CN113710709B - 含氟聚合物水性分散液的制造方法 - Google Patents

含氟聚合物水性分散液的制造方法 Download PDF

Info

Publication number
CN113710709B
CN113710709B CN202080030292.7A CN202080030292A CN113710709B CN 113710709 B CN113710709 B CN 113710709B CN 202080030292 A CN202080030292 A CN 202080030292A CN 113710709 B CN113710709 B CN 113710709B
Authority
CN
China
Prior art keywords
group
carbon atoms
general formula
less
mass
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN202080030292.7A
Other languages
English (en)
Chinese (zh)
Other versions
CN113710709A (zh
Inventor
米田聪
东昌弘
石原寿美
吉田裕俊
藤本阳平
岸川洋介
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Daikin Industries Ltd
Original Assignee
Daikin Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Daikin Industries Ltd filed Critical Daikin Industries Ltd
Publication of CN113710709A publication Critical patent/CN113710709A/zh
Application granted granted Critical
Publication of CN113710709B publication Critical patent/CN113710709B/zh
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00Processes of treating or compounding macromolecular substances
    • C08J3/02Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
    • C08J3/03Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media
    • C08J3/05Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media from solid polymers
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F114/00Homopolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
    • C08F114/18Monomers containing fluorine
    • C08F114/26Tetrafluoroethene
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F14/00Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
    • C08F14/18Monomers containing fluorine
    • C08F14/26Tetrafluoroethene
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00Processes of polymerisation
    • C08F2/12Polymerisation in non-solvents
    • C08F2/16Aqueous medium
    • C08F2/22Emulsion polymerisation
    • C08F2/24Emulsion polymerisation with the aid of emulsifying agents
    • C08F2/26Emulsion polymerisation with the aid of emulsifying agents anionic
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F6/00Post-polymerisation treatments
    • C08F6/14Treatment of polymer emulsions
    • C08F6/20Concentration
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00Processes of treating or compounding macromolecular substances
    • C08J3/02Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
    • C08J3/03Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00Processes of treating or compounding macromolecular substances
    • C08J3/12Powdering or granulating
    • C08J3/14Powdering or granulating by precipitation from solutions
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2327/00Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers
    • C08J2327/02Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers not modified by chemical after-treatment
    • C08J2327/12Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers not modified by chemical after-treatment containing fluorine atoms
    • C08J2327/18Homopolymers or copolymers of tetrafluoroethylene

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
CN202080030292.7A 2019-04-26 2020-04-27 含氟聚合物水性分散液的制造方法 Active CN113710709B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2019085977 2019-04-26
JP2019-085977 2019-04-26
PCT/JP2020/018039 WO2020218618A1 (ja) 2019-04-26 2020-04-27 フルオロポリマー水性分散液の製造方法

Publications (2)

Publication Number Publication Date
CN113710709A CN113710709A (zh) 2021-11-26
CN113710709B true CN113710709B (zh) 2024-09-17

Family

ID=72942591

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202080030292.7A Active CN113710709B (zh) 2019-04-26 2020-04-27 含氟聚合物水性分散液的制造方法

Country Status (5)

Country Link
US (1) US12187859B2 (https=)
EP (1) EP3960774A4 (https=)
JP (1) JP7564452B2 (https=)
CN (1) CN113710709B (https=)
WO (1) WO2020218618A1 (https=)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117015557A (zh) * 2021-03-18 2023-11-07 大金工业株式会社 氟树脂的制造方法、氟树脂和水性分散液
WO2024248144A1 (ja) * 2023-05-31 2024-12-05 ダイキン工業株式会社 フルオロポリマー水性分散液の製造方法およびフルオロポリマー水性分散液

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2018181898A1 (ja) * 2017-03-31 2018-10-04 ダイキン工業株式会社 フルオロポリマーの製造方法、重合用界面活性剤及び界面活性剤の使用
WO2019031617A1 (ja) * 2017-08-10 2019-02-14 ダイキン工業株式会社 精製ポリテトラフルオロエチレン水性分散液の製造方法、改質ポリテトラフルオロエチレン粉末の製造方法、ポリテトラフルオロエチレン成形体の製造方法、及び、組成物

