CN1169743A - 丙烯-乙烯共聚物组合物及其制备方法 - Google Patents
丙烯-乙烯共聚物组合物及其制备方法 Download PDFInfo
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- CN1169743A CN1169743A CN96191163A CN96191163A CN1169743A CN 1169743 A CN1169743 A CN 1169743A CN 96191163 A CN96191163 A CN 96191163A CN 96191163 A CN96191163 A CN 96191163A CN 1169743 A CN1169743 A CN 1169743A
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- Prior art keywords
- acid
- propylene
- dihydro
- oxy
- hydroxyl
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- 238000000034 method Methods 0.000 title claims description 84
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- 230000008569 process Effects 0.000 title description 2
- 238000006116 polymerization reaction Methods 0.000 claims abstract description 92
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- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 claims abstract description 41
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 claims abstract description 41
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims abstract description 36
- RFFLAFLAYFXFSW-UHFFFAOYSA-N 1,2-dichlorobenzene Chemical compound ClC1=CC=CC=C1Cl RFFLAFLAYFXFSW-UHFFFAOYSA-N 0.000 claims abstract description 30
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- 239000001257 hydrogen Substances 0.000 claims abstract description 21
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract description 21
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- 239000005977 Ethylene Substances 0.000 claims abstract description 19
- 239000000155 melt Substances 0.000 claims abstract description 18
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- 238000009826 distribution Methods 0.000 claims abstract description 10
- -1 amide compound Chemical class 0.000 claims description 299
- 150000001875 compounds Chemical class 0.000 claims description 262
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- 239000002253 acid Substances 0.000 claims description 32
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- 239000011574 phosphorus Substances 0.000 claims description 19
- 125000004122 cyclic group Chemical group 0.000 claims description 16
- RSJKGSCJYJTIGS-UHFFFAOYSA-N undecane Chemical compound CCCCCCCCCCC RSJKGSCJYJTIGS-UHFFFAOYSA-N 0.000 claims description 12
- 125000003118 aryl group Chemical group 0.000 claims description 11
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- ZLNQQNXFFQJAID-UHFFFAOYSA-L magnesium carbonate Chemical compound [Mg+2].[O-]C([O-])=O ZLNQQNXFFQJAID-UHFFFAOYSA-L 0.000 claims description 9
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- 125000000753 cycloalkyl group Chemical group 0.000 claims description 7
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 7
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims description 6
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- PGKOCQOKUIVFLG-UHFFFAOYSA-N [Mg].P(O)O Chemical compound [Mg].P(O)O PGKOCQOKUIVFLG-UHFFFAOYSA-N 0.000 claims description 3
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- PQDJYEQOELDLCP-UHFFFAOYSA-N trimethylsilane Chemical compound C[SiH](C)C PQDJYEQOELDLCP-UHFFFAOYSA-N 0.000 claims description 3
