TWI695824B - 製備3-氯-2-乙烯基苯基磺酸酯之方法 - Google Patents

製備3-氯-2-乙烯基苯基磺酸酯之方法 Download PDF

Info

Publication number
TWI695824B
TWI695824B TW105106437A TW105106437A TWI695824B TW I695824 B TWI695824 B TW I695824B TW 105106437 A TW105106437 A TW 105106437A TW 105106437 A TW105106437 A TW 105106437A TW I695824 B TWI695824 B TW I695824B
Authority
TW
Taiwan
Prior art keywords
chloro
formula
compound
ccl
patent application
Prior art date
Application number
TW105106437A
Other languages
English (en)
Chinese (zh)
Other versions
TW201643135A (zh
Inventor
彼得 布朗其爾
湯姆斯 喜米勒
塞爾吉 佩濟諾克
馬克 福特
Original Assignee
德商拜耳作物科學股份有限公司
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 德商拜耳作物科學股份有限公司 filed Critical 德商拜耳作物科學股份有限公司
Publication of TW201643135A publication Critical patent/TW201643135A/zh
Application granted granted Critical
Publication of TWI695824B publication Critical patent/TWI695824B/zh

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/42Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by hydrolysis
    • C07C45/43Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by hydrolysis of >CX2 groups, X being halogen
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/26Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of esters of sulfonic acids
    • C07C303/28Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of esters of sulfonic acids by reaction of hydroxy compounds with sulfonic acids or derivatives thereof
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/26Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of esters of sulfonic acids
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C309/00Sulfonic acids; Halides, esters, or anhydrides thereof
    • C07C309/63Esters of sulfonic acids
    • C07C309/64Esters of sulfonic acids having sulfur atoms of esterified sulfo groups bound to acyclic carbon atoms
    • C07C309/65Esters of sulfonic acids having sulfur atoms of esterified sulfo groups bound to acyclic carbon atoms of a saturated carbon skeleton
    • C07C309/66Methanesulfonates
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C309/00Sulfonic acids; Halides, esters, or anhydrides thereof
    • C07C309/63Esters of sulfonic acids
    • C07C309/64Esters of sulfonic acids having sulfur atoms of esterified sulfo groups bound to acyclic carbon atoms
    • C07C309/67Esters of sulfonic acids having sulfur atoms of esterified sulfo groups bound to acyclic carbon atoms of an unsaturated carbon skeleton
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/001Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by modification in a side chain
    • C07C37/002Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by modification in a side chain by transformation of a functional group, e.g. oxo, carboxyl
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/11Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by reactions increasing the number of carbon atoms
    • C07C37/20Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by reactions increasing the number of carbon atoms using aldehydes or ketones
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C39/00Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring
    • C07C39/24Halogenated derivatives
    • C07C39/245Halogenated derivatives monocyclic polyhydroxylic containing halogens bound to ring carbon atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C39/00Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring
    • C07C39/24Halogenated derivatives
    • C07C39/26Halogenated derivatives monocyclic monohydroxylic containing halogen bound to ring carbon atoms
    • C07C39/27Halogenated derivatives monocyclic monohydroxylic containing halogen bound to ring carbon atoms all halogen atoms being bound to ring carbon atoms
    • C07C39/28Halogenated derivatives monocyclic monohydroxylic containing halogen bound to ring carbon atoms all halogen atoms being bound to ring carbon atoms the halogen being one chlorine atom
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C47/00Compounds having —CHO groups
    • C07C47/52Compounds having —CHO groups bound to carbon atoms of six—membered aromatic rings
    • C07C47/56Compounds having —CHO groups bound to carbon atoms of six—membered aromatic rings containing hydroxy groups
    • C07C47/565Compounds having —CHO groups bound to carbon atoms of six—membered aromatic rings containing hydroxy groups all hydroxy groups bound to the ring
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/08Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/14Preparation of carboxylic acid esters from carboxylic acid halides
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/28Preparation of carboxylic acid esters by modifying the hydroxylic moiety of the ester, such modification not being an introduction of an ester group
    • C07C67/287Preparation of carboxylic acid esters by modifying the hydroxylic moiety of the ester, such modification not being an introduction of an ester group by introduction of halogen; by substitution of halogen atoms by other halogen atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C68/00Preparation of esters of carbonic or haloformic acids
    • C07C68/02Preparation of esters of carbonic or haloformic acids from phosgene or haloformates
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C68/00Preparation of esters of carbonic or haloformic acids
    • C07C68/06Preparation of esters of carbonic or haloformic acids from organic carbonates
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/62Halogen-containing esters
    • C07C69/63Halogen-containing esters of saturated acids
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/62Halogen-containing esters
    • C07C69/65Halogen-containing esters of unsaturated acids
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/96Esters of carbonic or haloformic acids