Family Cites Families (70)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3271341A (en) 1961-08-07 1966-09-06 Du Pont Aqueous colloidal dispersions of polymer
US3250808A (en) 1963-10-31 1966-05-10 Du Pont Fluorocarbon ethers derived from hexafluoropropylene epoxide
DE2908001C2 (de) * 1979-03-01 1981-02-19 Hoechst Ag, 6000 Frankfurt Verfahren zur Herstellung konzentrierter Dispersionen von Fluorpolymeren
DE3419822C2 (de) 1984-05-26 1986-04-03 Werner & Pfleiderer, 7000 Stuttgart Filtervorrichtung für Schneckenextruder
JPS6149327A (ja) 1984-08-16 1986-03-11 松下電器産業株式会社 温度過昇防止装置
JP2538783B2 (ja) 1987-09-24 1996-10-02 村樫石灰工業 株式会社 防塵処理剤組成物
JP2945450B2 (ja) 1990-07-24 1999-09-06 古野電気株式会社 傾斜センサおよび傾斜角測定装置
JPH0513961A (ja) 1991-06-28 1993-01-22 Toshiba Corp 多層配線板
JP2827152B2 (ja) 1994-07-11 1998-11-18 村樫石灰工業株式会社 塵埃抑制方法
FR2733504A1 (fr) 1995-04-28 1996-10-31 Gen Elec Plastics Abs Euro Bv Nouveaux alliages polymeres a base de polymerisat comprenant des motifs de derives de tetrafluoroethylene, procede de fabrication, articles obtenus a partir de tels alliages et utilisation de ces alliages dans des compositions polymeres
DE69617042T2 (de) 1995-12-28 2002-06-06 Daikin Industries, Ltd. Fluorhaltige, elastische copolymere, härtbare zusammensetzung und daraus hergestellte dichtungsmasse
JP3272985B2 (ja) 1996-07-31 2002-04-08 三菱レイヨン株式会社 ポリテトラフルオロエチレン含有混合粉体の製造方法
JP3931382B2 (ja) 1996-09-18 2007-06-13 ダイキン工業株式会社 ポリテトラフルオロエチレン粉末及びその製造方法
JP3718852B2 (ja) * 1997-02-13 2005-11-24 ダイキン工業株式会社 含フッ素重合体水性分散液の濃縮方法
US6040370A (en) 1997-04-17 2000-03-21 General Electric Company Aqueous fluoropolymer dispersion and method for making fluoropolymer-containing thermoplastic resin composition
ITMI981505A1 (it) * 1998-06-30 1999-12-30 Ausimont Spa Purificazione di polimeri fluorurati
CN1152894C (zh) 1998-07-07 2004-06-09 大金工业株式会社 含氟聚合物的制造方法
JP3711040B2 (ja) 2001-06-20 2005-10-26 三菱レイヨン株式会社 ポリテトラフルオロエチレン含有粉体の製造方法
US7279522B2 (en) 2001-09-05 2007-10-09 3M Innovative Properties Company Fluoropolymer dispersions containing no or little low molecular weight fluorinated surfactant
CA2458617A1 (en) 2001-09-05 2003-03-13 3M Innovative Properties Company Fluoropolymer dispersion containing no or little low molecular weight fluorinated surfactant
JP3900883B2 (ja) 2001-10-05 2007-04-04 ダイキン工業株式会社 含フッ素重合体ラテックスの製造方法
BR0215428A (pt) 2002-01-04 2004-12-14 Du Pont Dispersão aquosa, composição de revestimento da dispersão aquosa, substratos revestidos e filme auto-sustentado
JP4604453B2 (ja) * 2002-06-17 2011-01-05 ダイキン工業株式会社 含フッ素ポリマー分散体及び含フッ素ポリマー分散体製造方法
CN100347204C (zh) * 2002-11-29 2007-11-07 大金工业株式会社 含氟聚合物水性乳液的精制方法、精制乳液及含氟加工品
DE60301322T2 (de) 2003-02-28 2006-06-08 3M Innovative Properties Co., St. Paul Fluoropolymerdispersion enthaltend kein oder wenig fluorhaltiges Netzmittel mit niedrigem Molekulargewicht
US6841616B2 (en) 2003-03-28 2005-01-11 Arkema Inc. Polymerization of halogen-containing monomers using siloxane surfactant
CN1875035B (zh) 2003-10-31 2010-12-01 大金工业株式会社 含氟聚合物水性分散体的制造方法及含氟聚合物水性分散体
ITMI20040031A1 (it) * 2004-01-14 2004-04-14 Solvay Solexis Spa Processo per la preparazione di dispersori di fluoropolimeri
CA2612673C (en) 2005-06-29 2012-07-24 Nippo Corporation Method for dust-preventive treatment of material having dusting property
AU2005333936B2 (en) 2005-06-29 2010-09-23 Du Pont-Mitsui Flurochemicals Co.,Ltd. Dust-Preventive Treatment Agent
GB0523853D0 (en) 2005-11-24 2006-01-04 3M Innovative Properties Co Fluorinated surfactants for use in making a fluoropolymer
GB0514398D0 (en) 2005-07-15 2005-08-17 3M Innovative Properties Co Aqueous emulsion polymerization of fluorinated monomers using a fluorinated surfactant
GB0525978D0 (en) 2005-12-21 2006-02-01 3M Innovative Properties Co Fluorinated Surfactants For Making Fluoropolymers