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- 125000001118 alkylidene group Chemical group 0.000 claims 1
- 125000003968 arylidene group Chemical group [H]C(c)=* 0.000 claims 1
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- 125000005356 cycloalkylalkenyl group Chemical group 0.000 claims 1
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- 238000012360 testing method Methods 0.000 description 29
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 24
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- 239000000047 product Substances 0.000 description 15
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 14
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- 239000000654 additive Substances 0.000 description 14
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- 238000006884 silylation reaction Methods 0.000 description 13
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- QQVIHTHCMHWDBS-UHFFFAOYSA-N isophthalic acid Chemical compound OC(=O)C1=CC=CC(C(O)=O)=C1 QQVIHTHCMHWDBS-UHFFFAOYSA-N 0.000 description 9
- NFIYTPYOYDDLGO-UHFFFAOYSA-N phosphoric acid;sodium Chemical compound [Na].OP(O)(O)=O NFIYTPYOYDDLGO-UHFFFAOYSA-N 0.000 description 9
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- HQKMJHAJHXVSDF-UHFFFAOYSA-L magnesium stearate Chemical compound [Mg+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O HQKMJHAJHXVSDF-UHFFFAOYSA-L 0.000 description 6
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- HNNQYHFROJDYHQ-UHFFFAOYSA-N 3-(4-ethylcyclohexyl)propanoic acid 3-(3-ethylcyclopentyl)propanoic acid Chemical compound CCC1CCC(CCC(O)=O)C1.CCC1CCC(CCC(O)=O)CC1 HNNQYHFROJDYHQ-UHFFFAOYSA-N 0.000 description 5
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F297/00—Macromolecular compounds obtained by successively polymerising different monomer systems using a catalyst of the ionic or coordination type without deactivating the intermediate polymer
- C08F297/06—Macromolecular compounds obtained by successively polymerising different monomer systems using a catalyst of the ionic or coordination type without deactivating the intermediate polymer using a catalyst of the coordination type
- C08F297/08—Macromolecular compounds obtained by successively polymerising different monomer systems using a catalyst of the ionic or coordination type without deactivating the intermediate polymer using a catalyst of the coordination type polymerising mono-olefins
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F297/00—Macromolecular compounds obtained by successively polymerising different monomer systems using a catalyst of the ionic or coordination type without deactivating the intermediate polymer
- C08F297/06—Macromolecular compounds obtained by successively polymerising different monomer systems using a catalyst of the ionic or coordination type without deactivating the intermediate polymer using a catalyst of the coordination type
- C08F297/08—Macromolecular compounds obtained by successively polymerising different monomer systems using a catalyst of the ionic or coordination type without deactivating the intermediate polymer using a catalyst of the coordination type polymerising mono-olefins
