CN1127631A - 化妆品组合物 - Google Patents

化妆品组合物 Download PDF

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CN1127631A
CN1127631A CN95118264A CN95118264A CN1127631A CN 1127631 A CN1127631 A CN 1127631A CN 95118264 A CN95118264 A CN 95118264A CN 95118264 A CN95118264 A CN 95118264A CN 1127631 A CN1127631 A CN 1127631A
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silicon dioxide
trimethylization
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赫尔南多·布瑞瓦
胡里奥·甘斯·拉斯
伊达·玛丽·桑迪威兹
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Revlon Consumer Products LLC
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Abstract

本发明涉及改进抗转移性的化妆品组合物，它包括约0.1-约60％重量的三甲基化的二氧化硅；约0.1-约60％重量的挥发性溶剂，其粘度25℃时为0.5-100厘泊；约0.1-约60％重量的非挥发性油脂，其粘度25℃时为200-1,000,000厘泊，和；约0.1-约80％重量的化妆品可接受的载体。

Description

化妆品组合物
本发明涉及应用于皮肤或头发的化妆品领域。
化妆品组合物一般定义为适合用于人体的组合物。例如霜和乳剂等化妆品组合物被用于湿润皮肤，使其处于光滑，柔软的状态。着色化妆品，如(化妆)粉底，底红，口红，眼影等等都是用作对皮肤和唇进行着色。由于上色是化妆的最重要的原因之一，所以，必须非常仔细地配制含颜色的化妆品，以达到最大的上妆和效果。
长时间使用粉底或面部化妆物，口红，睫毛油等化妆品的问题之一是易于使化妆品从皮肤转移到其他如玻璃器皿，银制品或衣物上。这不仅产生污染，也迫使使用者要间断地重新再上妆。
例如，传统的化妆组合物是含染料的水或油乳剂，也可以是含有蜡，脂和染料的无水体系。使用这种配方，并进入皮肤以产生颜色，修正皮肤的局部使其出现平整，光滑的外表。由于仅仅是一层膜涂覆在皮肤表面，假如用手去触摸它，化妆品可能会转移或会弄脏和出现不均匀。出汗或汗珠会钻出那层膜并出现流堆或者涂抹。如皮肤接触衣物，可能会污染衣物。
本发明的目的在于提供一种可长期固着在皮肤上的化妆品的配方。
本发明的另一目的在于提供一种能产生膜的化妆品的配方，这种膜在擦汗时也不能被破坏。
本发明的另一目的在于提供一种能产生膜的化妆品的配方，它不容易转移到衣物或器皿上。
本发明的另一目的在于提供一种能产生膜的化妆品的配方，它能减少对油和水的通透性。
本发明涉及一种改进了抗转移性(TRANSFER RESISTANCE)的化妆品组合物包括：
A)约0.1-60％重量的三甲基化的二氧化硅(TRIMETHYLATEDSILICA)，
B)约0.1-60％重量的挥发性溶剂，其粘度25℃时为0.5-100厘泊；
C)0.1-60％重量的非挥发性油脂，其粘度25℃时为200-1,000,000厘泊，和；
D)0.1-80％重量的化妆品可接受的载体。
本发明之组合物含有0.1-60％重量的三甲基化的二氧化硅(也叫做三甲基甲硅烷氧基硅酸盐)(TRIMETHYLSILOXYSILICATE)，优选为0.5-50％，更优选为1-30％，其平均颗粒大小为0.5-100毫微米(millimicrons)。三甲基化的二氧化硅和挥发性溶剂可以分别加入，或者购得作为预混合混合物。二氧化硅颗粒可以是球形或非球形。适合于本发明使用的挥发性硅氧烷和三甲基化二氧化硅可参见美国专利4,983,388号制造。在本发明的优选实施方案中，三甲基化的二氧化硅和挥发性溶剂的结合物作为配料也可从DOW CORNINGCORPORATION购得，其商品名为Dow 2-0747或2-0749化妆液，它包括约等份的挥发性硅氧烷(十甲基环戊基硅氧烷和八甲基环丁基硅氧烷(decamethylcyclopentasiloxane andoctamethylcyclotetrasiloxane)以及三甲基化的二氧化硅的结合。该液体的粘度经DOW CORNING实验法CTM 0004A测得，为200-700厘泊，经DOW CORNING实验法CTM 0509C测得，25℃时其比重为1.000-1.100，经DOW CORNING实验法CTM0526A测得的反射指数(REFRACTIVE INDEX)为1.400-1.410。该配料包括占全部液体重量约49％的十甲基环戊基硅氧烷，1％的八甲基环丁基硅氧烷和50％三甲基化的二氧化硅。