GB0514387D0 (en) 2005-07-15 2005-08-17 3M Innovative Properties Co Aqueous emulsion polymerization of fluorinated monomers using a perfluoropolyether surfactant
US7671112B2 (en) 2005-07-15 2010-03-02 3M Innovative Properties Company Method of making fluoropolymer dispersion
CN100558753C (zh) 2005-10-17 2009-11-11 旭硝子株式会社 聚四氟乙烯水性乳化液、由其制得的聚四氟乙烯细粉和多孔体
JP5141256B2 (ja) 2005-10-20 2013-02-13 旭硝子株式会社 ポリテトラフルオロエチレン水性分散液およびその製品
WO2007046377A1 (ja) 2005-10-20 2007-04-26 Asahi Glass Company, Limited 溶融成形可能なフッ素樹脂の製造方法
US7728087B2 (en) * 2005-12-23 2010-06-01 3M Innovative Properties Company Fluoropolymer dispersion and method for making the same
JP2007254516A (ja) * 2006-03-22 2007-10-04 Seiko Epson Corp 水性顔料分散液、水性インク及びインクジェット記録液
US20090269044A1 (en) 2006-04-14 2009-10-29 Bridgestone Corporation Bridgestone corporation
US20070276103A1 (en) 2006-05-25 2007-11-29 3M Innovative Properties Company Fluorinated Surfactants
JP2007332321A (ja) * 2006-06-19 2007-12-27 Daikin Ind Ltd 含フッ素重合体濃縮方法および水溶性含フッ素乳化剤濃縮方法
US8119750B2 (en) 2006-07-13 2012-02-21 3M Innovative Properties Company Explosion taming surfactants for the production of perfluoropolymers
EP2079766B1 (en) 2006-11-09 2011-05-18 E.I. Du Pont De Nemours And Company Aqueous polymerization of fluorinated monomer using polymerization agent comprising high molecular weight fluoropolyether acid or salt and fluoropolyether acid or salt surfactant
JP5077350B2 (ja) * 2007-07-24 2012-11-21 ダイキン工業株式会社 新規化合物、その製造方法及びフルオロポリマーの製造方法
JP5119854B2 (ja) * 2007-10-22 2013-01-16 ダイキン工業株式会社 含フッ素ポリマー分散体及び含フッ素ポリマー分散体製造方法
JP2009172830A (ja) * 2008-01-23 2009-08-06 Mitsubishi Paper Mills Ltd インクジェット記録材料
US20090281261A1 (en) 2008-05-09 2009-11-12 E. I. Du Pont De Nemours And Company Abatement of Fluoroether Carboxylic Acids or Salts Employed in Fluoropolymer Resin Manufacture
WO2010003929A1 (en) 2008-07-08 2010-01-14 Solvay Solexis S.P.A. Method for manufacturing fluoropolymers
RU2522749C2 (ru) 2009-07-31 2014-07-20 Зм Инновейтив Пропертиз Компани Соединения фторполимера, содержащие многоатомные соединения, и способы из производства
KR101399733B1 (ko) 2010-06-30 2014-05-27 다이킨 고교 가부시키가이샤 불소 함유 중합체의 오르가노졸 조성물
EP3533811B1 (en) 2010-11-09 2021-08-11 The Chemours Company FC, LLC Nucleation in aqueous polymerization of fluoromonomer
JP6109073B2 (ja) 2010-11-09 2017-04-05 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニーE.I.Du Pont De Nemours And Company 炭化水素界面活性剤を用いたフルオロモノマーの水性重合
WO2012064858A1 (en) 2010-11-09 2012-05-18 E. I. Du Pont De Nemours And Company Reducing the telogenic behavior of hydrocarbon-containing surfactants in aqueous dispersion fluoromonomer polymerization
JP5919021B2 (ja) * 2012-02-15 2016-05-18 花王株式会社 インクジェット記録用顔料水分散液
EP2824143B1 (en) 2012-03-27 2018-07-04 Daikin Industries, Ltd. Aqueous fluoropolymer dispersion
JP5937870B2 (ja) 2012-03-30 2016-06-22 ダイキン工業株式会社 非イオン性界面活性剤組成物、及び、フルオロポリマー水性分散液
JP6381526B2 (ja) 2012-06-20 2018-08-29 ソルベイ スペシャルティ ポリマーズ イタリー エス.ピー.エー. テトラフルオロエチレンコポリマー
CN104583246B (zh) 2012-06-20 2016-08-24 索尔维特殊聚合物意大利有限公司 四氟乙烯共聚物
JP6266230B2 (ja) * 2013-05-15 2018-01-24 日揮触媒化成株式会社 表面改質金属酸化物微粒子、薄膜形成用の塗布液、薄膜付き基材、光電気セル、及び表面改質金属酸化物微粒子の製造方法
CN105263993B (zh) * 2013-06-04 2018-04-10 索尔维特殊聚合物意大利有限公司 用于制造氟聚合物复合物的方法
CN105612250A (zh) * 2013-10-07 2016-05-25 诺华股份有限公司 经处理的滤器
JP6622209B2 (ja) 2013-11-26 2019-12-18 ザ ケマーズ カンパニー エフシー リミテッド ライアビリティ カンパニー フルオロモノマーの水性重合において核を形成するためのポリアルキレンオキシドの使用
JP6902194B2 (ja) * 2014-06-20 2021-07-14 住友化学株式会社 水性エマルション並びに塗膜、硬化物及び積層体
WO2015194612A1 (ja) * 2014-06-20 2015-12-23 住友化学株式会社 水性エマルション並びに塗膜、硬化物及び積層体
CN108431055A (zh) * 2015-12-17 2018-08-21 3M创新有限公司 含胺聚合物、其分散体以及制备和使用它们的方法
WO2018181904A1 (ja) 2017-03-31 2018-10-04 ダイキン工業株式会社 フルオロポリマーの製造方法、重合用界面活性剤及び界面活性剤の使用
CN110997735B (zh) 2017-08-10 2024-03-01 大金工业株式会社 精制聚四氟乙烯水性分散液的制造方法、改性聚四氟乙烯粉末的制造方法、聚四氟乙烯成型体的制造方法以及组合物
WO2020105651A1 (ja) * 2018-11-19 2020-05-28 ダイキン工業株式会社 変性ポリテトラフルオロエチレンの製造方法及び組成物