- C08F297/083—Macromolecular compounds obtained by successively polymerising different monomer systems using a catalyst of the ionic or coordination type without deactivating the intermediate polymer using a catalyst of the coordination type polymerising mono-olefins the monomers being ethylene or propylene
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F110/00—Homopolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
- C08F110/04—Monomers containing three or four carbon atoms
- C08F110/06—Propene
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F210/00—Copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
- C08F210/16—Copolymers of ethene with alpha-alkenes, e.g. EP rubbers
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F4/00—Polymerisation catalysts
- C08F4/42—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors
- C08F4/44—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors selected from light metals, zinc, cadmium, mercury, copper, silver, gold, boron, gallium, indium, thallium, rare earths or actinides
- C08F4/60—Metals; Metal hydrides; Metallo-organic compounds; Use thereof as catalyst precursors selected from light metals, zinc, cadmium, mercury, copper, silver, gold, boron, gallium, indium, thallium, rare earths or actinides together with refractory metals, iron group metals, platinum group metals, manganese, rhenium technetium or compounds thereof
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L53/00—Compositions of block copolymers containing at least one sequence of a polymer obtained by reactions only involving carbon-to-carbon unsaturated bonds; Compositions of derivatives of such polymers
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- Chemical & Material Sciences (AREA)
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- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Transition And Organic Metals Composition Catalysts For Addition Polymerization (AREA)
- Graft Or Block Polymers (AREA)
Abstract
Description
聚合步骤(I) | 聚合步骤(II) | Log( | ||||||||
聚合比例(wt%) | MFR(i)(克/10分钟) | Cf(比值) | 韧性(兆帕) | 数均分子量 | 密度(克/立方厘米) | 聚合比例(wt%) | MFR(ii)(克/10分钟) | C″3/C″2(wt/比值) | MFR(i)/MFR(ii) | |
实施例1实施例2实施例3实施例4实施例5实施例6实施例7实施例8实施例9 | 909085909090929090 | 200198355150400900210190200 | 0.310.460.400.150.410.470.320.280.31 | 13.29.511.416.910.47.813.213.813.4 | 192001910016700210001620013200189001950019200 | 0.900.900.910.900.910.920.900.900.90 | 10101510101081010 | 0.0010.0010.0020.000010.0010.00070.00010.00010.0001 | 60/4060/4060/4060/4060/4060/4060/4065/3530/70 | 5.35.35.27.25.66.15.35.35.3 |
对比实施例1对比实施例2对比实施例3对比实施例4 | 90909092 | 200200200180 | 0.600.290.310.27 | 6.113.413.313.9 | 9000192001920014800 | 0.900.900.900.90 | 1010108 | 0.0010.00070.00070.01 | 50/4090/1010/9060/40 | 5.35.55.54.3 |
聚合物组合物 | |||
MFR(克/10分钟) | 挠曲模量(兆帕) | 悬臂梁式冲击强度(J/m,23℃) | |
实施例1实施例2实施例3实施例4实施例5实施例6实施例7实施例8实施例9 | 59585829110220795659 | 180016001600179018501850182018501800 | 90801102007050809086 |
对比实施例1对比实施例2对比实施例3对比实施例4 | 59575782 | 1200150015001550 | 70304078 |
实施例 | |||||||||||||
10 | 11 | 12 | 13 | 14 | 15 | 16 | 17 | 18 | 19 | 20 | |||
