Chemical compound ClCC1OC1CCl VUSYFNXNYLAECV-UHFFFAOYSA-N 0.000 description 1
- WQURFPNPTFZWGE-UHFFFAOYSA-N 2,3-dibutyloxirane Chemical compound CCCCC1OC1CCCC WQURFPNPTFZWGE-UHFFFAOYSA-N 0.000 description 1
- UKXROSORAUTSSH-UHFFFAOYSA-N 2-(1,2-dichloroethyl)oxirane Chemical compound ClCC(Cl)C1CO1 UKXROSORAUTSSH-UHFFFAOYSA-N 0.000 description 1
- STDUFFCKPIBQPO-UHFFFAOYSA-N 2-(1-chlorobutyl)-3-ethyloxirane Chemical compound ClC(C1C(CC)O1)CCC STDUFFCKPIBQPO-UHFFFAOYSA-N 0.000 description 1
- DQIZADWHMYXHGN-UHFFFAOYSA-N 2-(1-chlorobutyl)-3-propyloxirane Chemical compound ClC(C1C(CCC)O1)CCC DQIZADWHMYXHGN-UHFFFAOYSA-N 0.000 description 1
- RVWYSKJXNJEXQE-UHFFFAOYSA-N 2-(1-chloroethyl)-3-(1-chlorohexyl)oxirane Chemical compound ClC(C)C1C(C(CCCCC)Cl)O1 RVWYSKJXNJEXQE-UHFFFAOYSA-N 0.000 description 1
- LVZPWXWJBDPQNI-UHFFFAOYSA-N 2-(1-chloroethyl)-3-(1-chloropropyl)oxirane Chemical compound ClC(C)C1C(C(CC)Cl)O1 LVZPWXWJBDPQNI-UHFFFAOYSA-N 0.000 description 1
- NHAUMRVLSFBRBE-UHFFFAOYSA-N 2-(1-chloroethyl)-3-ethyloxirane Chemical compound CCC1OC1C(C)Cl NHAUMRVLSFBRBE-UHFFFAOYSA-N 0.000 description 1
- ZPENLTGGQAFXHN-UHFFFAOYSA-N 2-(1-chloroethyl)-3-methyloxirane Chemical compound CC(Cl)C1OC1C ZPENLTGGQAFXHN-UHFFFAOYSA-N 0.000 description 1
- VPCIBEXVZVMHNG-UHFFFAOYSA-N 2-(1-chloroethyl)-3-pentyloxirane Chemical compound ClC(C)C1C(CCCCC)O1 VPCIBEXVZVMHNG-UHFFFAOYSA-N 0.000 description 1
- ZATZNIFQGGUBOE-UHFFFAOYSA-N 2-(1-chloroethyl)-3-propyloxirane Chemical compound ClC(C)C1C(CCC)O1 ZATZNIFQGGUBOE-UHFFFAOYSA-N 0.000 description 1
- MOBNLCPBAMKACS-UHFFFAOYSA-N 2-(1-chloroethyl)oxirane Chemical compound CC(Cl)C1CO1 MOBNLCPBAMKACS-UHFFFAOYSA-N 0.000 description 1
- JSAPJQPHCHLOPE-UHFFFAOYSA-N 2-(1-chloropentyl)-3-methyloxirane Chemical compound ClC(C1C(C)O1)CCCC JSAPJQPHCHLOPE-UHFFFAOYSA-N 0.000 description 1
- BTWDUBZHKKGYSO-UHFFFAOYSA-N 2-(1-chloropropyl)-3-methyloxirane Chemical compound ClC(C1C(C)O1)CC BTWDUBZHKKGYSO-UHFFFAOYSA-N 0.000 description 1
- UPBIKILYCMODQW-UHFFFAOYSA-N 2-(1-chloropropyl)-3-pentyloxirane Chemical compound ClC(CC)C1C(CCCCC)O1 UPBIKILYCMODQW-UHFFFAOYSA-N 0.000 description 1
- SRXBOKMHGNRUSG-UHFFFAOYSA-N 2-(1-chloropropyl)-3-propyloxirane Chemical compound CCCC1OC1C(Cl)CC SRXBOKMHGNRUSG-UHFFFAOYSA-N 0.000 description 1
- VVHFXJOCUKBZFS-UHFFFAOYSA-N 2-(chloromethyl)-2-methyloxirane Chemical compound ClCC1(C)CO1 VVHFXJOCUKBZFS-UHFFFAOYSA-N 0.000 description 1
- XSVIGJOAWHFBOP-UHFFFAOYSA-N 2-(chloromethyl)-3-(1-chloropropyl)oxirane Chemical compound ClCC1C(C(CC)Cl)O1 XSVIGJOAWHFBOP-UHFFFAOYSA-N 0.000 description 1
- UVFWLQQAZYMJFB-UHFFFAOYSA-N 2-butyl-3-(1-chloroethyl)oxirane Chemical compound ClC(C)C1C(CCCC)O1 UVFWLQQAZYMJFB-UHFFFAOYSA-N 0.000 description 1
- GSTZVCRHAKCHCF-UHFFFAOYSA-N 2-heptyl-3-methyloxirane Chemical compound CCCCCCCC1OC1C GSTZVCRHAKCHCF-UHFFFAOYSA-N 0.000 description 1
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 1
- 239000004604 Blowing Agent Substances 0.000 description 1
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 1
- DKPFZGUDAPQIHT-UHFFFAOYSA-N Butyl acetate Natural products CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- QKYMMOMTGZGNAF-UHFFFAOYSA-N ClC(C)C1C(C(CCC)Cl)O1 Chemical compound ClC(C)C1C(C(CCC)Cl)O1 QKYMMOMTGZGNAF-UHFFFAOYSA-N 0.000 description 1
