CN108884051A - 卤素取代的二酮化合物、吡唑化合物及用于制造吡唑化合物的方法 - Google Patents

卤素取代的二酮化合物、吡唑化合物及用于制造吡唑化合物的方法 Download PDF

Info

Publication number
CN108884051A
CN108884051A CN201780019913.XA CN201780019913A CN108884051A CN 108884051 A CN108884051 A CN 108884051A CN 201780019913 A CN201780019913 A CN 201780019913A CN 108884051 A CN108884051 A CN 108884051A
Authority
CN
China
Prior art keywords
compound
formula
group
alkyl
vii
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201780019913.XA
Other languages
English (en)
Chinese (zh)
Inventor
S.瓦斯曼
J.尧恩宙斯
S.莫罗斯
J.法布尔
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Solvay SA
Original Assignee
Solvay SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Solvay SA filed Critical Solvay SA
Publication of CN108884051A publication Critical patent/CN108884051A/zh
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D231/00Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/18One oxygen or sulfur atom
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C225/00Compounds containing amino groups and doubly—bound oxygen atoms bound to the same carbon skeleton, at least one of the doubly—bound oxygen atoms not being part of a —CHO group, e.g. amino ketones
    • C07C225/02Compounds containing amino groups and doubly—bound oxygen atoms bound to the same carbon skeleton, at least one of the doubly—bound oxygen atoms not being part of a —CHO group, e.g. amino ketones having amino groups bound to acyclic carbon atoms of the carbon skeleton
    • C07C225/14Compounds containing amino groups and doubly—bound oxygen atoms bound to the same carbon skeleton, at least one of the doubly—bound oxygen atoms not being part of a —CHO group, e.g. amino ketones having amino groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being unsaturated
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D231/00Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/12Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with only hydrogen atoms, hydrocarbon or substituted hydrocarbon radicals, directly attached to ring carbon atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
CN201780019913.XA 2016-01-28 2017-01-27 卤素取代的二酮化合物、吡唑化合物及用于制造吡唑化合物的方法 Pending CN108884051A (zh)

Applications Claiming Priority (7)

Application Number Priority Date Filing Date Title
EP16153112 2016-01-28
EP16153112.4 2016-01-28
EP16162487 2016-03-25
EP16162487.9 2016-03-25
EP16196175.0 2016-10-28
EP16196175 2016-10-28
PCT/EP2017/051797 WO2017129759A1 (en) 2016-01-28 2017-01-27 Halogen substituted diketones, pyrazole compounds and processes for the manufacture of pyrazole compounds

Publications (1)

Publication Number Publication Date
CN108884051A true CN108884051A (zh) 2018-11-23

Family

ID=57960426

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201780019913.XA Pending CN108884051A (zh) 2016-01-28 2017-01-27 卤素取代的二酮化合物、吡唑化合物及用于制造吡唑化合物的方法

Country Status (6)

Country Link
US (2) US10829456B2 (enExample)
EP (1) EP3408259A1 (enExample)
JP (1) JP2019504840A (enExample)
KR (1) KR20180108695A (enExample)
CN (1) CN108884051A (enExample)
WO (1) WO2017129759A1 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110461822A (zh) * 2017-03-27 2019-11-15 Agc株式会社 含卤素吡唑羧酸及其中间体的制造方法

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105541716B (zh) 2015-03-26 2024-02-23 Agc株式会社 吡唑衍生物的制造方法
EP3494107A1 (en) * 2016-08-02 2019-06-12 Solvay Sa Manufacture of hydrazinyl compounds useful in the manufacture of pyrazole carboxylic acid and derivatives, hydrazinyl compounds and their use
JP2020532524A (ja) 2017-09-04 2020-11-12 ソルヴェイ(ソシエテ アノニム) ジフルオロアセチルクロリドの製造方法及び製造中間体
CN107987021A (zh) * 2017-11-24 2018-05-04 上海应用技术大学 一种3-二氟甲基-1-甲基-1h-吡唑-4-羧酸的制备方法
EP3495351A1 (en) * 2017-12-08 2019-06-12 Solvay Sa Oxidation of a pyrazolyl ketone compound to the corresponding carboxylic acid
EP3728195A1 (en) * 2017-12-22 2020-10-28 Solvay Sa Process for the manufacture of pyrazole compounds
KR20200103744A (ko) * 2017-12-22 2020-09-02 솔베이(소시에떼아노님) 이미늄 화합물의 제조 방법 및 피라졸 유도체 제조에서의 이의 응용
US20210171468A1 (en) 2017-12-22 2021-06-10 Solvay Sa Process for the manufacture of pyrazole carboxylic derivatives and precursors thereof
CN110526810A (zh) * 2018-05-25 2019-12-03 浙江蓝天环保高科技股份有限公司 一种1,1,1-三氟-4-乙氧基戊-3-烯-2-酮的制备方法
EP3605699A1 (en) 2018-07-31 2020-02-05 Solvay Sa New components for electrolyte compositions