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
TW105106437A 2015-03-05 2016-03-03 製備3-氯-2-乙烯基苯基磺酸酯之方法 TWI695824B (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP15157832.5 2015-03-05
EP15157832 2015-03-05

Publications (2)

Publication Number Publication Date
TW201643135A TW201643135A (zh) 2016-12-16
TWI695824B true TWI695824B (zh) 2020-06-11

Family

ID=52736817

Family Applications (1)

Application Number Title Priority Date Filing Date
TW105106437A TWI695824B (zh) 2015-03-05 2016-03-03 製備3-氯-2-乙烯基苯基磺酸酯之方法

Country Status (12)

Country Link
US (1) US10618872B2 (https=)
EP (1) EP3265439B1 (https=)
JP (1) JP6771475B2 (https=)
KR (1) KR102595410B1 (https=)
CN (1) CN107406374B (https=)
BR (1) BR112017018993B1 (https=)
DK (1) DK3265439T3 (https=)
ES (1) ES2732045T3 (https=)
IL (1) IL253877B (https=)
MX (1) MX389099B (https=)
TW (1) TWI695824B (https=)
WO (1) WO2016139161A1 (https=)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2018104105A1 (de) 2016-12-05 2018-06-14 Bayer Cropscience Aktiengesellschaft Verfahren zur herstellung von 3-substituierten 2-vinylphenylsulfonaten
CN107043321B (zh) * 2017-04-25 2021-01-15 连云港市工业投资集团有限公司 一种高选择性合成2,3-二氯苯甲醛的方法
CN108911982B (zh) * 2018-07-19 2022-08-26 徐州博康信息化学品有限公司 一种合成酰氧基取代的苯乙烯类化合物的环保方法
CN111416150A (zh) * 2020-02-28 2020-07-14 合肥国轩高科动力能源有限公司 一种含氟磺酸酯类锂离子电池添加剂的制备方法
WO2023007426A1 (en) 2021-07-29 2023-02-02 Pi Industries Ltd. Novel styrene compounds and a process for the preparation thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5817890A (en) * 1991-04-17 1998-10-06 Rhone-Poulenc Chimie Process for preparation of halogenated or pseudohalogenated cyclic organic compounds
WO2014206896A1 (en) * 2013-06-24 2014-12-31 Bayer Cropscience Ag Piperidinecarboxylic acid derivatives as fungicides

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5124460A (en) 1991-05-06 1992-06-23 Merck Sharp & Dohme Ltd. Enantioselective synthesis of 3-substituted 1-azabicyclo (2.2.1)heptanes
KR19990014856A (ko) * 1995-05-17 1999-02-25 미디암 디, 메코너헤이 살진균성 시클릭 아미드
DE10021413A1 (de) 2000-05-03 2001-11-08 Bayer Ag Verfahren zur Herstellung von 2-Alkyl-3-chlorphenolen
EP2358716B1 (en) * 2008-11-12 2016-01-06 Merck Sharp & Dohme Corp. Inhibitors of fatty acid binding protein (fabp)
EP2445891A4 (en) 2009-06-26 2012-11-14 Glaxo Group Ltd 5-CHAIN HETEROARYL DERIVATIVES AS SPHINOSINE-1-PHOSPHATE RECEPTOR AGONISTS
MX2012007200A (es) 2009-12-21 2012-07-10 Bayer Cropscience Ag Bis(difluorometil)pirazoles como fungicidas.
EP2547662A4 (en) 2010-03-17 2013-10-02 Glaxo Group Ltd PYRIMIDINE DERIVATIVES FOR USE AS AGONISTS OF SPHINGOSIN 1-PHOSPHATE 1 (S1P1) RECEPTORS
US9790231B2 (en) * 2013-06-24 2017-10-17 Lupin Limited Chromane and chromene derivatives and their use as CRAC modulators
TWI665192B (zh) 2014-05-28 2019-07-11 德商拜耳作物科學股份有限公司 製備二氫異唑衍生物之方法

