CY1107234T1 - Μεθοδος για ενζυμικη διασπαση ελαιων και λιπων - Google Patents

Μεθοδος για ενζυμικη διασπαση ελαιων και λιπων

Info

Publication number
CY1107234T1
CY1107234T1 CY20081100264T CY081100264T CY1107234T1 CY 1107234 T1 CY1107234 T1 CY 1107234T1 CY 20081100264 T CY20081100264 T CY 20081100264T CY 081100264 T CY081100264 T CY 081100264T CY 1107234 T1 CY1107234 T1 CY 1107234T1
Authority
CY
Cyprus
Prior art keywords
fat
oil
fatty acids
separator
glycerol
Prior art date
Application number
CY20081100264T
Other languages
English (en)
Inventor
Karlheinz Dr Brunner
Rainer Dr Frische
Dirk Dr Kilian
Original Assignee
T + T Oleochemie Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by T + T Oleochemie Gmbh filed Critical T + T Oleochemie Gmbh
Publication of CY1107234T1 publication Critical patent/CY1107234T1/el

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/64—Fats; Fatty oils; Ester-type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
    • C12P7/6409—Fatty acids
    • C12P7/6418—Fatty acids by hydrolysis of fatty acid esters
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
    • C11C1/007—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids using organic solvents
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C1/00—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids
    • C11C1/02—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids from fats or fatty oils
    • C11C1/04—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids from fats or fatty oils by hydrolysis
    • C11C1/045—Preparation of fatty acids from fats, fatty oils, or waxes; Refining the fatty acids from fats or fatty oils by hydrolysis using enzymes or microorganisms, living or dead
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/003—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/04—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fats or fatty oils
    • C11C3/10—Ester interchange
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/02—Preparation of oxygen-containing organic compounds containing a hydroxy group
    • C12P7/04—Preparation of oxygen-containing organic compounds containing a hydroxy group acyclic
    • C12P7/18—Preparation of oxygen-containing organic compounds containing a hydroxy group acyclic polyhydric
    • C12P7/20—Glycerol
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/62—Carboxylic acid esters
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/64—Fats; Fatty oils; Ester-type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
    • C12P7/6436—Fatty acid esters
    • C12P7/6445—Glycerides
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/64—Fats; Fatty oils; Ester-type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
    • C12P7/6436—Fatty acid esters
    • C12P7/6445—Glycerides
    • C12P7/6454—Glycerides by esterification

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Biochemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Biotechnology (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Fats And Perfumes (AREA)
  • Apparatus Associated With Microorganisms And Enzymes (AREA)

Abstract

Μέθοδος για ενζυμική διάσπαση ελαίων και λιπών για την παραλαβή λιπαρών οξέων και γλυκερίνης με χρήση λιπασών σε ένα μείγμα, το οποίο περιέχει έλαιο ή λίπος και νερό, όπου η αντίδραση διάσπασης διεξάγεται μόνο έως κάποιο βαθμό διάσπασης, όπου για το χρησιμοποιούμενο μείγμα η επιβράδυνση της αντίδρασης διάσπασης βρίσκεται κάτω από μία προκαθορισμένη τιμή, τα προς παραλαβή λιπαρά οξέα διαχωρίζονται από το μερικώς διασπασμένο μείγμα της αντίδρασης, διαχωρίζοντας αρχικά την περιέχουσα γλυκερίνη υδατική φάση, η οποία σχηματίζεται κατά τη διαδικασία διάσπασης, από την μερικώς διασπασμένη οργανική φάση με τα αποχωρισμένα λιπαρά οξέα σε έναν αυτόματης εκκένωσης διαχωριστήρα με δίσκους και στη συνέχεια διαχωρίζοντας τα λιπαρά οξέα από την μερικώς διασπασμένη οργανική φάση, και το απαλλαγμένο από τα ελεύθερα οργανικά οξέα παραμένον υπόλειμμα της οργανικής φάσης επιστρέφει πάλι στη διαδικασία διάσπασης, όπου η διάσπαση των λιπών διεξάγεται ασυνεχώς σε αντιδραστήρες διάσπασης, οι οποίοι λειτουργούν με σύστημα ανακύκλωσης με κυκλοφορία του περιεχομένου του αντιδραστήρα και προβλέπονται περισσότεροι αντιδραστήρες παράλληλα για μια ενός ή περισσότερων σταδίων διάσπαση λιπών.
CY20081100264T 2001-06-21 2008-03-07 Μεθοδος για ενζυμικη διασπαση ελαιων και λιπων CY1107234T1 (el)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
EP01115081A EP1270734B1 (de) 2001-06-21 2001-06-21 Verfahren zur enzymatischen Spaltung von Ölen und Fetten

Publications (1)

Publication Number Publication Date
CY1107234T1 true CY1107234T1 (el) 2012-11-21

Family

ID=8177782

Family Applications (1)