本发明之溶剂具有25℃时0.5-100的低粘度，优选为0.5-20，更优选为0.5-10厘泊。适用于本发明组合物的挥发性溶剂包括低粘度的硅氧烷液体，如环硅氧烷，其通式为：
Figure A9511826400081
其中n是1-7。挥发性线性聚二甲基硅氧烷也适用，通常它具有2-9个硅原子，其通式为：
(CH3)Si--O-[Si(CH3)2--O-]n--Si(CH3)3
其中n为0-7。这些硅氧烷可利用各种来源，包括DowCorning Corporation和General Electric。市售的DowCorning硅氧烷其商品名为Dow Corning 244，245，344，345和200液体。这些液体包括八甲基环丁基硅氧烷，十甲基环戊基硅氧烷，六甲基二硅氧烷，或其混和物。
8-20碳原子，优选为10-16的直链或支链烃也适合于做为挥发性溶剂组份。其适用的烃为癸烷，十二烷，十四烷，十三烷，和US Patent 3,439,088和3,818,105公布的C8-20异链烷烃。优选的挥发性链烷烃的分子量为160-180，沸点是105320℃，粘度为25℃时小于20厘泊。这种链烷烃可从EXXON公司购得，其商标为ISOPARS，也可从PERMETHYL CORPORATION购得。这种C8-20的链烷烃，例如PERMETHYL CORPORATION生产的C12异链烷烃，其商标为PERMETHYL 99(注册商标)，或者其商标为PERMETHYL 99A(注册商标)由PRESPERSE销售的C12异链烷烃(异十二烷)。可以使用各种市售的C16异链烷烃，例如也可用商标为PERMETHYL R的异十六烷。挥发性溶剂可以是挥发性硅氧烷和异链烷烃的混合物，建议的混合比为1∶20-20∶1。挥发性溶剂优选范围为全部组合物重的1-40％，更优选为5-30％。
在本发明的优选实施方案中，占5-35％重量的全部组合物包括挥发性硅氧烷和三甲基化的二氧化硅的配料，具有本文所述特征的液体，该组合物除了配料中的挥发性硅氧烷还可含有额外量的挥发性硅氧烷。
非挥发性油脂的粘度25℃时为200-1,000,000厘泊，优选为200-600,000厘泊，优选为占组合物重量的0.1-40％，更优选为0.5-30％。
非挥发性油脂可以包括通式为RCO-OR’的酯，其中R和R’分别为C1-25，优选为C4-20，直链或支链烷基，烷氧基或链烯基。这种酯的实例包括异三癸基异壬烷酸酯(isotridecylisononanoate)，PEG-4二庚烷酸酯(PEG-4 diheptanoate)，异硬脂酰新戊烷酸酯(isostearyl neopentanoate)，新戊烷酸十三烷基酯(tridecyl neopentanoate)，辛烷酸十六烷基酯(cetyl octanoate)，棕榈酸酯(cetyl palmitate)，蓖麻醇酸酯(cetyl ricinoleate)，硬脂酸十六烷基酯(cetyl stearate)，肉豆蔻酸十六烷基酯(cetyl myristate)，椰-二辛酸酯/癸酸酯(coco-dicaprylate/caprate)，异硬脂酸癸基酯(decyl isostearate)，油酸异癸酯(isodecyloleate)，新戊烷酸异癸酯(isodecyl neopentanoate)，新戊烷酸异己酯(isohexyl neopentanoate)，棕榈酸辛酯(octylpalmitate)，马来酸二辛酯(dioctyl malate)，辛烷酸十三烷基酯(tridecyl octanoate)，肉豆蔻酸十四烷基酯(myristylmyristate)，八十二烷醇(octododecanol)，以及C.T.F.A.COSMETIC INGREDIENT HANDBOOK第一版，1988，24-26页公布的酯。
非挥发性油脂也可包括其25时粘度为100,000-250,000厘泊的高粘度表面优4脂。这种表面油脂包括蓖麻油，羊毛脂，羊毛脂的衍生物，柠檬酸三异十六烷基酯，C10-18甘油三脂，辛酸/癸酸甘油三脂，椰油，玉米油，棉子油，氢化蓖麻油，亚麻子油，貂油，橄榄油，棕榈油，illine黄油，菜子油，豆油，葵花子油，动物脂，三癸精，三羟硬脂精，triisotearin，三月桂酸，三亚油精，三肉豆蔻精，三油精，三棕榈精，三硬脂精，三山嵛精(tribehenin)，核桃油，麦胚油，胆固醇，以及C.T.F.A.COSMATIC INGREDIENT HANDBOOK，第一版，1988 26-27页记载的油脂。
适合于作非挥发油的也可是甘油酯和其衍生物，如乙酰化的蓖麻油，硬脂酸甘油酯，二油酸甘油酯，二硬脂酸甘油酯，PEG蓖麻油酯，PEG油酸甘油酯，PEG硬脂酸甘油酯，三辛烷酸甘油酯，亚麻油酸甘油酯，肉豆蔻酸甘油酯，异硬脂酸甘油酯，PEG动物脂酸甘油酯，以及C.T.F.A.COSMETIC HANDBOOK第一版1988，28-29页记载的那些油脂。