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5817890A (en) * 1991-04-17 1998-10-06 Rhone-Poulenc Chimie Process for preparation of halogenated or pseudohalogenated cyclic organic compounds
WO2014206896A1 (en) * 2013-06-24 2014-12-31 Bayer Cropscience Ag Piperidinecarboxylic acid derivatives as fungicides

Also Published As

Publication number Publication date
EP3265439B1 (en) 2019-03-27
BR112017018993B1 (pt) 2021-08-10
IL253877B (en) 2020-03-31
KR102595410B1 (ko) 2023-10-27
US10618872B2 (en) 2020-04-14
US20180079717A1 (en) 2018-03-22
KR20170126939A (ko) 2017-11-20
CN107406374B (zh) 2020-07-14
MX389099B (es) 2025-03-20
JP6771475B2 (ja) 2020-10-21
WO2016139161A1 (en) 2016-09-09
EP3265439A1 (en) 2018-01-10
DK3265439T3 (da) 2019-06-11
MX2017011389A (es) 2018-03-16
JP2018507871A (ja) 2018-03-22
CN107406374A (zh) 2017-11-28
TW201643135A (zh) 2016-12-16
ES2732045T3 (es) 2019-11-20
IL253877A0 (en) 2017-10-31
BR112017018993A2 (pt) 2018-04-17

Similar Documents

Publication Publication Date Title
TWI695824B (zh) 製備3-氯-2-乙烯基苯基磺酸酯之方法
JP5721720B2 (ja) メチレンジスルホネート化合物の製造方法
RU2539578C1 (ru) Способ получения 4-амино-3-хлор-5-фтор-6-(замещенных)пиколинатов
JP2025026926A (ja) 特定の殺線虫性スルホンアミドを調製するためのプロセス及び中間体
KR20180034862A (ko) 환상 1,3-프로펜 설톤의 제조방법
KR20210005663A (ko) 방향족 니트릴 화합물의 제조 방법
KR20090108934A (ko) 1,3-프로펜설톤의 제조방법
JP2003335735A (ja) パーフルオロイソプロピルアニリン類の製造方法
KR102695101B1 (ko) 화학선택적 티오에테르 산화에 의한 2-알킬-4-트리플루오로메틸-3-알킬설포닐벤조산의 제조 방법
JP2020537680A (ja) 除草性ピリダジノン化合物を製造するプロセス
EP1873145B1 (en) Method for producing nicotinic acid derivative or salt thereof
WO2010122793A1 (ja) ピラジン誘導体の製造方法及びその中間体
KR102546866B1 (ko) 3-치환된 2-비닐페닐 설포네이트의 제조 방법
TW202321195A (zh) (2,2,2-三氟乙基)硫烷基苯胺衍生物的製備方法
TW202542121A (zh) 經取代的1-(4-(5-(鹵甲基)-1,2,4-噁二唑-3-基)苯基)乙烷-1-酮的製備方法
CN85105925A (zh) N-苯基(吡啶基)磺酰二胺的制备方法
JPH01117849A (ja) 2,6‐ジハロアニリン誘導体の製造方法
KR20070086762A (ko) 티오카르바메이트 유도체의 제조방법
KR20050108739A (ko) E형의 2-벤조일-3-디메틸아미노아크릴레이트 유도체의 제조방법
EP0791583A1 (en) Process for producing 3-(aminomethyl)-6-chloropyridines
HK1114084B (en) Method for producing thiocarbamate derivative
JPS62240661A (ja) 2−ハロ−4−ピリジルケトンオキシム及びその誘導体
JPH05230010A (ja) パラクロロフェニルカルバミン酸エステルの製造方法
JPH05294931A (ja) 新規中間体及び2−クロロ−5−(アミノメチル)ピリジンの製造方法
JP2006137711A (ja) ピリジン誘導体の製造方法