Application Number Title Priority Date Filing Date
CY20081100264T CY1107234T1 (el) 2001-06-21 2008-03-07 Μεθοδος για ενζυμικη διασπαση ελαιων και λιπων

Country Status (14)

Country Link
US (2) US20070077635A1 (el)
EP (2) EP1270734B1 (el)
JP (2) JP4222937B2 (el)
CN (1) CN1518600A (el)
AT (2) ATE380877T1 (el)
AU (1) AU2002314131B2 (el)
CA (1) CA2451372A1 (el)
CY (1) CY1107234T1 (el)
DE (3) DE50113375D1 (el)
DK (1) DK1270734T3 (el)
ES (1) ES2298178T3 (el)
PT (1) PT1270734E (el)
WO (1) WO2003010323A1 (el)
ZA (1) ZA200309779B (el)

Families Citing this family (36)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8250357B2 (en) 2000-09-13 2012-08-21 Fortinet, Inc. Tunnel interface for securing traffic over a network
DK1270734T3 (da) * 2001-06-21 2008-05-05 T & T Oleochemie Gmbh Fremgangsmåde til enzymatisk spaltning af olier og fedtstoffer
US7181547B1 (en) 2001-06-28 2007-02-20 Fortinet, Inc. Identifying nodes in a ring network
DE10161274A1 (de) * 2001-12-13 2003-06-26 Cognis Deutschland Gmbh Verfahren zur Herstellung von C4-C12-Fettsäuren
US7203192B2 (en) 2002-06-04 2007-04-10 Fortinet, Inc. Network packet steering
US7161904B2 (en) 2002-06-04 2007-01-09 Fortinet, Inc. System and method for hierarchical metering in a virtual router based network switch
US7177311B1 (en) 2002-06-04 2007-02-13 Fortinet, Inc. System and method for routing traffic through a virtual router-based network switch
US7096383B2 (en) 2002-08-29 2006-08-22 Cosine Communications, Inc. System and method for virtual router failover in a network routing system
US7266120B2 (en) 2002-11-18 2007-09-04 Fortinet, Inc. System and method for hardware accelerated packet multicast in a virtual routing system
US7720095B2 (en) 2003-08-27 2010-05-18 Fortinet, Inc. Heterogeneous media packet bridging
WO2005072477A2 (en) * 2004-01-26 2005-08-11 Martek Biosciences Corporation Method for the separation of phospholipids from phospholipid-containing materials
US7499419B2 (en) 2004-09-24 2009-03-03 Fortinet, Inc. Scalable IP-services enabled multicast forwarding with efficient resource utilization
DE102005002711A1 (de) * 2005-01-19 2006-07-27 Cognis Deutschland Gmbh & Co. Kg Herstellung und Verwendung von Monoglyceriden
JP4719476B2 (ja) * 2005-02-04 2011-07-06 花王株式会社 油脂の加水分解方法
AU2015202786A1 (en) * 2006-07-19 2015-06-11 Nazzareno De Angelis Integrated process for the production of biofuels from different types of starting materials and related products
ITRM20060377A1 (it) * 2006-07-19 2008-01-20 Angelis Nazzareno De Procedimento integrato per la produzione di biocombustibili e biocarburanti da diverse tipologie di materie prime e relativi prodotti
CN101657543A (zh) 2007-04-11 2010-02-24 诺维信公司 用于产生生物柴油的方法
GB0807619D0 (en) * 2008-04-28 2008-06-04 Whitton Peter A Production of bio fuels from plant tissue culture sources
CN101381614B (zh) * 2008-10-17 2012-02-08 清华大学 一种回收非固定化脂肪酶催化油脂制备生物柴油工艺
FR2942628B1 (fr) * 2009-03-02 2011-07-01 Arkema France Procede de production d'ester d'acide ricinoleique par transesterification enzymatique selective
CN102510897B (zh) 2009-08-13 2013-07-17 科学与工业研究委员会 生产脂肪酸的方法
EP2298727B1 (de) * 2009-09-05 2015-03-04 Cognis IP Management GmbH Verfahren zur Herstellung von Estern kurzkettiger Alkohole aus triglyceridreichen Ölen
US9040263B2 (en) 2010-07-28 2015-05-26 Butamax Advanced Biofuels Llc Production of alcohol esters and in situ product removal during alcohol fermentation
AU2011268220B2 (en) 2010-06-18 2015-01-29 Butamax(Tm) Advanced Biofuels Llc Extraction solvents derived from oil for alcohol removal in extractive fermentation
US20140335580A1 (en) * 2011-09-21 2014-11-13 Board Of Supervisors Of Lousiana State University And Agricultural And Mechanical College Method for Enrichment of Eicosapentaenoic Acid and Docosahexaenoic Acid in Source Oils
SG11201404463PA (en) * 2012-01-30 2014-10-30 Arvind Mallinath Lali Enzymatic process for fat and oil hydrolysis
US9499768B2 (en) 2012-09-07 2016-11-22 Aak Ab (Publ) Method for processing a vegetable fat composition
US8927796B2 (en) * 2012-09-13 2015-01-06 Chevron U.S.A. Inc. Base oil upgrading by co-feeding a ketone or beta-keto-ester feedstock
US11053184B2 (en) * 2013-03-07 2021-07-06 Genomatica, Inc. Downstream processing of fatty alcohol compositions produced by recombinant host cells
KR101511744B1 (ko) * 2014-04-28 2015-04-22 티케이엘 주식회사 효소순환공정을 이용한 세틸화된 지방산 복합물의 생산장치
EP3266857B1 (de) * 2016-07-08 2020-01-01 L'air Liquide, Société Anonyme Pour L'Étude Et L'exploitation Des Procédés Georges Claude Verfahren zum herstellen von fettsäuren durch hydrolytische esterspaltung in wasser bei hohen temperatur
JP6990019B2 (ja) * 2016-10-26 2022-01-12 花王株式会社 脂肪酸類の製造方法
US11643606B2 (en) 2018-12-31 2023-05-09 Neste Oyj Method for producing renewable base oil and renewable fuel components
US11111203B2 (en) 2019-04-04 2021-09-07 Lg Chem, Ltd. System and method for manufacturing ester-based composition
WO2020204555A1 (ko) * 2019-04-04 2020-10-08 주식회사 엘지화학 에스터계 조성물의 제조 시스템 및 방법
WO2024041562A1 (en) * 2022-08-24 2024-02-29 Novozymes A/S Improved enzymatic splitting of oils and fats to produce free fatty acid