适合于用作非挥发性油也可是非挥发的烃，如异链烷烃，氢化聚异丁烯，矿物油，角鲨烯，矿脂，等等。
适合于用作非挥发行油也可是各种羊毛脂衍生物，如乙酰化羊毛脂醇，乙酰化羊毛脂蓖麻油酸酯，LANETH PHOSPHATESAND ACETATES，羊毛脂酸，羊毛脂亚麻油酸酯，羊毛脂蜡，PEG氢化羊毛脂，PRG羊毛脂，PPG羊毛脂醇醚，和C.T.F.A.COSMETIC HANDBOOK第一版1988，35页记载的那些羊毛脂。
非挥发性非氟化硅氧烷也适用于用作非挥发性组份。这种硅氧烷(SILICONE)的粘度25℃时为200-600,000厘沱(CENTISTOKES)，优选为350-100,000。适用的硅氧烷为，amodimethicone，双苯基六甲基聚硅氧烷(bisphenylhexamethicone)，二甲基聚硅氧烷(dimehticone)，二甲基聚硅氧烷共聚醇(dimethicone copolyol)，二甲基聚硅氧烷醇(dimethiconol)，十六烷基甲基聚硅氧烷(hexadecyl methicone)，hexamethyldisiloxane，甲基聚硅氧烷(methicone)，苯基三甲基聚硅氧烷(phenyl trimethicone)，simethicone，二甲基氢硅氧烷(dimethylhydrogensiloxane)，硬脂氧基二甲基聚硅氧烷(stearoxy dimethicone)，硬脂氧基三甲基硅烷，乙烯基二甲基聚硅氧烷(vinyldimethicone)，以及它们的混合物。这种硅氧烷可购自DOW CORNING的3225C配方，DOW 190和193液，或由Goldschmidt公司的商品名为ABIL的产品。
非挥发性油也可用各种氟化油，如氟化硅氧烷或过氟聚醚(perfluropolyethers)。特别适用的是氟硅氧烷，如三甲基甲硅烷基端封氟硅氧烷油，聚三氟丙基甲基硅氧烷，以及US专利5,118,496公开的相同的硅氧烷。非挥发性组份可以包括氟硅氧烷和二甲基聚硅氧烷的混和物。非挥发性组份可以包括US专利5,183,589和4,803,067以及5,183,588中披露的那些过氟聚醚。这种过氟聚醚可从市场上购得，Montefluos公司产，商标为FOMBLIN。
其他适当的非挥发性油包括脱水山梨醇衍生物，如PEG脱水山梨醇蜂蜡，PEG异硬脂酸脱水山梨醇酯，PEG脱水山梨醇羊毛脂酸酯(PEG sorbitan lanolate)，PEG油酸脱水山梨醇酯，PEG棕榈酸脱水山梨醇酯，PEG硬脂酸脱水山梨醇酯，多乙氧基醚，三油酸脱水山梨醇酯，三硬脂酸脱水山梨醇酯，等等，以及C.T.F.A.COSMETIC HANDBOOK第一版1988，44页记载的那些物质。
本发明的组合物含有0.1-80％的化妆品可接受的载体，它可以是水/油乳液，上色化妆品如睫毛油，上妆粉或水，眼影，底红，遮盖霜，口红等。
霜或者乳液通常是水和油的乳浊液，它含有水，湿润剂，表面活性剂，稳定剂，防晒剂，干燥剂等等。通常这些组份的范围为：0.1-80％的水，0.01-10％的湿润剂，0.01-5％的表面活性剂，0.001-5％的稳定剂，以及0.001-10％的防晒剂。合适的乳化剂，湿润剂，表面活性剂，稳定剂和防晒剂参见C.T.F.A.COSMETIC HANDBOOK第一版1988，所记载的那些物质。
霜可以是有水，或无水的，也可以包括水，湿润剂，表面活性剂，增稠剂，稳定剂防晒剂。
本发明所述的霜剂和乳液是防晒剂最好的载体。特别是，可加入约0.001-10％重量的各种防晒化合物，如PABA(对氨基苯甲酸)及其衍生物。因为该组合物显示出优良的抗转移的特性，这样防晒既能够在皮肤上保留较长的时间。本发明特别适合的霜剂是防晒霜，它包括：
1-30％三甲基化二氧化硅
1-40％挥发性溶剂
0.5-30％非挥发性油
0.1-70％干燥，特别物质
这种干燥，特别物选自二氧化钛和其它粉状物质，它提供良好的防晒作用。通常二氧化钛形成绝大多数的干燥，特别物质。
优选的是，本发明的组合物包括一种载体，它是一种有色化妆品组合物，如口红，上妆粉，底色，眼影，油底或粉底等等。
合适的粉饼一般含干燥特别物，它的颗粒大小为0.02-200，优选为0.5-100微米。所述的特别物可以是有色或无色的，(如白色)，特别是，染料粉用于本发明的目的。合适的粉剂包括氯氧化铋，钛酸盐云母，烟蒸过的(FUMED)二氧化硅，球形氧化硅，聚甲基丙烯酸甲酯，微化的特富龙(TEFLON商标)，一氮化硼，丙烯酸聚合物，硅酸铝，辛基琥珀酸淀粉铝(aluminium starch octenylsuccinate)，benonite，硅酸钙，纤维素，白垩，玉米淀粉，硅藻土，漂白土，甘又淀粉，水辉石，水合二氧化硅，高岭土，硅酸镁铝，碳酸镁，氢氧化镁，氧化镁，硅酸镁，三硅酸镁，麦芽糖糊精，蒙托土，微结晶纤维素，米淀粉，二氧化硅，滑石，云母，二氧化钛，月桂酸锌，肉桂酸锌，新十六烷酸锌，松脂酸锌，硬脂酸锌，聚乙烯，氧化铝，attapulgite，碳酸钙，硅酸钙，糊精，高岭土，尼龙，甲硅烷酸硅(SILICA SILYLATE)，丝份，丝云母，大豆粉，氧化锡，氢氧化钛，磷酸三镁，核桃壳粉，或其混合物。上述的粉可以是用卵磷质，氨基酸，矿物质油，硅氧烷油或其他试剂单独或混合后处理其表面，使其包被粉剂的表面，显示出颗粒疏水性。