- QXCXKXNWODTYFX-UHFFFAOYSA-N ClC(C)C1C(CCCCCC)O1 Chemical compound ClC(C)C1C(CCCCCC)O1 QXCXKXNWODTYFX-UHFFFAOYSA-N 0.000 description 1
- JQESLVHQYLWCGN-UHFFFAOYSA-N ClC(C1C(C)O1)CCC Chemical compound ClC(C1C(C)O1)CCC JQESLVHQYLWCGN-UHFFFAOYSA-N 0.000 description 1
- ZVVZRHYEMABVRZ-UHFFFAOYSA-N ClC(C1C(C)O1)CCCCC Chemical compound ClC(C1C(C)O1)CCCCC ZVVZRHYEMABVRZ-UHFFFAOYSA-N 0.000 description 1
- YEEGLNPAVJHECH-UHFFFAOYSA-N ClC(C1C(CC)O1)CCCC Chemical compound ClC(C1C(CC)O1)CCCC YEEGLNPAVJHECH-UHFFFAOYSA-N 0.000 description 1
- LDGGSRLPRAHLBH-UHFFFAOYSA-N ClC(C1C(CC)O1)CCCCC Chemical compound ClC(C1C(CC)O1)CCCCC LDGGSRLPRAHLBH-UHFFFAOYSA-N 0.000 description 1
- AHAQERCMXHPIRR-UHFFFAOYSA-N ClC(C1C(CCC)O1)CCCC Chemical compound ClC(C1C(CCC)O1)CCCC AHAQERCMXHPIRR-UHFFFAOYSA-N 0.000 description 1
- OQJZONJARLODSA-UHFFFAOYSA-N ClC(CC)C1C(C(CCCC)Cl)O1 Chemical compound ClC(CC)C1C(C(CCCC)Cl)O1 OQJZONJARLODSA-UHFFFAOYSA-N 0.000 description 1
- XWHGDIRBGUOWBW-UHFFFAOYSA-N ClCC1C(C(CCCCC)Cl)O1 Chemical compound ClCC1C(C(CCCCC)Cl)O1 XWHGDIRBGUOWBW-UHFFFAOYSA-N 0.000 description 1
- YNPJKAKKSXIVGL-UHFFFAOYSA-N ClCC1C(C(CCCCCC)Cl)O1 Chemical compound ClCC1C(C(CCCCCC)Cl)O1 YNPJKAKKSXIVGL-UHFFFAOYSA-N 0.000 description 1
- JOYRKODLDBILNP-UHFFFAOYSA-N Ethyl urethane Chemical compound CCOC(N)=O JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- ABLZXFCXXLZCGV-UHFFFAOYSA-N Phosphorous acid Chemical compound OP(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 1
- 229910052794 bromium Inorganic materials 0.000 description 1
- 239000004566 building material Substances 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- YACLQRRMGMJLJV-UHFFFAOYSA-N chloroprene Chemical compound ClC(=C)C=C YACLQRRMGMJLJV-UHFFFAOYSA-N 0.000 description 1
- 238000006482 condensation reaction Methods 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 239000003431 cross linking reagent Substances 0.000 description 1
- 125000003700 epoxy group Chemical group 0.000 description 1
- 239000003822 epoxy resin Substances 0.000 description 1
- 239000011552 falling film Substances 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 239000003254 gasoline additive Substances 0.000 description 1
- LNEPOXFFQSENCJ-UHFFFAOYSA-N haloperidol Chemical compound C1CC(O)(C=2C=CC(Cl)=CC=2)CCN1CCCC(=O)C1=CC=C(F)C=C1 LNEPOXFFQSENCJ-UHFFFAOYSA-N 0.000 description 1
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 description 1
- 229920001519 homopolymer Polymers 0.000 description 1
- BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical compound [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000012442 inert solvent Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000002917 insecticide Substances 0.000 description 1
- 239000011810 insulating material Substances 0.000 description 1
- 229910052740 iodine Inorganic materials 0.000 description 1
- 239000011630 iodine Substances 0.000 description 1
- 239000012948 isocyanate Substances 0.000 description 1
- 150000002513 isocyanates Chemical class 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 150000002924 oxiranes Chemical class 0.000 description 1
