DE10190479T1 - 1,3-Butylenglycol von hoher Reinheit, Verfahren zur Herstellung von 1,3-Butylenglycol und Verfahren zur Herstellung von Butanol als Nebenprodukt sowie von Butylacetat - Google Patents

1,3-Butylenglycol von hoher Reinheit, Verfahren zur Herstellung von 1,3-Butylenglycol und Verfahren zur Herstellung von Butanol als Nebenprodukt sowie von Butylacetat

Info

Publication number
DE10190479T1
DE10190479T1 DE10190479T DE10190479T DE10190479T1 DE 10190479 T1 DE10190479 T1 DE 10190479T1 DE 10190479 T DE10190479 T DE 10190479T DE 10190479 T DE10190479 T DE 10190479T DE 10190479 T1 DE10190479 T1 DE 10190479T1
Authority
DE
Germany
Prior art keywords
butylene glycol
producing
product
high purity
butyl acetate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
DE10190479T
Other languages
English (en)
Inventor
Yasuo Tsuji
Hiroaki Uenakai
Hiroshi Koyama
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Daicel Corp
Original Assignee
Daicel Chemical Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from JP2000027033A external-priority patent/JP4530461B2/ja
Priority claimed from JP2000027031A external-priority patent/JP2001213824A/ja
Priority claimed from JP2000027037A external-priority patent/JP4397495B2/ja
Priority claimed from JP2000027039A external-priority patent/JP2001213825A/ja
Priority claimed from JP2000027026A external-priority patent/JP2001213823A/ja
Application filed by Daicel Chemical Industries Ltd filed Critical Daicel Chemical Industries Ltd
Publication of DE10190479T1 publication Critical patent/DE10190479T1/de
Ceased legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/18—Polyhydroxylic acyclic alcohols
    • C07C31/20—Dihydroxylic alcohols
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
    • C07C29/14—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of a —CHO group
    • C07C29/141—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of a —CHO group with hydrogen or hydrogen-containing gases
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
DE10190479T 2000-02-04 2001-02-02 1,3-Butylenglycol von hoher Reinheit, Verfahren zur Herstellung von 1,3-Butylenglycol und Verfahren zur Herstellung von Butanol als Nebenprodukt sowie von Butylacetat Ceased DE10190479T1 (de)

Applications Claiming Priority (7)

Application Number Priority Date Filing Date Title
JP2000027033A JP4530461B2 (ja) 2000-02-04 2000-02-04 １，３−ブチレングリコールの精製方法
JP2000027031A JP2001213824A (ja) 2000-02-04 2000-02-04 精製１，３−ブチレングリコールの製造方法
JP2000027037A JP4397495B2 (ja) 2000-02-04 2000-02-04 １，３−ブチレングリコールの製造方法
JP2000027039A JP2001213825A (ja) 2000-02-04 2000-02-04 高純度１，３−ブチレングリコール
JP2000027026A JP2001213823A (ja) 2000-02-04 2000-02-04 副生ブタノール及び酢酸ブチルの製造方法
JP2000027028 2000-02-04
PCT/JP2001/000771 WO2001056963A1 (en) 2000-02-04 2001-02-02 High-purity 1,3-butylene glycol, process for producing 1,3-butylene glycol, and process for producing by-product butanol and butyl acetate

Publications (1)

Publication Number Publication Date
DE10190479T1 true DE10190479T1 (de) 2002-05-08

Family

ID=27554720

Family Applications (1)

Application Number Title Priority Date Filing Date
DE10190479T Ceased DE10190479T1 (de) 2000-02-04 2001-02-02 1,3-Butylenglycol von hoher Reinheit, Verfahren zur Herstellung von 1,3-Butylenglycol und Verfahren zur Herstellung von Butanol als Nebenprodukt sowie von Butylacetat

Country Status (4)