MFR(克/10分钟) | 0.4 | 3 | 30 | 150 | 10 | 50 | 22 | 7 | 11 | 45 | 125 | ||
Cf值(比值) | 0.31 | 0.46 | 0.40 | 0.15 | 0.41 | 0.47 | 0.32 | 0.28 | 0.31 | 0.11 | 0.24 | ||
聚合步骤(II)的聚合物 | 比例(wt%) | 10 | 10 | 10 | 10 | 15 | 15 | 10 | 10 | 8 | 8 | 8 | |
R-C2 **(wt%) | 40 | 40 | 40 | 40 | 40 | 40 | 40 | 40 | 40 | 40 | 50 | ||
共混重量份* | α-晶体成核剂[1] | 0.05 | - | - | - | - | - | - | - | - | - | - | |
ditto[2] | - | 0.1 | - | - | - | - | - | - | - | - | - | ||
ditto[3] | - | - | 0.25 | - | - | - | - | - | - | - | - | ||
ditto[4] | - | - | - | 0.3 | - | - | - | - | - | - | - | ||
ditto[5] | - | - | - | - | 0.15 | - | - | - | - | - | - | ||
ditto[6] | - | - | - | - | - | 0.2 | - | - | - | - | - | ||
ditto[7] | - | - | - | - | - | - | 0.1 | - | - | - | - | ||
ditto[8] | - | - | - | - | - | - | - | 0.5 | - | - | - | ||
ditto[9] | - | - | - | - | - | - | - | - | 0.4 | - | - | ||
ditto[10] | - | - | - | - | - | - | - | - | - | 0.1 | - | ||
ditto[11] | - | - | - | - | - | - | - | - | - | - | 0.2 | ||
ditto[12] | - | - | - | - | - | - | - | - | - | - | - | ||
ditto[13] | - | - | - | - | - | - | - | - | - | - | - | ||
ditto[14] | - | - | - | - | - | - | - | - | - | - | - | ||
酚类抗氧化剂 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | ||
含磷抗氧化剂 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | ||
Ca-St | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | ||
韧性(兆帕) | 6.5 | 6.1 | 6.2 | 6.9 | 6.5 | 6.1 | 6.5 | 6.8 | 6.3 | 6.8 | 6.5 | ||
弯曲模量×103(兆帕) | 1.58 | 1.55 | 1.56 | 1.58 | 1.45 | 1.46 | 1.54 | 1.55 | 1.733 | 1.76 | 1.70 | ||
悬臂梁式冲击强度(J/m.-20℃) | 56 | 55 | 54 | 53 | 65 | 54 | 54 | 55 | 54 | 53 | 54 |
实施例 | 参比实施例 | ||||||||||||
21 | 22 | 23 | 24 | 25 | 26 | 27 | 1 | 2 | 3 | 4 | |||
MFR(克/10分钟) | 82 | 60 | 35 | 23 | 23 | 23 | 23 | 20 | 20 | 20 | 20 | ||
Cf值(比值) | 0.37 | 0.36 | 0.30 | 0.31 | 0.31 | 0.31 | 0.31 | 0.60 | 0.60 | 0.60 | 0.60 | ||
聚合步骤(II)的聚合物 | 比例(wt%) | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | |
R-C2 **(wt%) | 35 | 60 | 70 | 40 | 40 | 40 | 40 | 40 | 40 | 40 | 40 | ||
共混重量份* | α-晶体成核剂[1] | - | - | - | 0.1 | - | - | 0.1 | - | - | - | - | |
ditto[2] | - | - | - | 0.1 | - | - | - | 0.1 | - | - | - | ||
ditto[3] | - | - | - | - | 0.05 | - | - | - | - | - | - | ||
ditto[4] | - | - | - | - | 0.05 | 0.1 | - | - | 0.3 | - | - | ||
ditto[5] | - | - | - | - | 0.05 | - | - | - | - | - | - | ||
ditto[6] | - | - | - | - | 0.05 | - | - | - | - | - | - | ||
ditto[7] | - | - | - | - | 0.05 | 0.1 | - | - | - | - | - | ||
ditto[8] | - | - | - | - | 0.05 | - | - | - | - | - | - | ||
ditto[9] | - | - | - | - | - | - | - | - | - | - | - | ||
ditto[10] | - | - | - | - | - | 0.1 | 0.1 | - | - | 0.1 | - | ||
ditto[11] | - | - | - | - | - | - | - | - | - | - | - | ||
ditto[12] | 10-3 | - | - | - | - | - | 0.01 | - | - | - | 10-3 | ||
ditto[13] | - | 10-4 | - | - | - | - | - | - | - | - | - | ||
ditto[14] | - | - | 0.01 | - | - | - | - | - | - | - | - | ||
酚类抗氧化剂 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | ||
含磷抗氧化剂 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | ||
Ca-St | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | ||
韧性(兆帕) | 6.2 | 6.3 | 6.5 | 6.7 | 6.9 | 6.5 | 6.6 | -6.9 | -6.8 | -7.2 | -7.0 | ||