- 125000000466 oxiranyl group Chemical group 0.000 description 1
- 230000000590 parasiticidal effect Effects 0.000 description 1
- 239000002297 parasiticide Substances 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- OJMIONKXNSYLSR-UHFFFAOYSA-N phosphorous acid Chemical compound OP(O)O OJMIONKXNSYLSR-UHFFFAOYSA-N 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 239000004848 polyfunctional curative Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 150000004756 silanes Chemical class 0.000 description 1
- 229920002050 silicone resin Polymers 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 229920002994 synthetic fiber Polymers 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- 239000000057 synthetic resin Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 150000003673 urethanes Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M1/00—Liquid compositions essentially based on mineral lubricating oils or fatty oils; Their use as lubricants
- C10M1/08—Liquid compositions essentially based on mineral lubricating oils or fatty oils; Their use as lubricants with additives
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
- A01N57/10—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds
- A01N57/12—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds containing acyclic or cycloaliphatic radicals
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/08—Esters of oxyacids of phosphorus
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/08—Esters of oxyacids of phosphorus
- C07F9/09—Esters of phosphoric acids
- C07F9/091—Esters of phosphoric acids with hydroxyalkyl compounds with further substituents on alkyl
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/08—Esters of oxyacids of phosphorus
- C07F9/141—Esters of phosphorous acids
- C07F9/1411—Esters of phosphorous acids with hydroxyalkyl compounds with further substituents on alkyl
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/48—Polyethers
- C08G18/50—Polyethers having heteroatoms other than oxygen
- C08G18/5075—Polyethers having heteroatoms other than oxygen having phosphorus
- C08G18/5078—Polyethers having heteroatoms other than oxygen having phosphorus having phosphorus bound to carbon and/or to hydrogen
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/48—Polyethers
- C08G18/50—Polyethers having heteroatoms other than oxygen
- C08G18/5075—Polyethers having heteroatoms other than oxygen having phosphorus
- C08G18/5081—Polyethers having heteroatoms other than oxygen having phosphorus having phosphorus bound to oxygen only
- C08G18/5084—Phosphate compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/67—Unsaturated compounds having active hydrogen
- C08G18/6795—Unsaturated polyethers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/40—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
- C08G59/4007—Curing agents not provided for by the groups C08G59/42 - C08G59/66
- C08G59/4071—Curing agents not provided for by the groups C08G59/42 - C08G59/66 phosphorus containing compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/49—Phosphorus-containing compounds
- C08K5/51—Phosphorus bound to oxygen
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
- C10M2223/04—Phosphate esters