粉剂组份也可包括各种有机无机颜料(PIGMENTS)。有机颜料通常是芳香型的，包括偶氮，靛类染料，三苯甲烷，蒽琨，和黄嘌呤染料，可称为D&C和FD&C兰，棕，绿，桔黄，红，黄，等。有机颜料一般包括不溶性的金属盐或鉴定的颜色添加剂，称之为色淀。无机颜料包括氧化铁，群青铬或氢氧化铬色料，以及它们的混合物。
粉组份中使用的颜料的百分比将取决于要配制的化装品的类型。底色(BLUSHERS)，眼影，口红和类似的化妆品将在粉相中含有大量的颜料，通常占化妆品组合物总量的5-50％。一般颜料∶粉的配比为：1∶20-20∶1。
优选的面部用扑粉(FACE POWDER)组合物包括：
0.1-60％三甲基化二氧化硅；
0.1-60％挥发性溶剂，其粘度25℃时为0.5-100厘泊；
0.1-60％非挥发性油，其粘度25℃时为200-1,000,000厘泊；
0.1-80％干燥特别物质(DRY PARTICULATE MATTER)。
本发明组合物也可加入睫(眉)毛油中，睫毛油通常含有膜成形剂，蜡，乳化剂，以及颜料。
合适的睫(眉)毛油组合物包括：
0.1-15％三甲基化二氧化硅；
0.1-40％挥发性溶剂，其粘度25℃时为0.5-100厘泊；
0.1-10％非挥发性油；
0.1-30％干燥特别物质；
0.1-20％膜形成剂；
0.1-30％蜡；和0.1-100％乳化剂。
优选的是，挥发性溶剂包括挥发性硅氧烷和挥发性烃的混合物，干燥特别物质包括颜料和非颜料粉末的组合。
膜形成剂包括阿拉伯胶，纤维素衍生物，瓜耳胶衍生物以及C.T.F.A.COSMETIC HANDBOOK第一版1988，68-69页记载的那些物质。
其溶点为35℃-120℃的蜡包括天然和合成蜡，如月桂子蜡，蜂蜡，小烛树蜡，巴西棕榈蜡，地蜡，十六烷基脂，氢化西蒙得木油(JOJOBA OIL)，氢化西蒙得木蜡，氢化米糠蜡，日本蜡，西蒙得木脂(JOJOBA BUTTER)，西蒙得木油，西蒙得木蜡，羊毛脂蜡，微结晶蜡，貂油，褐煤酸，褐煤，小冠巴西棕蜡，地蜡，米糠，紫胶蜡，合成蜂蜡和合成蜡等等。
合适的乳化剂参见C.T.F.A.COSMETIC HANDBOOK第一版1988，90-94页记载的那些物质。
本发明的组合物也可以加入水和油乳剂化妆品组合物或底妆中。配制除了油相外，通常含有水和颜料。合适的化妆品配制组合物包括：
0.1-20％三甲基化二氧化硅；
0.1-40％挥发性溶剂，其粘度25℃时为0.5-100厘泊；
0.1-10％非挥发性油，其粘度25度时为350-1,000,000厘泊；
0.1-70％干燥特别物质，其颗粒大小为0.02-100微米，和
0.1-50％水。
优选的是，非挥发性油是二甲基聚硅氧烷(dimethicone)和二甲基聚硅氧烷共聚醇(dimethicone copolyol)，颜料与粉末的比例是1∶20-20∶1。
化妆品可接受的载体也可是底色(BLUSHER)。优选的底色包括：
0.1-20％三甲基化二氧化硅；
0.1-30％挥发性溶剂，其粘度25℃时为0.5-100厘泊；
0.1-25％非挥发性油，其粘度25度时为200-1,000,000厘泊；
0.1-10％水，和
0.1-70％干燥的特别物质，其颗粒大小为0.02-100微米。
在上述的组合物中，优选的是，非挥发性油是二甲基氢硅氧烷(dimethicone)，二甲基聚硅氧烷醇(dimethiconol)和氟硅氧烷。
化妆品可接受的载体也可以是眼影。眼影一般除含蜡和油以外还含有颜料或者粉末。优选的眼影组合物包括：
0.1-20％三甲基化二氧化硅；
0.1-30％挥发性溶剂，其粘度25℃时为0.5-100厘泊，
0.1-40％非挥发性油，
0.1-60％干燥特别物质，其颗粒大小为0.02-100微米。
在上述的眼影组合物中，优选的是挥发性溶剂包括环甲基聚硅氧烷(cyclomethicone)，而非挥发性油包括二甲基聚硅氧烷醇(dimethiconol)。
化妆品可接受的载体也可以是遮盖(物)霜，它一般包括颜料或粉末，蜡和其他成分，如湿润剂，稳定剂和其他上述的成分。本发明遮盖物优选的组份包括：
0.1-15％三甲基化二氧化硅；
0.1-40％挥发性溶剂，其粘度25℃时为0.5-100厘泊；
0.1-35％非挥发性油，其粘度25度时为350-1,000,000厘泊；
0.1-40％干燥特别物质，其颗粒大小为0.02-100微米。
在这一遮盖物组合物中，优选的是非挥发性油包括氟化硅，二甲基聚硅氧烷或其混合物。