弯曲模量×103(兆帕) | 1.71 | 1.70 | 1.68 | 1.54 | 1.52 | 1.70 | 1.75 | 1.40 | 1.38 | 1.53 | 1.50 | ||
悬臂梁式冲击强度(J/m.-20℃) | 533 | 55 | 54 | 55 | 53 | 55 | 56 | 47 | 48 | 49 | 48 |
实施例 | |||||||||||||
28 | 29 | 30 | 31 | 32 | 33 | 34 | 35 | 36 | 37 | 38 | |||
MFR(克/10分钟) | 0.4 | 3 | 30 | 150 | 10 | 50 | 22 | 7 | 11 | 45 | 125 | ||
Cf值(比值) | 0.31 | 0.46 | 0.40 | 0.15 | 0.41 | 0.47 | 0.32 | 0.28 | 0.31 | 0.11 | 0.24 | ||
聚合步骤(II)的聚合物 | 比例(wt%) | 10 | 10 | 10 | 10 | 15 | 15 | 10 | 10 | 8 | 8 | 8 | |
R-C2 **(wt%) | 40 | 40 | 40 | 40 | 40 | 40 | 40 | 40 | 40 | 40 | 50 | ||
共混重量份* | β-晶体成核剂[1] | 10-4 | - | - | - | - | - | - | - | - | - | - | |
ditto[2] | - | 0.01 | - | - | - | - | - | - | - | - | - | ||
ditto[4] | - | - | 0.05 | - | - | - | - | - | - | - | - | ||
ditto[6] | - | - | - | 0.1 | - | - | - | - | - | - | - | ||
ditto[8] | - | - | - | - | 0.2 | - | - | - | - | - | - | ||
ditto[10] | - | - | - | - | - | 0.3 | - | - | - | - | - | ||
ditto[12] | - | - | - | - | - | - | 0.5 | - | - | - | - | ||
ditto[14] | - | - | - | - | - | - | - | 10-3 | - | - | - | ||
ditto[16] | - | - | - | - | - | - | - | - | 0.4 | - | - | ||
ditto[18] | - | - | - | - | - | - | - | - | - | 0.1 | - | ||
ditto[20] | - | - | - | - | - | - | - | - | - | - | 0.2 | ||
ditto[22] | - | - | - | - | - | - | - | - | - | - | - | ||
ditto[24] | - | - | - | - | - | - | - | - | - | - | - | ||
ditto[26] | - | - | - | - | - | - | - | - | - | - | - | ||
酚类抗氧化剂 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | ||
含磷抗氧化剂 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | ||
Ca-St | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | ||
韧性(兆帕) | 11.5 | 11.8 | 12.0 | 12.5 | 12.2 | 11.9 | 12.0 | 11.5 | 11.6 | 11.0 | 10.8 |
实施例 | 参比实施例 | ||||||||||||
39 | 40 | 41 | 42 | 43 | 44 | 45 | 5 | 6 | 7 | 8 | |||
MFR(克/10分钟) | 82 | 60 | 35 | 23 | 23 | 23 | 23 | 20 | 20 | 20 | 20 | ||
Cf值(比值) | 0.37 | 0.36 | 0.30 | 0.31 | 0.31 | 0.31 | 0.31 | 0.60 | 0.60 | 0.60 | 0.60 | ||
聚合步骤(II)的聚合物 | 比例(wt%) | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | |
R-C2 **(wt%) | 35 | 60 | 70 | 40 | 40 | 40 | 40 | 40 | 40 | 40 | 40 | ||
共混重量份* | β-晶体成核剂[1] | - | - | - | - | - | - | 10-3 | 10-4 | - | - | - | |
ditto[2] | - | - | - | 0.01 | - | - | - | - | - | - | - | ||
ditto[4] | - | - | - | 0.01 | - | - | - | - | - | - | - | ||
ditto[6] | - | - | - | 0.01 | - | - | 0.1 | - | 0.1 | - | - | ||
ditto[8] | - | - | - | 0.01 | - | - | - | - | - | - | - | ||
ditto[10] | - | - | - | 0.01 | - | - | - | - | - | - | - | ||
ditto[12] | - | - | - | 0.01 | - | - | - | - | - | - | - | ||
ditto[14] | - | - | - | 0.01 | - | - | - | - | - | - | - | ||
ditto[16] | - | - | - | 0.01 | - | - | - | - | - | - | - | ||
ditto[18] | - | - | - | - | 0.05 | 0.1 | 0.02 | - | - | 0.2 | - | ||
ditto[20] | - | - | - | - | 0.05 | 0.1 | 0.02 | - | - | - | - | ||
ditto[22] | 0.3 | - | - | - | 0.05 | 0.1 | 0.02 | - | - | - | - | ||
ditto[24] | - | 0.5 | - | - | 0.05 | 0.1 | 0.02 | - | - | - | - | ||
ditto[26] | - | - | 1.0 | - | - | 0.1 | 0.02 | - | - | - | 0.2 | ||
酚类抗氧化剂 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | ||
含磷抗氧化剂 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | ||