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
- C10M2223/04—Phosphate esters
- C10M2223/042—Metal salts thereof
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Polymers & Plastics (AREA)
- Medicinal Chemistry (AREA)
- General Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Molecular Biology (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- General Chemical & Material Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Polyurethanes Or Polyureas (AREA)
- Epoxy Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US86034459A | 1959-12-18 | 1959-12-18 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1139478B true DE1139478B (de) | 1962-11-15 |
Family
ID=25333006
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEU7660A Pending DE1139478B (de) | 1959-12-18 | 1960-12-17 | Verfahren zur Herstellung von Glykolestern der Phosphorsaeure und phosphorigen Saeure |
Country Status (4)
| Country | Link |
|---|---|
| CH (1) | CH453320A (OSRAM) |
| DE (1) | DE1139478B (OSRAM) |
| GB (1) | GB922198A (OSRAM) |
| NL (1) | NL259180A (OSRAM) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2510034A1 (de) * | 1974-03-08 | 1975-09-18 | Philagro Sa | Fungizide zusammensetzungen |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1254150B (de) * | 1964-07-31 | 1967-11-16 | Walter Bloechl | Verfahren zur Herstellung von Fluoralkylphosphonsaeureglyzidylestern |
| GB1115043A (en) * | 1964-08-06 | 1968-05-22 | Albright & Wilson Mfg Ltd | Polyesters having improved flame retardancy and the preparation thereof |
| CN106397475B (zh) * | 2016-08-18 | 2018-06-26 | 中国林业科学研究院林产化学工业研究所 | 一种植物油基多元醇及其制备方法和应用 |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2610978A (en) * | 1949-12-02 | 1952-09-16 | Union Carbide & Carbon Corp | Production of halogen containing organic compounds of phosphorus |
| FR1032240A (fr) * | 1950-11-27 | 1953-06-30 | Bougie d'allumage avec dispositif antiparasite | |
| DE1032240B (de) * | 1956-12-19 | 1958-06-19 | Hoechst Ag | Verfahren zur Herstellung von organischen Phosphorsaeureestern durch Umsetzen von Phosphoroxychlorid oder Derivaten desselben mit Alkylenoxyden |
-
0
- NL NL259180D patent/NL259180A/xx unknown
-
1960
- 1960-12-02 GB GB4151160A patent/GB922198A/en not_active Expired
- 1960-12-09 CH CH1382160A patent/CH453320A/fr unknown
- 1960-12-17 DE DEU7660A patent/DE1139478B/de active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2610978A (en) * | 1949-12-02 | 1952-09-16 | Union Carbide & Carbon Corp | Production of halogen containing organic compounds of phosphorus |
| FR1032240A (fr) * | 1950-11-27 | 1953-06-30 | Bougie d'allumage avec dispositif antiparasite | |
| DE1032240B (de) * | 1956-12-19 | 1958-06-19 | Hoechst Ag | Verfahren zur Herstellung von organischen Phosphorsaeureestern durch Umsetzen von Phosphoroxychlorid oder Derivaten desselben mit Alkylenoxyden |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2510034A1 (de) * | 1974-03-08 | 1975-09-18 | Philagro Sa | Fungizide zusammensetzungen |
Also Published As
| Publication number | Publication date |
|---|---|
| NL259180A (OSRAM) | |
| CH453320A (fr) | 1968-06-14 |
| GB922198A (en) | 1963-03-27 |
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