CN1174546A - 生产2,6－二氟苄腈的无溶剂方法 - Google Patents

生产2,6－二氟苄腈的无溶剂方法 Download PDF

Info

Publication number
CN1174546A
CN1174546A CN95197478A CN95197478A CN1174546A CN 1174546 A CN1174546 A CN 1174546A CN 95197478 A CN95197478 A CN 95197478A CN 95197478 A CN95197478 A CN 95197478A CN 1174546 A CN1174546 A CN 1174546A
Authority
CN
China
Prior art keywords
benzonitrile
mixture
fluoride
reaction
tar
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN95197478A
Other languages
English (en)
Chinese (zh)
Inventor
M·W·泽特勒
R·E·托贝
R·B·兰格
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Corteva Agriscience LLC
Original Assignee
DowElanco LLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by DowElanco LLC filed Critical DowElanco LLC
Publication of CN1174546A publication Critical patent/CN1174546A/zh
Pending legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/30—Preparation of carboxylic acid nitriles by reactions not involving the formation of cyano groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Saccharide Compounds (AREA)
CN95197478A 1994-12-28 1995-11-17 生产2,6－二氟苄腈的无溶剂方法 Pending CN1174546A (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US08/365,726 1994-12-28
US08/365,726 US5502235A (en) 1994-12-28 1994-12-28 Solventless process for making 2,6 difluorobenzonitrile

Publications (1)

Publication Number Publication Date
CN1174546A true CN1174546A (zh) 1998-02-25

Family

ID=23440092

Family Applications (1)

Application Number Title Priority Date Filing Date
CN95197478A Pending CN1174546A (zh) 1994-12-28 1995-11-17 生产2,6－二氟苄腈的无溶剂方法

Country Status (18)

Country Link
US (1) US5502235A (en:Method)
EP (1) EP0800506B1 (en:Method)
JP (1) JPH10511941A (en:Method)
CN (1) CN1174546A (en:Method)
AR (1) AR000556A1 (en:Method)
AT (1) ATE187959T1 (en:Method)
AU (1) AU702641B2 (en:Method)
BR (1) BR9510428A (en:Method)
CA (1) CA2209141A1 (en:Method)
DE (1) DE69514122T2 (en:Method)
DK (1) DK0800506T3 (en:Method)
ES (1) ES2139951T3 (en:Method)
FI (1) FI972742A7 (en:Method)
HU (1) HU215936B (en:Method)
IL (1) IL116634A (en:Method)
TW (1) TW307748B (en:Method)
WO (1) WO1996020168A1 (en:Method)
ZA (1) ZA9510902B (en:Method)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103044388A (zh) * 2011-10-17 2013-04-17 张家港市国泰华荣化工新材料有限公司 一种3,4—二氟环丁砜的制备方法
CN112939782A (zh) * 2019-12-11 2021-06-11 浙江华晶氟化学科技有限公司 一种含氟芳基化合物的制备方法
CN113024414A (zh) * 2021-03-23 2021-06-25 江苏合泰新材料科技有限公司 一种高效合成含氟化合物的方法

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ATE204843T1 (de) * 1995-06-20 2001-09-15 Nippon Soda Co 2,3-dihalogen-6-trifluormethylbenzol-derivate und verfahren zu ihrer herstellung
DE19702282C2 (de) * 1997-01-23 1998-11-19 Hoechst Ag Katalysator für Halex-Reaktionen
CN100545133C (zh) * 2001-05-17 2009-09-30 罗狄亚化学公司 离子性质的组合物作为取代试剂的用途,由氟化试剂构成的组合物及其使用方法
DE10227223A1 (de) * 2002-06-18 2004-01-08 Kühlein, Klaus, Prof.Dr. Verfahren zur Herstellung substituierter organischer Verbindungen und Verwendung von Katalysatoren für Substitutionsreaktionen
CN104387289B (zh) * 2014-10-30 2017-09-01 天津河清化学工业有限公司 二氟苯腈生产中降低催化剂用量的方法