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2299090A1 (fr) * 1975-02-01 1976-08-27 Westfalia Separator Ag Bol sep
US4035402A (en) * 1975-03-17 1977-07-12 The Procter & Gamble Company Dewaxing process for vegetable oils
JPS635787Y2 (el) * 1981-12-11 1988-02-17
JPS61149098A (ja) * 1984-12-25 1986-07-07 Meito Sangyo Kk アルカリ油滓からの脂肪酸の製造法
JPH0695950B2 (ja) * 1985-08-29 1994-11-30 吉川製油株式会社 脂肪酸エステル類の製造法
DE3672270D1 (de) * 1985-03-06 1990-08-02 Yoshikawa Oil & Fat Verfahren zur herstellung von fettsaeureestern.
US5219733A (en) * 1985-03-06 1993-06-15 Yoshikawa Oil & Fat Co., Ltd. Process for preparing fatty acid esters
JPH0716425B2 (ja) * 1987-05-20 1995-03-01 花王株式会社 油脂類のエステル交換反応方法
JPH0213389A (ja) * 1988-06-30 1990-01-17 Ito Seiyu Kk ひまし油の高加水分解方法
ATE181745T1 (de) * 1994-08-16 1999-07-15 Frische Gmbh Verfahren zur gewinnung von nicht wasserlöslichen, nativen produkten aus nativen stoffgemengen mit hilfe der zentrifugalkraft
DE19922882C2 (de) * 1999-05-19 2001-03-15 Cognis Deutschland Gmbh Verfahren zur Herstellung von Fettsäuren und Glycerin
JP2001054396A (ja) * 1999-06-08 2001-02-27 Nippon Suisan Kaisha Ltd リパーゼによる高度不飽和脂肪酸含有油脂の製造方法
DK1270734T3 (da) * 2001-06-21 2008-05-05 T & T Oleochemie Gmbh Fremgangsmåde til enzymatisk spaltning af olier og fedtstoffer

Also Published As

Publication number Publication date
JP2003064394A (ja) 2003-03-05
EP1402044B1 (de) 2009-08-12
ATE380877T1 (de) 2007-12-15
US6933139B2 (en) 2005-08-23
US20070077635A1 (en) 2007-04-05
ATE439450T1 (de) 2009-08-15
PT1270734E (pt) 2008-03-24
DE50213766D1 (de) 2009-09-24
US20020197687A1 (en) 2002-12-26
ES2298178T3 (es) 2008-05-16
EP1402044A1 (de) 2004-03-31
ZA200309779B (en) 2006-08-30
WO2003010323A1 (de) 2003-02-06
AU2002314131B2 (en) 2007-11-01
JP2004535821A (ja) 2004-12-02
EP1270734A1 (de) 2003-01-02
EP1270734B1 (de) 2007-12-12
JP4222937B2 (ja) 2009-02-12
DK1270734T3 (da) 2008-05-05
JP4038398B2 (ja) 2008-01-23
DE50113375D1 (de) 2008-01-24
DE10156584A1 (de) 2003-01-09
CA2451372A1 (en) 2003-02-06
CN1518600A (zh) 2004-08-04

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