Country Link
US (1) US6900360B2 (de)
KR (1) KR20010102420A (de)
DE (1) DE10190479T1 (de)
WO (1) WO2001056963A1 (de)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2003096006A (ja) * 2001-09-26 2003-04-03 Kyowa Yuka Co Ltd １，３−ブチレングリコールおよびその製造方法
KR20030088211A (ko) * 2002-05-13 2003-11-19 재원산업 주식회사 노말 부탄올 정제방법
KR20030088212A (ko) * 2002-05-13 2003-11-19 재원산업 주식회사 메탄올 및 올쏘자이렌의 정제방법
US20050154239A1 (en) * 2004-01-08 2005-07-14 Windhorst Kenneth A. Methods for preparing 1,3 butylene glycol
US8445733B1 (en) 2011-07-26 2013-05-21 Oxea Bishop Llc 1,3 butylene glycol with reduced odor
CA2927166C (en) 2013-10-23 2021-12-28 Basf Se Method for preparing 1,4-butanediol having an apha color index of less than 30
WO2016130547A1 (en) * 2015-02-11 2016-08-18 Hulu, LLC Relevance table aggregation in a database system
CN105585448B (zh) * 2016-03-09 2019-11-05 辽宁科隆精细化工股份有限公司 一种合成化妆品级1,3-丁二醇的方法
TWI787215B (zh) 2016-11-22 2022-12-21 美商Ｗ Ｒ 康格雷氏公司 降低損耗的催化劑及其製造方法
KR20190023466A (ko) 2017-08-29 2019-03-08 한국화학연구원 고순도의 1,3-부탄디올 및 그 제조방법
CN108383684B (zh) * 2018-03-28 2021-07-30 中国科学院兰州化学物理研究所苏州研究院 一种1，3-丁二醇的合成方法及系统
CN110790634B (zh) * 2019-10-14 2022-07-12 万华化学集团股份有限公司 一种1，3-丁二醇的制备方法
JP7380161B2 (ja) * 2019-12-09 2023-11-15 株式会社レゾナック パラアルドールの製造方法
JP7380181B2 (ja) * 2019-12-20 2023-11-15 株式会社レゾナック パラアルドールの製造方法
WO2021132368A1 (ja) * 2019-12-28 2021-07-01 株式会社ダイセル １，３－ブチレングリコールの製造方法
CN112778082B (zh) * 2021-01-15 2022-07-12 万华化学集团股份有限公司 一种乙醛缩合制备1,3-丁二醇的方法
JP7086254B1 (ja) 2021-06-04 2022-06-17 Ｋｈネオケム株式会社 製品１，３－ブチレングリコール
WO2023201205A2 (en) * 2022-04-11 2023-10-19 Genomatica, Inc. Neutral taste 1,3-butylene glycol products and compositions thereof
WO2024086005A1 (en) 2022-10-17 2024-04-25 Oq Chemmicals Bishop Llc Improved 1,3-butylene glycol process

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB853266A (en) 1956-02-24 1960-11-02 Celanese Corp 1,3-butylene glycol
US3489655A (en) * 1967-12-26 1970-01-13 Celanese Corp Method of decreasing the odor of 1,3-butylene glycol
JPS6165834A (ja) 1984-09-07 1986-04-04 Daicel Chem Ind Ltd １，３−ブチレングリコ−ルの精製法
JPS62212384A (ja) 1986-03-13 1987-09-18 Daicel Chem Ind Ltd パラアルド−ルの製造方法
JPS62246529A (ja) 1986-03-24 1987-10-27 Daicel Chem Ind Ltd １，３−ブチレングリコ−ルの製造方法
US4768512A (en) 1986-05-13 1988-09-06 Mieczyslaw Mirowski Cardioverting system and method with high-frequency pulse delivery
JPH07116081B2 (ja) 1986-12-22 1995-12-13 ダイセル化学工業株式会社 １，３−ブチレングリコ−ルの精製法
DE69320454T3 (de) * 1993-03-24 2009-08-20 Daicel Chemical Industries, Ltd. Verfahren zur Herstellung von 1,3-butylenglykol
JP3369707B2 (ja) 1994-03-17 2003-01-20 ダイセル化学工業株式会社 １，３−ブチレングリコ−ルの精製方法
JP3016727B2 (ja) * 1996-02-27 2000-03-06 大▲連▼化學工業股▲分▼有限公司 改質ラニーニッケル触媒とその触媒によるジオール化合物の製造方法
BE1014031A3 (fr) * 1997-07-04 2003-03-04 Basf Ag La preparation d'esters.
JP4559625B2 (ja) 1998-08-07 2010-10-13 ダイセル化学工業株式会社 高純度１，３−ブチレングリコール及びその製造方法

Also Published As

Publication number Publication date
KR20010102420A (ko) 2001-11-15
US6900360B2 (en) 2005-05-31
WO2001056963A1 (en) 2001-08-09
US20030018224A1 (en) 2003-01-23

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