Family Cites Families (29)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB995927A (en) * 1962-10-23 1965-06-23 Imp Smelting Corp Ltd Fluorination of perhalo compounds
NL302228A (en:Method) * 1962-12-20
NL129620C (en:Method) * 1963-04-01
US4051168A (en) * 1976-05-12 1977-09-27 E. I. Du Pont De Nemours And Company Fluorination process
US4229365A (en) * 1977-05-28 1980-10-21 Basf Aktiengesellschaft Manufacture of substituted fluorobenzenes
DE2803259A1 (de) * 1978-01-26 1979-08-02 Basf Ag Verfahren zur herstellung von fluorbenzolen
DE2902877C2 (de) * 1978-01-28 1983-05-05 I.S.C. Chemicals Ltd., London Verfahren zur Herstellung eines Fluorbenzomononitrils
DE2938939A1 (de) * 1978-10-05 1980-04-17 Boots Co Ltd Verfahren zur herstellung von fluornitrobenzolen
US4174349A (en) * 1978-10-30 1979-11-13 Allied Chemical Corporation Preparation of fluoroorganic compounds with calcium fluoride
FR2490634A1 (fr) * 1980-09-25 1982-03-26 Rhone Poulenc Ind Procede de preparation de fluorobenzonitriles
JPS57197226A (en) * 1981-05-30 1982-12-03 Dainippon Ink & Chem Inc Preparation of aromatic fluorine compound
EP0073372B1 (en) * 1981-08-31 1984-08-01 Ishihara Sangyo Kaisha, Ltd. Process for producing 2,6-difluorobenzonitrile
EP0120575B1 (en) * 1983-02-18 1989-06-14 Nippon Shokubai Kagaku Kogyo Co., Ltd Organic fluorine compounds
JPS604159A (ja) * 1983-06-23 1985-01-10 Ishihara Sangyo Kaisha Ltd フルオロベンゾニトリル系化合物の製造方法
US4704483A (en) * 1984-04-27 1987-11-03 Occidental Chemical Corporation 3,4-difluoro-5-nitrobenzotrifluoride and preparation of fluoro-nitro-benzotrifluorides
US4952719A (en) * 1984-10-15 1990-08-28 Occidental Chemical Corporation Process for the preparation of halo aromatic compounds
GB8500180D0 (en) * 1985-01-04 1985-02-13 Ici Plc Chemical process
US4680406A (en) * 1985-10-15 1987-07-14 The Dow Chemical Company Process for fluorinating halogenated organo-compounds
JPS62114939A (ja) * 1985-11-14 1987-05-26 Sumitomo Chem Co Ltd フルオロベンゼン誘導体の製造法
US4642398A (en) * 1986-01-06 1987-02-10 Mallinckrodt, Inc. Preparation of fluoronitrobenzene compounds in dispersion of potassium fluoride
US4927980A (en) * 1986-01-06 1990-05-22 Mallinckrodt Inc. Catalytic method for producing fluoroaromatic compounds using branched alkyl pyridinium salts
US4849552A (en) * 1986-01-06 1989-07-18 Mallinckrodt, Inc. Preparation of fluoroaromatic compounds in dispersion of potassium fluoride
DE3681033D1 (de) * 1986-01-06 1991-09-26 Mallinckrodt Inc Katalytisches verfahren zur herstellung von fluoraomatischen verbindungen mittels n-sek-alkylpyridiniumsalze.
DE3642326A1 (de) * 1986-12-11 1988-06-23 Bayer Ag Verfahren zur gewinnung von substituierten fluorbenzolen
US4973772A (en) * 1987-02-07 1990-11-27 Mallinckrodt, Inc. Catalytic method for producing fluoroarmatic compounds using substituted pyridinium salts
JP2577567B2 (ja) * 1987-07-07 1997-02-05 イハラケミカル工業株式会社 芳香族フッ素化合物の製造方法
DE3827436A1 (de) * 1988-08-12 1990-02-15 Bayer Ag Verfahren zum einfuehren von fluoratomen an aromatische kerne durch nucleophilen austausch
US5545768A (en) * 1990-06-25 1996-08-13 Hoechet Ag Process for the preparation of chlorofluronitrobenzenes and difluoronitrobenzenes
DE59407426D1 (de) * 1993-07-21 1999-01-21 Clariant Gmbh Verfahren zur Herstellung von Fluorbenzonitrilen