化妆品可接受的载体也可以是口红，口红通常由蜡，油脂和颜料组成。优选的口红组合物包括：
0.1-60％三甲基化二氧化硅；
0.1-60％挥发性溶剂，
0.1-60％非挥发性油，
0.1-60％干燥特别物质，
0.1-40％蜡。
口红组合物另外可含有一或多种稳定剂，抗氧化剂，乳化剂，增稠剂等等。对应于这些组份可参见C.T.F.A.COSMETICHANDBOOK第一版1988。
本发明组合物提供了能粘附在皮肤上并显示出改进的抗转移性的化妆品。
以下将结合实施例详细描述本发明。
实施例1
按以下配制一种组合物：
                                             W/W％
1 环甲基聚硅氧烷/二甲基聚硅氧烷共聚醇        20.85
  (Cyclomethicone/dimehticone copolyol)
1 倍半油酸脱水山梨酸酯                       0.05
1 丙基对苯(propyl paraben)                   0.10
1 氧化钛/甲基聚硅氧烷(methicone)             8.00
1 红氧化铁/甲基聚硅氧烷(methicone)           0.47
1 黄氧化铁/甲基聚硅氧烷(methicone)           1.16
1 黑氧化铁/甲基聚硅氧烷(methicone)           0.18
1 云母/二聚硅氧烷(dimethicone)               0.98
2 尼龙12/卵磷质                              2.00
2 一氮化硼                                   4.00
3 环甲基聚硅氧烷(cyclomethicone)             1.00
3 二甲基聚硅氧烷(dimethicone)                1.50
3 Dow Corning 2-0747                         15.00
3 三山嵛精(tribehenin)                       2.00
4 松脂酸甘油酯/C9-11异链烷烃                 5.00
5 水                                         30.00
6 甲基对苯(Methyl paraben)                  0.20
6 三钠EDTA                                  0.20
6 丁二醇                                    4.50
7 SD醇40-B                                  3.00
在胶体磨中研磨顺序1的成份，一种接一种地进行，一直到无不分散的白色存在。然后，研磨顺序2的成份直到分散。在主烧瓶中混合顺序1和2的成份并加热到55-60℃。然后，加入顺序3的成份。当所有的三山嵛精熔化时，加入顺序4的成份。为形成水相，在一副烧瓶中，将顺序5的成份和顺序6的预混物加热到50-55℃。就在乳化之前，把顺序7的成份加入水相中。然后用均质机乳化水相和油相15分钟。浆轮混合器冷却混合物。
实施例2
按以下配制睫(眉)毛油：
                                            W/W％
巴西棕榈蜡                                  4.25
小烛树蜡                                    9.25
蜂蜡                                        4.60
合成蜡                                      4.85
BHA                                         0.05
丙基对苯                                    0.10
松脂酸甘油酯/C9-11异链烷烃                  12.00
羊毛脂酸                                    6.00
异十二烷                                    16.40
油醇                                        1.00
黑氧化铁                                    10.00
二氧化硅                                    4.50
聚乙烯                                      2.00
水                                          7.60
