CN107406374B - 制备3-氯-2-乙烯基苯基磺酸酯的方法 - Google Patents

制备3-氯-2-乙烯基苯基磺酸酯的方法 Download PDF

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CN107406374B
CN107406374B CN201680013948.8A CN201680013948A CN107406374B CN 107406374 B CN107406374 B CN 107406374B CN 201680013948 A CN201680013948 A CN 201680013948A CN 107406374 B CN107406374 B CN 107406374B
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CN107406374A (zh
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P·布鲁克纳
T·希姆勒
S·帕斯诺克
M·J·福特
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Bayer CropScience AG
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    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/42Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by hydrolysis
    • C07C45/43Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by hydrolysis of >CX2 groups, X being halogen
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    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/26Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of esters of sulfonic acids
    • C07C303/28Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of esters of sulfonic acids by reaction of hydroxy compounds with sulfonic acids or derivatives thereof
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    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/26Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of esters of sulfonic acids
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    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C309/00Sulfonic acids; Halides, esters, or anhydrides thereof
    • C07C309/63Esters of sulfonic acids
    • C07C309/64Esters of sulfonic acids having sulfur atoms of esterified sulfo groups bound to acyclic carbon atoms
    • C07C309/65Esters of sulfonic acids having sulfur atoms of esterified sulfo groups bound to acyclic carbon atoms of a saturated carbon skeleton
    • C07C309/66Methanesulfonates
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    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C309/00Sulfonic acids; Halides, esters, or anhydrides thereof
    • C07C309/63Esters of sulfonic acids
    • C07C309/64Esters of sulfonic acids having sulfur atoms of esterified sulfo groups bound to acyclic carbon atoms
    • C07C309/67Esters of sulfonic acids having sulfur atoms of esterified sulfo groups bound to acyclic carbon atoms of an unsaturated carbon skeleton
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/001Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by modification in a side chain
    • C07C37/002Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by modification in a side chain by transformation of a functional group, e.g. oxo, carboxyl
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/11Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by reactions increasing the number of carbon atoms
    • C07C37/20Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by reactions increasing the number of carbon atoms using aldehydes or ketones
    • CCHEMISTRY; METALLURGY
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    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C39/00Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring
    • C07C39/24Halogenated derivatives
    • C07C39/245Halogenated derivatives monocyclic polyhydroxylic containing halogens bound to ring carbon atoms
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    • C07C39/00Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring
    • C07C39/24Halogenated derivatives
    • C07C39/26Halogenated derivatives monocyclic monohydroxylic containing halogen bound to ring carbon atoms
    • C07C39/27Halogenated derivatives monocyclic monohydroxylic containing halogen bound to ring carbon atoms all halogen atoms being bound to ring carbon atoms
    • C07C39/28Halogenated derivatives monocyclic monohydroxylic containing halogen bound to ring carbon atoms all halogen atoms being bound to ring carbon atoms the halogen being one chlorine atom
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C47/00Compounds having —CHO groups
    • C07C47/52Compounds having —CHO groups bound to carbon atoms of six—membered aromatic rings
    • C07C47/56Compounds having —CHO groups bound to carbon atoms of six—membered aromatic rings containing hydroxy groups
    • C07C47/565Compounds having —CHO groups bound to carbon atoms of six—membered aromatic rings containing hydroxy groups all hydroxy groups bound to the ring
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/08Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/14Preparation of carboxylic acid esters from carboxylic acid halides
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/28Preparation of carboxylic acid esters by modifying the hydroxylic moiety of the ester, such modification not being an introduction of an ester group
    • C07C67/287Preparation of carboxylic acid esters by modifying the hydroxylic moiety of the ester, such modification not being an introduction of an ester group by introduction of halogen; by substitution of halogen atoms by other halogen atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C68/00Preparation of esters of carbonic or haloformic acids
    • C07C68/02Preparation of esters of carbonic or haloformic acids from phosgene or haloformates
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C68/00Preparation of esters of carbonic or haloformic acids
    • C07C68/06Preparation of esters of carbonic or haloformic acids from organic carbonates
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    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/62Halogen-containing esters
    • C07C69/63Halogen-containing esters of saturated acids
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    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/62Halogen-containing esters
    • C07C69/65Halogen-containing esters of unsaturated acids
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/96Esters of carbonic or haloformic acids

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN201680013948.8A 2015-03-05 2016-02-29 制备3-氯-2-乙烯基苯基磺酸酯的方法 Active CN107406374B (zh)

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Application Number Priority Date Filing Date Title
EP15157832.5 2015-03-05
EP15157832 2015-03-05
PCT/EP2016/054189 WO2016139161A1 (en) 2015-03-05 2016-02-29 Process for preparing 3-chloro-2-vinylphenylsulfonates

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CN107406374A CN107406374A (zh) 2017-11-28
CN107406374B true CN107406374B (zh) 2020-07-14

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US (1) US10618872B2 (https=)
EP (1) EP3265439B1 (https=)
JP (1) JP6771475B2 (https=)
KR (1) KR102595410B1 (https=)
CN (1) CN107406374B (https=)
BR (1) BR112017018993B1 (https=)
DK (1) DK3265439T3 (https=)
ES (1) ES2732045T3 (https=)
IL (1) IL253877B (https=)
MX (1) MX389099B (https=)
TW (1) TWI695824B (https=)
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Publication number Priority date Publication date Assignee Title
WO2018104105A1 (de) 2016-12-05 2018-06-14 Bayer Cropscience Aktiengesellschaft Verfahren zur herstellung von 3-substituierten 2-vinylphenylsulfonaten
CN107043321B (zh) * 2017-04-25 2021-01-15 连云港市工业投资集团有限公司 一种高选择性合成2,3-二氯苯甲醛的方法
CN108911982B (zh) * 2018-07-19 2022-08-26 徐州博康信息化学品有限公司 一种合成酰氧基取代的苯乙烯类化合物的环保方法
CN111416150A (zh) * 2020-02-28 2020-07-14 合肥国轩高科动力能源有限公司 一种含氟磺酸酯类锂离子电池添加剂的制备方法
WO2023007426A1 (en) 2021-07-29 2023-02-02 Pi Industries Ltd. Novel styrene compounds and a process for the preparation thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5424460A (en) * 1991-04-17 1995-06-13 Rhone-Poulenc Chimie Synthesis intermediates containing a hexane ring and processes for their preparation
WO2014206896A1 (en) * 2013-06-24 2014-12-31 Bayer Cropscience Ag Piperidinecarboxylic acid derivatives as fungicides
WO2014207648A1 (en) * 2013-06-24 2014-12-31 Lupin Limited Chromane and chromene derivatives and their use as crac modulators

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US5124460A (en) 1991-05-06 1992-06-23 Merck Sharp & Dohme Ltd. Enantioselective synthesis of 3-substituted 1-azabicyclo (2.2.1)heptanes
KR19990014856A (ko) * 1995-05-17 1999-02-25 미디암 디, 메코너헤이 살진균성 시클릭 아미드
DE10021413A1 (de) 2000-05-03 2001-11-08 Bayer Ag Verfahren zur Herstellung von 2-Alkyl-3-chlorphenolen
EP2358716B1 (en) * 2008-11-12 2016-01-06 Merck Sharp & Dohme Corp. Inhibitors of fatty acid binding protein (fabp)
EP2445891A4 (en) 2009-06-26 2012-11-14 Glaxo Group Ltd 5-CHAIN HETEROARYL DERIVATIVES AS SPHINOSINE-1-PHOSPHATE RECEPTOR AGONISTS
MX2012007200A (es) 2009-12-21 2012-07-10 Bayer Cropscience Ag Bis(difluorometil)pirazoles como fungicidas.
EP2547662A4 (en) 2010-03-17 2013-10-02 Glaxo Group Ltd PYRIMIDINE DERIVATIVES FOR USE AS AGONISTS OF SPHINGOSIN 1-PHOSPHATE 1 (S1P1) RECEPTORS
TWI665192B (zh) 2014-05-28 2019-07-11 德商拜耳作物科學股份有限公司 製備二氫異唑衍生物之方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5424460A (en) * 1991-04-17 1995-06-13 Rhone-Poulenc Chimie Synthesis intermediates containing a hexane ring and processes for their preparation
WO2014206896A1 (en) * 2013-06-24 2014-12-31 Bayer Cropscience Ag Piperidinecarboxylic acid derivatives as fungicides
WO2014207648A1 (en) * 2013-06-24 2014-12-31 Lupin Limited Chromane and chromene derivatives and their use as crac modulators

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
"Ortho-Vinylation Reaction of Phenols with Ethyne";Masahiko Yamaguchi等;《J. Org. Chem.》;19980919;第63卷;第7298-7305页 *

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EP3265439B1 (en) 2019-03-27
BR112017018993B1 (pt) 2021-08-10
IL253877B (en) 2020-03-31
KR102595410B1 (ko) 2023-10-27
US10618872B2 (en) 2020-04-14
US20180079717A1 (en) 2018-03-22
TWI695824B (zh) 2020-06-11
KR20170126939A (ko) 2017-11-20
MX389099B (es) 2025-03-20
JP6771475B2 (ja) 2020-10-21
WO2016139161A1 (en) 2016-09-09
EP3265439A1 (en) 2018-01-10
DK3265439T3 (da) 2019-06-11
MX2017011389A (es) 2018-03-16
JP2018507871A (ja) 2018-03-22
CN107406374A (zh) 2017-11-28
TW201643135A (zh) 2016-12-16
ES2732045T3 (es) 2019-11-20
IL253877A0 (en) 2017-10-31
BR112017018993A2 (pt) 2018-04-17

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