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103044388A (zh) * 2011-10-17 2013-04-17 张家港市国泰华荣化工新材料有限公司 一种3,4—二氟环丁砜的制备方法
CN103044388B (zh) * 2011-10-17 2015-04-15 张家港市国泰华荣化工新材料有限公司 一种3,4—二氟环丁砜的制备方法
CN112939782A (zh) * 2019-12-11 2021-06-11 浙江华晶氟化学科技有限公司 一种含氟芳基化合物的制备方法
CN112939782B (zh) * 2019-12-11 2022-09-30 兰州康鹏威耳化工有限公司 一种含氟芳基化合物的制备方法
CN113024414A (zh) * 2021-03-23 2021-06-25 江苏合泰新材料科技有限公司 一种高效合成含氟化合物的方法

Also Published As

Publication number Publication date
EP0800506A1 (en) 1997-10-15
TW307748B (en:Method) 1997-06-11
HUT77239A (hu) 1998-03-02
ATE187959T1 (de) 2000-01-15
DK0800506T3 (da) 2000-05-15
BR9510428A (pt) 1998-07-07
AU702641B2 (en) 1999-02-25
HU215936B (hu) 1999-03-29
FI972742A0 (fi) 1997-06-25
FI972742L (fi) 1997-08-27
WO1996020168A1 (en) 1996-07-04
FI972742A7 (fi) 1997-08-27
IL116634A (en) 2003-04-10
US5502235A (en) 1996-03-26
IL116634A0 (en) 1996-03-31
DE69514122D1 (de) 2000-01-27
JPH10511941A (ja) 1998-11-17
ZA9510902B (en) 1997-06-23
AR000556A1 (es) 1997-07-10
DE69514122T2 (de) 2000-04-20
AU4164596A (en) 1996-07-19
CA2209141A1 (en) 1996-07-04
ES2139951T3 (es) 2000-02-16
EP0800506B1 (en) 1999-12-22

Similar Documents

Publication Publication Date Title
CN1147484C (zh) 制备支链羧酸的缩水甘油酯的方法
CN1286788C (zh) 2,2,2－三氟乙醇的制造方法
CN1974511A (zh) 用于生产有机化合物的方法
CN1827592A (zh) 制备环己酮肟的方法
CN101184715B (zh) 一种由甘油和盐酸生产α，γ-二氯丙醇的生产方法
CN1191229C (zh) 制备4－氨基二苯基胺的方法
JP5668319B2 (ja) ２，２−ビス（４−ヒドロキシフェニル）ヘキサフルオロプロパンの製造方法
CN112390748B (zh) 一种2-氰基-3-氟-5-三氟甲基吡啶的制备方法
CN1174546A (zh) 生产2,6－二氟苄腈的无溶剂方法
CN101663286B (zh) 四缩水甘油氨基化合物的制备方法
JP5585445B2 (ja) ラウロラクタムの製造方法
EP1542957B9 (en) Process for preparing fluorocarboxylic acids
CN1437582A (zh) 提纯内酰胺的方法
CN1956941A (zh) 制备1,3－二溴丙酮、1,3－二氯丙酮和表氯醇的方法
CN1653029A (zh) 高纯度(氟烷基)苯衍生物及其制备方法
CN1793114A (zh) 环己酮肟的制备方法
CN1182110C (zh) 制备二苯醚化合物的方法
CN1196665C (zh) 5－[(4－氯苯基)甲基]－2,2－二甲基环戊酮的制备方法
CN1074410C (zh) 制备4,6－二氨基间苯二酚的方法
CN1174948C (zh) 制备全氟乙烷的方法
CN1053800A (zh) 具中性或官能端基和受控分子量的氟代聚醚和全氟聚醚的制备方法
CN1561319A (zh) 六氟乙烷的制备方法及其使用
JP2017521386A (ja) （ｓ）−２−アセチルオキシプロピオン酸およびその誘導体の製造方法
CN1077095C (zh) 对氟苯酚的制备方法
CN118479959B (zh) 一种1,2-二甲氧基-1,1,2,2-四氟乙烷的制备方法

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C02 Deemed withdrawal of patent application after publication (patent law 2001)
WD01 Invention patent application deemed withdrawn after publication