甲基对苯                                 0.35
钠EDTA                                   0.10
脱氢乙酸钠                               0.30
酵母糖蛋白                               1.00
水解角蛋白                               0.05
氢氧化氨                                 0.60
Dow Corning 2-0747                       15.00
按顺序混合各成份。
实施例3
按以下配制底色：
                                         W/W％
Dow Corning 2-747化妆液                  32.50
Dow Crning silastic Q7-4350
(氧化硅，甲基，甲基乙烯基硅氧烷)         5.50
二甲基聚硅氧烷(Dimethicone)/             3.00
二甲基聚硅氧烷醇(dimethicohol)
一氮化硼                                 5.00
滑石                                     4.00
水                                       2.00
乙基醇                                   3.00
氧化铁                                   3.00
红#30色淀                                1.80
二氧化钛                                 4.00
Quaternium 18 hectorite/
环甲基聚硅氧烷(cyclomethicone)           20.00
环甲基聚硅氧环(Cyclomethicone)           12.20
三氟丙基甲基聚硅氧烷                     4.00
(Dow Gorning FS-1265)
实施例4
按以下配制遮盖霜(CONCEALER)
                                      W/W/％
Dow Corning  2-0747                   20.00
氧化铁                                4.00
二氧化钛                              14.00
滑石                                  8.00
水                                    3.00
乙基醇                                3.00
Dow Corning Silastic Q7-4350          7.00
二甲基聚硅氧烷                        10.00
环甲基聚硅氧烷(Cyclomethicone)        19.00
三氟丙基甲基聚硅氧烷                  4.00
(Dow Corning FS-1265)
实施例5
按以下配制眼影：
                                      W/W％
滑石                                  22.41
云母                                  20.00
硬脂酸锌                              1.50
聚乙烯/滑石                           5.00
云母/二氧化钛                         10.00
聚乙烯                                1.50
氯氧化铋                              4.49
二氧化钛                              4.00
黑氧化铁                                0.15
黄氧化铁                                0.35
红氧化铁                                0.60
Dow Corning 2-0747                      22.00
环甲基聚硅氧硅烷(Cyclomethicone)        2.00
环甲基聚硅氧硅烷(Cyclomethicone)/
二甲基聚硅氧烷醇(dimethiconol)          3.00
椰锌酸酯癸酸酯                          3.00
实施例6
按以下配制防晒霜：
                                        W/W％
Dow Corning 2-0747                      30.00
氧化铁                                  3.50
二氧化钛                                20.00
氧化锌                                  5.00
一氮化硼                                8.00
Dow Corning Silastic Q7-4350            7.00
六甲基二硅氧烷                          10.00
环甲基聚硅氧烷(Cyclomethicone)          11.50
三氟丙基甲基聚硅氧烷                    5.00
实施例7
用实施例5(ES)的眼影配方进行分组试验。请三个试验者试用在眼皮上眼影。14个小时后，对眼影有如下评价：
                                     试验者数
                                    是       否眼影光滑，油腻感吗？                    3        0容易使用眼影吗？                        3        0眼影保藏良好吗？                        3        0眼影覆盖均匀吗？                        3        0外观好吗？                              3        0能保持多长时间？                        3        0
                                    12小时   -2试验者
                                    10小时   -1试验者

Claims (27)

1.一种化妆品组合物，它包括：
A)约0.1-60％重量的三甲基化的二氧化硅(TRIMETHYLATEDSILICA)，
B)约0.1-60％重量的挥发性溶剂，其粘度25℃时为0.5-100厘泊；
C)0.1-60％重量的非挥发性油脂，其粘度25℃时为200-1,000,000厘泊，和；
D)0.1-80％重量的化妆品可接受的载体。
2.如权利要求1所述的组合物，其中三甲基化的二氧化硅的平均颗粒大小为0.5-100毫微米。
3.如权利要求1或2所述的组合物，其中挥发性溶剂包括环状硅氧烷，线性硅氧烷，C8-20链烷烃，或者其混合物。
4.按上述任一权利要求所述的组合物，它包括：
A)0.5-50％重量的三甲基化的二氧化硅；
B)1-40％重量的挥发性硅氧烷；
C)0.1-40％重量的非挥发性油脂，和；
D)10-70％重量的化妆品可接受的载体；
其中，三甲基化的二氧化硅和挥发性硅氧烷作为液体配料，其粘度为400-700厘泊。
5.按上述任一权利要求所述的组合物，其中所述的化妆品可接受的载体是乳液(Lotion)形式。
6.按上述权利要求1至4所述的组合物，其中所述的化妆品可接受的载体是无水霜的(anhydrous cream)形式。
7.如权利要求6所述的组合物，它包括：
A)1-30％重量的三甲基化的二氧化硅；
B)1-40％重量的挥发性溶剂；
C)0.5-30％重量的非挥发性油脂，和；
D)0.1-70％重量干燥特别物质。
8.如权利要求1至3之一所述的组合物，其中所述的化妆品可接受的载体是面部扑粉(face powder)形式。
9.如权利要求8所述的组合物，具有如下配方：
A)0.1-60％重量的三甲基化的二氧化硅；
B)0.1-60％重量的挥发性溶剂；
C)0.1-60％重量的非挥发性油脂，和；
D)0.1-80％重量的在粉相中具有5-50％颜料的干燥特别物质。
10.如权利要求1至3之一所述的组合物，其中所述的化妆品可接受的载体是睫(眉)毛油的形式。
11.如权利要求10所述的组合物，它包括：
A)0.1-15％重量的三甲基化的二氧化硅；
B)0.1-40％重量的挥发性溶剂；
C)0.1-10％重量的非挥发性硅氧烷，和；
D)0.1-30％重量的在颗粒相中具有5-50％颜料的干燥特别物质。
E)0.1-20％膜形成剂；
F)0.1-30％蜡，和
G)0.1-10％乳化剂。
12.如权利要求1至3之一所述的组合物，其中所述的化妆品可接受的载体是水和油乳化配制品或基础物(FOUNDATION)。
13.如权利要求12所述的组合物，它包括：
0.1-20％重量的三甲基化的二氧化硅；