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0569912A1 (de) * 1992-05-15 1993-11-18 Hoechst Schering AgrEvo GmbH 4-Alkyl-substituierte Pyrimidin-5-carboxanilide, Verfahren zu deren Herstellung, diese enthaltende Mittel und deren Verwendung als Fungizide
US20050020564A1 (en) * 2003-05-01 2005-01-27 Atkinson Robert N. Pyrazole-amides and sulfonamides as sodium channel modulators
JP2006273844A (ja) * 2005-02-17 2006-10-12 Shionogi & Co Ltd 新規ベンゾジアゼピン類

Family Cites Families (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4342601A1 (de) 1993-08-13 1995-02-16 Solvay Fluor & Derivate Verfahren zur Herstellung von Poly- und Perfluorcarbonsäurechloriden
ES2119952T3 (es) 1993-12-23 1998-10-16 Solvay Fluor & Derivate Procedimiento para la preparacion de cloruros de acidos polifluoroclorocarboxilicos y perfluorocarboxilicos bajo adicion de cloro.
JP3632243B2 (ja) 1994-07-28 2005-03-23 旭硝子株式会社 ジフルオロ酢酸フルオリドおよびジフルオロ酢酸エステルの製造方法
US5905169A (en) 1995-03-20 1999-05-18 E. I. Du Pont De Nemours And Company Process for producing polyfluoroacyl compositions
US6248923B1 (en) 1999-09-03 2001-06-19 Eastman Chemical Company Process for the production of fluorocarboxylic acid anhydrides
DE10215292A1 (de) 2002-02-19 2003-08-28 Bayer Cropscience Ag Disubstitutierte Pyrazolylcarbocanilide
GB0224316D0 (en) 2002-10-18 2002-11-27 Syngenta Participations Ag Chemical compounds
MXPA05011775A (es) * 2003-05-01 2006-02-17 Abbott Lab Sulfonamidas y pirazolamidas como moduladores de canal de sodio.
DE10325715A1 (de) 2003-06-06 2004-12-23 Solvay Fluor Und Derivate Gmbh Vereinfachte Herstellung von Alkenonen
GB0418048D0 (en) 2004-08-12 2004-09-15 Syngenta Participations Ag Method for protecting useful plants or plant propagation material
DE102005007160A1 (de) 2005-02-16 2006-08-24 Basf Ag Pyrazolcarbonsäureanilide, Verfahren zu ihrer Herstellung und sie enthaltende Mittel zur Bekämpfung von Schadpilzen
JP2009501742A (ja) 2005-07-18 2009-01-22 シンジェンタ パーティシペーションズ アクチェンゲゼルシャフト 殺微生物剤としてのピラゾール−4−カルボキサミド誘導体
BRPI0616238B1 (pt) 2005-09-16 2016-01-19 Syngenta Ltd processo para a produção de amidas
AU2006308128B2 (en) 2005-10-25 2011-07-28 Syngenta Crop Protection Ag Heterocyclic amide derivatives useful as microbiocides
BRPI0812958A2 (pt) 2007-06-15 2014-12-09 Basf Se Processo para preparar compostos, uso de compostos, e, compostos
CN101801906A (zh) 2007-08-16 2010-08-11 索尔维公司 制备4-氟取代的3-氧代-烷酸酯的方法
CN102015653B (zh) 2008-05-02 2013-09-11 巴斯夫欧洲公司 制备卤素取代的2-(氨基亚甲基)-3-氧代丁酸酯的方法
CA2729362C (en) 2008-07-04 2016-09-27 Solvay Sa Process for the manufacture of alkenones
JP2010030970A (ja) 2008-07-31 2010-02-12 Bayer Cropscience Ag 殺虫性ベンゼンジカルボキサミド誘導体
EP2184273A1 (de) 2008-11-05 2010-05-12 Bayer CropScience AG Halogen-substituierte Verbindungen als Pestizide
CN103068805A (zh) 2010-07-23 2013-04-24 索尔维公司 1-取代-3-氟烷基-吡唑-4-羧酸酯的制备方法
US8987470B2 (en) 2010-10-27 2015-03-24 Solvay Sa Process for the preparation of pyrazole-4-carboxamides
EP2810931B1 (en) 2013-06-06 2018-04-25 Solvay SA Process for the preparation of halogenated carboxylic anhydrides
ITMI20132201A1 (it) 2013-12-23 2015-06-24 Isagro Spa Processo per la sintesi regioselettiva di pirazoli

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0569912A1 (de) * 1992-05-15 1993-11-18 Hoechst Schering AgrEvo GmbH 4-Alkyl-substituierte Pyrimidin-5-carboxanilide, Verfahren zu deren Herstellung, diese enthaltende Mittel und deren Verwendung als Fungizide
US20050020564A1 (en) * 2003-05-01 2005-01-27 Atkinson Robert N. Pyrazole-amides and sulfonamides as sodium channel modulators
JP2006273844A (ja) * 2005-02-17 2006-10-12 Shionogi & Co Ltd 新規ベンゾジアゼピン類

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
ETSUJI OKADA等: "FACILE SYNTHETIC METHODS FOR 3- AND 5-TRIFLUOROMETHY-4-TRIFLUOROACETYL PYRAZOLES AND THEIR CONVERSION INTO PYRAZOLE-4-CARBOXYLIC ACIDS", 《HETEROCYCLES》 *
FERNANDA A ROSA等: "N- and C-acylation in β-enamino ketones: structural effects on regiocontrol", 《SYNLETT》 *
NORIO OTA等: "A CONVENIENT SYNTHESIS OF FLUORINE-CONTAINING DIHYDROBENZO[b][1,4]DIAZEPINOLS AND ITS APPLICATION TO A SYNTHESIS OF NOVEL N-SULFINYLANILINES", 《HETEROCYCLES》 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110461822A (zh) * 2017-03-27 2019-11-15 Agc株式会社 含卤素吡唑羧酸及其中间体的制造方法

Also Published As

Publication number Publication date
US10829456B2 (en) 2020-11-10
WO2017129759A1 (en) 2017-08-03
KR20180108695A (ko) 2018-10-04
EP3408259A1 (en) 2018-12-05
JP2019504840A (ja) 2019-02-21
US20190031616A1 (en) 2019-01-31
US20210040043A1 (en) 2021-02-11

Similar Documents

Publication Publication Date Title
CN108884051A (zh) 卤素取代的二酮化合物、吡唑化合物及用于制造吡唑化合物的方法
CN104245676B (zh) 用于制备3,5-双(氟烷基)吡唑-4-甲酸衍生物和3,5-双(氟烷基)吡唑类化合物的方法
JP2019515938A (ja) 3−(ハロアルキルまたはホルミル)−1h−ピラゾール−4−カルボン酸またはエステルを含む組成物、その製造、およびカルボキサミド調製のためのその使用
WO2018024644A1 (en) Manufacture of hydrazinyl compounds useful in the manufacture of pyrazole carboxylic acid and derivatives, hydrazinyl compounds and their use
TWI651306B (zh) 自α,α-二鹵胺類與酮亞胺類製備3,5-雙(鹵烷基)吡唑衍生物之方法
US20190031617A1 (en) Process for the manufacture of carboxamides
TW201607928A (zh) 自α,α-二鹵胺製備3,5-雙鹵烷基吡唑衍生物之方法
CN111587241A (zh) 亚胺鎓化合物的制造方法及其在制造吡唑衍生物中的应用
CN106458918B (zh) 经由酮亚胺的酰化来制备3,5-双(卤代烷基)吡唑的方法
CN111587242A (zh) 用于制造吡唑化合物的方法
JP2021506879A (ja) ピラゾールカルボン酸誘導体及びその前駆体の製造のための方法
JPH0361664B2 (enExample)
TWI692470B (zh) 藉由腙之醯化製備3,5-雙(鹵烷基)吡唑衍生物之方法
TW202005957A (zh) 雙取代的3-吡唑羧酸酯及其經由烯醇酯醯化的製備方法
JP2004519456A (ja) 1−アルキル−3−アリール−5−ジフルオロメトキシ−1h−ピラゾールの製造方法

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20181123

WD01 Invention patent application deemed withdrawn after publication