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2018181898A1 (ja) * 2017-03-31 2018-10-04 ダイキン工業株式会社 フルオロポリマーの製造方法、重合用界面活性剤及び界面活性剤の使用
WO2019031617A1 (ja) * 2017-08-10 2019-02-14 ダイキン工業株式会社 精製ポリテトラフルオロエチレン水性分散液の製造方法、改質ポリテトラフルオロエチレン粉末の製造方法、ポリテトラフルオロエチレン成形体の製造方法、及び、組成物

Also Published As

Publication number Publication date
CN113710709A (zh) 2021-11-26
US20220213277A1 (en) 2022-07-07
US12187859B2 (en) 2025-01-07
EP3960774A1 (en) 2022-03-02
WO2020218618A1 (ja) 2020-10-29
JPWO2020218618A1 (https=) 2020-10-29
EP3960774A4 (en) 2023-01-04
JP7564452B2 (ja) 2024-10-09

Similar Documents

Publication Publication Date Title
CN111836835B (zh) 含氟聚合物的制造方法
JP7522375B2 (ja) フルオロポリマーの製造方法、ポリテトラフルオロエチレンの製造方法、パーフルオロエラストマーの製造方法および組成物
JP7492153B2 (ja) フルオロポリマーの製造方法
JP7791447B2 (ja) フルオロポリマーの製造方法
JP7617462B2 (ja) フルオロポリマー水性分散液の製造方法、排水の処理方法、及び、フルオロポリマー水性分散液
CN114127131B (zh) 含氟聚合物的制造方法、聚四氟乙烯组合物和聚四氟乙烯粉末
CN113728015B (zh) 氟聚合物水性分散液的制造方法和氟聚合物水性分散液
JP7644392B2 (ja) フルオロポリマー水性分散液の製造方法
CN111699203B (zh) 含氟聚合物的制造方法、聚合用表面活性剂、表面活性剂的用途和组合物
JP2023085494A (ja) フルオロポリマー粉末の製造方法
CN113710709B (zh) 含氟聚合物水性分散液的制造方法
CN117500848A (zh) 含氟聚合物组合物的制造方法和含氟聚合物组合物
CN119095886A (zh) 含氟聚合物的制造方法
CN119072500A (zh) 含有氟树脂的组合物的制造方法和含有氟树脂的组合物
CN117500847A (zh) 含有高纯度含氟聚合物的组合物的制造方法和含有高纯度含氟聚合物的组合物
JP7791483B2 (ja) フルオロポリマーの製造方法および組成物
CN117015557A (zh) 氟树脂的制造方法、氟树脂和水性分散液
CN121219330A (zh) 含氟聚合物水性分散液的制造方法和含氟聚合物水性分散液

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant