CN108147980B - 通过二胺悬浮体的光气化制备二异氰酸酯的方法 - Google Patents

通过二胺悬浮体的光气化制备二异氰酸酯的方法 Download PDF

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Publication number
CN108147980B
CN108147980B CN201810140876.4A CN201810140876A CN108147980B CN 108147980 B CN108147980 B CN 108147980B CN 201810140876 A CN201810140876 A CN 201810140876A CN 108147980 B CN108147980 B CN 108147980B
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Prior art keywords
diamine
phosgene
suspension
diisocyanate
bar
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Chinese (zh)
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CN108147980A (zh
Inventor
J.劳厄
C.斯蒂芬斯
J.克劳泽
S.韦斯霍芬
W.基利安
M.泽坎普
M.鲁兰
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Covestro Deutschland AG
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Covestro Deutschland AG
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C263/00—Preparation of derivatives of isocyanic acid
    • C07C263/10—Preparation of derivatives of isocyanic acid by reaction of amines with carbonyl halides, e.g. with phosgene
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2602/00—Systems containing two condensed rings
    • C07C2602/02—Systems containing two condensed rings the rings having only two atoms in common
    • C07C2602/04—One of the condensed rings being a six-membered aromatic ring
    • C07C2602/10—One of the condensed rings being a six-membered aromatic ring the other ring being six-membered, e.g. tetraline

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Polyurethanes Or Polyureas (AREA)
CN201810140876.4A 2012-09-24 2013-09-18 通过二胺悬浮体的光气化制备二异氰酸酯的方法 Active CN108147980B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP12185575 2012-09-24
EP12185575.3 2012-09-24
CN201380049612.3A CN104640840B (zh) 2012-09-24 2013-09-18 通过二胺悬浮体的光气化制备二异氰酸酯的方法

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CN108147980A CN108147980A (zh) 2018-06-12
CN108147980B true CN108147980B (zh) 2020-10-23

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CN201380049612.3A Active CN104640840B (zh) 2012-09-24 2013-09-18 通过二胺悬浮体的光气化制备二异氰酸酯的方法

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US (1) US9272988B2 (OSRAM)
EP (1) EP2897933B1 (OSRAM)
JP (1) JP6225190B2 (OSRAM)
CN (2) CN108147980B (OSRAM)
ES (1) ES2639120T3 (OSRAM)
HU (1) HUE034355T2 (OSRAM)
WO (1) WO2014044699A1 (OSRAM)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110167913A (zh) 2017-01-18 2019-08-23 科思创德国股份有限公司 从蒸馏残余物中回收二异氰酸酯的方法
US10590069B2 (en) 2017-10-06 2020-03-17 International Business Machines Corporation Pinene-derived diisocyanates
CN109305930A (zh) * 2018-05-28 2019-02-05 江阴市万丰化工物资有限公司 3,3′-二甲基-4,4′-联苯二异氰酸酯的合成方法
EP3597632A1 (de) 2018-07-18 2020-01-22 Covestro Deutschland AG Verfahren zur rückgewinnung von diisocyanaten aus destillationsrückständen
EP3828213A1 (de) 2019-11-28 2021-06-02 Covestro Deutschland AG Schüttgut enthaltend feste diisocyanate und daraus erhältliche urethangruppen-enthaltende prepolymere
WO2021148419A1 (de) 2020-01-22 2021-07-29 Covestro Deutschland Ag Verfahren zur rückgewinnung von diisocyanaten aus destillationsrückständen
CN111349020A (zh) * 2020-05-06 2020-06-30 江苏快达农化股份有限公司 光气连续法制备3,3-二甲基-4,4-联苯二异氰酸酯的合成方法
CN115490829B (zh) * 2021-06-17 2025-04-01 万华化学集团股份有限公司 一种异氰酸酯组合物及其制备方法、一种光学材料
EP4227292A1 (de) 2022-02-10 2023-08-16 Covestro Deutschland AG Verfahren zur herstellung von isocyanaten
EP4227291A1 (de) 2022-02-10 2023-08-16 Covestro Deutschland AG Verfahren zur herstellung von isocyanaten
WO2023152039A1 (de) 2022-02-10 2023-08-17 Covestro Deutschland Ag Verfahren zur herstellung von isocyanaten
CN116178668B (zh) * 2023-01-03 2025-07-04 万华化学集团股份有限公司 一种萘二异氰酸酯组合物及其制备方法和应用

Citations (5)

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US3960916A (en) * 1975-01-24 1976-06-01 Basf Aktiengesellschaft Manufacture of organic isocyanates
JPS5759849A (en) * 1980-09-30 1982-04-10 Mitsui Toatsu Chem Inc Preparation of organic isocyanate by two-stage cooling and heating method
US4851571A (en) * 1987-05-21 1989-07-25 Bayer Aktiengesellschaft Process for the production of isocyanates
CN1575276A (zh) * 2001-10-23 2005-02-02 巴斯福股份公司 制备异氰酸酯的改进方法
WO2009013303A1 (de) * 2007-07-25 2009-01-29 Basf Se Kontinuierliches verfahren zur herstellung von isocyanaten

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CA832432A (en) 1970-01-20 Mobay Chemical Company Phosgenation of amines
DE949227C (de) 1953-03-27 1956-09-13 Bayer Ag Verfahren zur kontinuierlichen Herstellung von Isocyanaten
DE1175666B (de) 1955-03-17 1964-08-13 Toulousaine De Prod Chim Iatol Verfahren zur kontinuierlichen Herstellung von Isocyanaten
FR69428E (fr) 1955-03-17 1958-11-06 Le Ministre De La Defense Nationale Perfectionnements à la fabrication des isocyanates
US3054565A (en) 1955-08-12 1962-09-18 Willems Peter Kneading and mixing apparatus
DE1146872B (de) 1959-01-29 1963-04-11 Bayer Ag Verfahren zur Herstellung von organischen Isocyanaten
US3226410A (en) 1962-07-20 1965-12-28 Fmc Corp Continuous method of preparing aromatic isocyanates
US3321283A (en) 1963-12-23 1967-05-23 Mobay Chemical Corp Apparatus for conducting rapid chemical reactions
GB1120770A (en) * 1966-08-05 1968-07-24 Ici Ltd Manufacture of organic isocyanates
GB1238669A (OSRAM) 1968-03-12 1971-07-07
US3781320A (en) * 1971-02-09 1973-12-25 Du Pont Process for manufacture of organic isocyanates
DE2404774A1 (de) 1974-02-01 1975-08-21 Basf Ag Verfahren zur herstellung von organischen isocyanaten
DD132340B1 (de) 1975-09-23 1983-06-08 Hans Iben Verfahren zur phosgenierung von aminen zu mono-,di-und polyisocyanaten
JPS5823862B2 (ja) * 1978-07-10 1983-05-18 東レ株式会社 脂肪族トリイソシアネ−トの製造法
CA1137076A (en) 1978-12-13 1982-12-07 John R. Bauer Fluid spray mixer - reactor system
US4289732A (en) 1978-12-13 1981-09-15 The Upjohn Company Apparatus for intimately admixing two chemically reactive liquid components
DE3121036A1 (de) 1981-05-27 1982-12-16 Bayer Ag, 5090 Leverkusen Verfahren zur kontinuierlicehn herstellung von organischen mono- oder polyisocyanaten
DE3744001C1 (de) 1987-12-24 1989-06-08 Bayer Ag Verfahren zur kontinuierlichen Herstellung von Mono- oder Polyisocyanaten
DD300168A7 (de) 1988-12-21 1992-05-27 Schwarzheide Synthesewerk Veb Verfahren und Vorrichtung zur kontinuierlichen Umsetzung von Diaminodiphenylmethan/Polyamin-Gemischen mit Phosgen zu Polyisocyanaten
DE19651041A1 (de) 1996-12-09 1998-06-10 Bayer Ag Verfahren zur Herstellung von Isocyanaten aus schwerlöslichen primären Aminen
DE19720959B4 (de) * 1997-05-17 2004-08-26 Dorr-Oliver Deutschland Gmbh Rotor-Stator-Maschine
DE19800529A1 (de) 1998-01-09 1999-07-15 Bayer Ag Verfahren zur Phosgenierung von Aminen in der Gasphase unter Einsatz von Mikrostrukturmischern
DE10260082A1 (de) 2002-12-19 2004-07-01 Basf Ag Verfahren zur kontinuierlichen Herstellung von Isocyanaten
DE102005006765A1 (de) 2005-02-15 2006-08-17 Basf Ag Rotor/Stator-Vorrichtung und Verfahren zur salzfreien Koagulation von Polymerdispersionen
BRPI0610688A2 (pt) * 2005-04-08 2012-10-30 Huntsman Int Llc aparelho e processo para misturar pelo menos um primeiro e um segundo fluidos e processo para fabricar isocianatos
WO2008006775A1 (de) 2006-07-13 2008-01-17 Basf Se Verfahren zur herstellung von isocyanaten

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3960916A (en) * 1975-01-24 1976-06-01 Basf Aktiengesellschaft Manufacture of organic isocyanates
JPS5759849A (en) * 1980-09-30 1982-04-10 Mitsui Toatsu Chem Inc Preparation of organic isocyanate by two-stage cooling and heating method
US4851571A (en) * 1987-05-21 1989-07-25 Bayer Aktiengesellschaft Process for the production of isocyanates
CN1575276A (zh) * 2001-10-23 2005-02-02 巴斯福股份公司 制备异氰酸酯的改进方法
WO2009013303A1 (de) * 2007-07-25 2009-01-29 Basf Se Kontinuierliches verfahren zur herstellung von isocyanaten

Also Published As

Publication number Publication date
EP2897933B1 (de) 2017-06-07
CN104640840A (zh) 2015-05-20
ES2639120T3 (es) 2017-10-25
EP2897933A1 (de) 2015-07-29
US9272988B2 (en) 2016-03-01
CN104640840B (zh) 2018-03-02
HUE034355T2 (en) 2018-02-28
WO2014044699A1 (de) 2014-03-27
JP2015530395A (ja) 2015-10-15
US20150246873A1 (en) 2015-09-03
CN108147980A (zh) 2018-06-12
JP6225190B2 (ja) 2017-11-01

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