Ca-St | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | ||
韧性(兆帕) | 10.5 | 10.8 | 11.1 | 12.3 | 11.6 | 11.2 | 11.9 | -6.0 | -5.8 | -6.6 | -6.3 |
实施例 | |||||||||||||
46 | 47 | 48 | 49 | 50 | 51 | 52 | 53 | 54 | 55 | 56 | |||
MFR(克/10分钟) | 0.1 | 3 | 30 | 150 | 10 | 50 | 22 | 7 | 11 | 45 | 125 | ||
Cf值(比值) | 0.30 | 0.46 | 0.40 | 0.15 | 0.41 | 0.47 | 0.32 | 0.28 | 0.31 | 0.11 | 0.24 | ||
聚合步骤(II)的聚合物 | 比例(wt%) | 10 | 10 | 10 | 10 | 15 | 15 | 10 | 10 | 8 | 8 | 8 | |
R-C2 **(wt%) | 40 | 40 | 40 | 40 | 40 | 40 | 40 | 40 | 40 | 40 | 50 | ||
共混重量份* | β-晶体成核剂[1] | 10-4 | - | - | - | - | - | - | - | - | - | - | |
ditto[3] | - | 0.01 | - | - | - | - | - | - | - | - | - | ||
ditto[5] | - | - | 0.05 | - | - | - | - | - | - | - | - | ||
ditto[7] | - | - | - | 0.1 | - | - | - | - | - | - | - | ||
ditto[9] | - | - | - | - | 0.2 | - | - | - | - | - | - | ||
ditto[11] | - | - | - | - | - | 0.3 | - | - | - | - | - | ||
ditto[13] | - | - | - | - | - | - | 0.5 | - | - | - | - | ||
ditto[15] | - | - | - | - | - | - | - | 10-3 | - | - | - | ||
ditto[17] | - | - | - | - | - | - | - | - | 0.4 | - | - | ||
ditto[19] | - | - | - | - | - | - | - | - | - | 0.1 | - | ||
ditto[21] | - | - | - | - | - | - | - | - | - | - | 0.2 | ||
ditto[23] | - | - | - | - | - | - | - | - | - | - | - | ||
ditto[25] | - | - | - | - | - | - | - | - | - | - | - | ||
ditto[27] | - | - | - | - | - | - | - | - | - | - | - | ||
酚类抗氧化剂 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | ||
含磷抗氧化剂 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | ||
Ca-St | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | ||
韧性(兆帕) | 11.6 | 11.8 | 12.1 | 12.5 | 12.3 | 11.9 | 12.0 | 11.6 | 11.6 | 11.2 | 10.8 |
实施例 | 参比实施例 | ||||||||||||
57 | 58 | 59 | 60 | 61 | 62 | 63 | 9 | 10 | 11 | 12 | |||
MFR(克/10分钟) | 82 | 60 | 35 | 23 | 23 | 23 | 23 | 20 | 20 | 20 | 20 | ||
Cf值(比值) | 0.37 | 0.36 | 0.30 | 0.31 | 0.31 | 0.31 | 0.31 | 0.60 | 0.60 | 0.60 | 0.60 | ||
聚合步骤(II)的聚合物 | 比例(wt%) | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | 10 | |
R-C2 **(wt%) | 35 | 60 | 70 | 40 | 40 | 40 | 40 | 40 | 40 | 40 | 40 | ||
共混重量份* | β-晶体成核剂[1] | - | - | - | - | - | - | 10-3 | 10-3 | - | - | - | |
ditto[3] | - | - | - | 0.01 | - | - | - | - | - | - | - | ||
ditto[5] | - | - | - | 0.01 | - | - | 0.1 | - | 0.1 | - | - | ||
ditto[7] | - | - | - | 0.01 | - | - | - | - | - | - | - | ||
ditto[9] | - | - | - | 0.01 | - | - | - | - | - | - | - | ||
ditto[11] | - | - | - | 0.01 | - | - | - | - | - | - | - | ||
ditto[13] | - | - | - | 0.01 | - | - | - | - | - | - | - | ||
ditto[15] | - | - | - | 0.01 | - | - | - | - | - | - | - | ||
ditto[17] | - | - | - | 0.01 | - | - | - | - | - | - | - | ||
ditto[19] | - | - | - | - | 0.05 | - | 0.02 | - | - | - | - | ||
ditto[21] | - | - | - | - | 0.05 | - | 0.02 | - | - | 0.2 | - | ||
ditto[23] | 0.3 | - | - | - | 0.05 | - | 0.02 | - | - | - | - | ||
ditto[25] | - | 0.5 | - | - | - | 0.1 | 0.02 | - | - | - | 0.2 | ||
ditto[27] | - | - | 1.0 | - | - | 0.1 | 0.02 | - | - | - | - | ||
酚类抗氧化剂 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | ||
含磷抗氧化剂 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | ||