0.1-40％重量的挥发性溶剂；
0.1-25％重量的非挥发性油；
0.1-70％重量其颜料与粉末的比例为1∶20至20∶1的干燥特别物质；和
0.1-50％重量水。
14.如权利要求1至3之一所述的组合物，其中所述的化妆品可接受的载体是眼影。
15.如权利要求14所述的组合物，它包括：
0.1-20％重量的三甲基化的二氧化硅；
0.1-30％重量的挥发性溶剂；
0.1-40％重量的非挥发性油；和
0.1-60％重量的干燥特别物质。
16.如权利要求1至3之一所述的组合物，其中所述的化妆品可接受的载体是覆盖物。
17.如权利要求16所述的组合物，它包括：
0.1-15％重量的三甲基化的二氧化硅；
0.1-40％重量的挥发性溶剂；
0.1-35％重量的非挥发性油；和
0.1-40％重量的干燥特别物质。
18.如权利要求1至3之一所述的组合物，其中所述的化妆品可接受的载体是口红。
19.如权利要求18所述的组合物，它包括：
0.1-60％重量的三甲基化的二氧化硅；
0.1-60％重量的挥发性硅氧烷；
0.1-60％重量的非挥发性油；和
0.1-80％重量的干燥特别物质；和
0.1-40％重量的蜡。
20.一种如权利要求1至19所述的装入适当容器的化妆品组合物的化妆品产品。
21.一种制备前述任何权利要求所述的化妆品组合物的方法，包括：将
A)约0.1-约60％重量的三甲基化的二氧化硅，
B)约0.1-约60％重量的挥发性溶剂，其粘度25℃时为0.5-100厘泊；
C)约0.1-约60％重量的非挥发性油脂，其粘度25℃时为200-1,000,000厘泊，加入具有约0.1-约80％重量的化妆品可接受的载体的完全物理混合物中。
22.一种按权利要求1至20任何权利要求所述的，按权利要求21的方法制备的化妆品组合物。
23.A)约0.1-约60％重量的三甲基化的二氧化硅，
   B)约0.1-约60％重量的挥发性溶剂，其粘度25℃时为0.5-100厘泊；
   C)约0.1-约60％重量的非挥发性油脂，其粘度25℃时为200-1,000,000厘泊在制备改进化妆品的皮肤粘着性和/或抗转移性的化妆品组合物中的应用。
24.一种如说明书和实施例所描述的化妆品组合物，其制备方法，化妆品产品或用途。
25.如权利要求13所述的组合物，其中至少部分三甲基化的二氧化硅和挥发性溶剂被作为液体配料，其粘度为400-700厘泊。
26.如权利要求25所述的组合物，其中非挥发性油脂包括非氟化的硅氧烷，氟化的硅氧烷，前述通式RCO-OR’限定的酯，或者它们的混合物。
27.如权利要求26所述的组合物，其中干燥特别物质包括二氧化钛，氧化铁，云母，尼龙，一氮化硼，或者它们的混合物。
CN95118264A 1994-10-25 1995-10-25 化妆品组合物 Pending CN1127631A (zh)

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CN100413488C (zh) * 2000-12-12 2008-08-27 欧莱雅股份有限公司 含有至少一种杂聚物和至少一种成膜硅氧烷树脂的化妆用组合物及其使用方法
CN100421640C (zh) * 2003-12-03 2008-10-01 株式会社Lg生活健康 油包水形式的化妆品组合物
CN102065826A (zh) * 2008-03-25 2011-05-18 玫琳凯有限公司 皮脂吸收组合物
CN102065826B (zh) * 2008-03-25 2014-06-04 玫琳凯有限公司 皮脂吸收组合物
CN102753136A (zh) * 2009-11-20 2012-10-24 株式会社爱茉莉太平洋 包含无机粉末的化妆组合物
CN102753136B (zh) * 2009-11-20 2016-08-03 株式会社爱茉莉太平洋 包含无机粉末的化妆组合物
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CN103347483A (zh) * 2010-12-21 2013-10-09 莱雅公司 包含二氧化硅气凝胶颗粒和烃基油的化妆品组合物
CN103347483B (zh) * 2010-12-21 2017-06-20 莱雅公司 包含二氧化硅气凝胶颗粒和烃基油的化妆品组合物

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US20060088562A1 (en) 2006-04-27
NO954201D0 (no) 1995-10-20
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US5911974A (en) 1999-06-15
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