Ca-St | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | ||
韧性(兆帕) | 10.7 | 10.8 | 11.0 | 12.3 | 11.6 | 11.1 | 11.9 | -6.0 | -5.9 | -6.5 | -6.4 |
Claims (11)
Applications Claiming Priority (12)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP24877595 | 1995-08-31 | ||
JP248775/1995 | 1995-08-31 | ||
JP248775/95 | 1995-08-31 | ||
JP119298/96 | 1996-05-14 | ||
JP11929896 | 1996-05-14 | ||
JP119298/1996 | 1996-05-14 | ||
JP120012/96 | 1996-05-15 | ||
JP120011/1996 | 1996-05-15 | ||
JP12001296 | 1996-05-15 | ||
JP120011/96 | 1996-05-15 | ||
JP120012/1996 | 1996-05-15 | ||
JP12001196 | 1996-05-15 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1169743A true CN1169743A (zh) | 1998-01-07 |
CN1119364C CN1119364C (zh) | 2003-08-27 |
Family
ID=27470582
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN96191163A Expired - Fee Related CN1119364C (zh) | 1995-08-31 | 1996-08-30 | 丙烯-乙烯共聚物组合物及其制备方法 |
Country Status (9)
Country | Link |
---|---|
US (1) | US6005034A (zh) |
EP (1) | EP0790262B1 (zh) |
JP (1) | JP3231332B2 (zh) |
KR (1) | KR100430512B1 (zh) |
CN (1) | CN1119364C (zh) |
AU (1) | AU717990B2 (zh) |
DE (1) | DE69608240T2 (zh) |
TW (1) | TW416962B (zh) |
WO (1) | WO1997008218A1 (zh) |
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-
1996
- 1996-08-30 DE DE69608240T patent/DE69608240T2/de not_active Expired - Lifetime
- 1996-08-30 EP EP96928713A patent/EP0790262B1/en not_active Expired - Lifetime
- 1996-08-30 JP JP51012997A patent/JP3231332B2/ja not_active Expired - Fee Related
- 1996-08-30 CN CN96191163A patent/CN1119364C/zh not_active Expired - Fee Related
- 1996-08-30 KR KR1019970703010A patent/KR100430512B1/ko not_active IP Right Cessation
- 1996-08-30 AU AU68382/96A patent/AU717990B2/en not_active Ceased
- 1996-08-30 US US08/817,850 patent/US6005034A/en not_active Expired - Lifetime
- 1996-08-30 WO PCT/JP1996/002449 patent/WO1997008218A1/ja active IP Right Grant
- 1996-09-19 TW TW085111469A patent/TW416962B/zh not_active IP Right Cessation
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1090250C (zh) * | 1997-04-22 | 2002-09-04 | 智索股份有限公司 | 纤维、无纺布、针织物及其应用 |
CN102165006A (zh) * | 2008-10-07 | 2011-08-24 | 博里利斯股份公司 | 高流动性多相聚丙烯 |
CN102165006B (zh) * | 2008-10-07 | 2013-11-27 | 博里利斯股份公司 | 高流动性多相聚丙烯 |
CN106029771A (zh) * | 2013-12-23 | 2016-10-12 | 布拉斯科美国有限公司 | 具有增强的外观和优良模塑流动性的基于丙烯的组合物 |
CN106029771B (zh) * | 2013-12-23 | 2019-07-26 | 布拉斯科美国有限公司 | 具有增强的外观和优良模塑流动性的基于丙烯的组合物 |
CN109422959A (zh) * | 2017-09-05 | 2019-03-05 | 中国石油化工股份有限公司 | 一种抗冲聚丙烯组合物及其制备方法 |
CN109422959B (zh) * | 2017-09-05 | 2021-11-19 | 中国石油化工股份有限公司 | 一种抗冲聚丙烯组合物及其制备方法 |
Also Published As
Publication number | Publication date |
---|---|
DE69608240T2 (de) | 2000-11-23 |
TW416962B (en) | 2001-01-01 |
WO1997008218A1 (fr) | 1997-03-06 |
DE69608240D1 (de) | 2000-06-15 |
JP3231332B2 (ja) | 2001-11-19 |
CN1119364C (zh) | 2003-08-27 |
EP0790262A1 (en) | 1997-08-20 |
US6005034A (en) | 1999-12-21 |
EP0790262A4 (en) | 1998-04-01 |
KR970707190A (ko) | 1997-12-01 |
EP0790262B1 (en) | 2000-05-10 |
AU717990B2 (en) | 2000-04-06 |
KR100430512B1 (ko) | 2004-07-23 |
AU6838296A (en) | 1997-03-19 |
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