CN105193920A - Freshly squeezed vacuum drying peppermint powdery decoction pieces and preparation process thereof - Google Patents
Freshly squeezed vacuum drying peppermint powdery decoction pieces and preparation process thereof Download PDFInfo
- Publication number
- CN105193920A CN105193920A CN201510774854.XA CN201510774854A CN105193920A CN 105193920 A CN105193920 A CN 105193920A CN 201510774854 A CN201510774854 A CN 201510774854A CN 105193920 A CN105193920 A CN 105193920A
- Authority
- CN
- China
- Prior art keywords
- vacuum drying
- herba menthae
- peppermint
- decoction pieces
- carrying
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses freshly squeezed vacuum drying peppermint powdery decoction pieces and a preparation process thereof. The process is characterized by harvesting the medicinal material peppermint, then cleaning, selecting and drip-washing peppermint, squeezing peppermint while peppermint is fresh and taking the juice after filtration; adding water to the dregs, stirring the dregs and carrying out filtering and squeezing; mixing the obtained juice and then carrying out vacuum concentration, and carrying out vacuum drying; concentrating condensate, separating volatile oil, mixing the volatile oil with a vacuum drying product and carrying out sieving and bagging. The peppermint powdery decoction pieces prepared by the method furthest retain the active ingredients in the medicinal material, are easy to store and transport and convenient to regulate, are controllable in quality, have reliable curative effects and have great significance in guaranteeing the clinical effects of traditional Chinese medicines. Popularization and implementation of the method has remarkable social significance and economic benefits.
Description
Technical field
The invention belongs to Chinese crude drug manufacture field, particularly relate to the processing technique of Chinese medicine Herba Menthae decoction pieces.
Background technology
Chinese medicine Herba Menthae is labiate Herba Menthae
menthahaplocalyxbriq. dry aerial parts.This product is pungent, cool, returns lung, Liver Channel.There is dispelling wind and heat pathogens, the clear sharp head, sore-throat relieving, rash, the functions such as soothing the liver circulation of qi promoting.Be mainly used in anemopyretic cold, headache, conjunctival congestion, sore throat, aphtha, rubella, measles, breast side of body feeling of distension and oppression etc.
The processing mode of conventional Herba Menthae decoction pieces is: the summer, season in autumn two stem and leaf luxuriant or the flowers are in blossom to three-wheel time, select fine day, gradation is tapped, and dries or dries in the shade, then packing storage and transport.After these Herba Menthae medical materials of packing are transported to prepared slices of Chinese crude drugs factory, need drip washing, section, and redry or dry in the shade.Existing technique time and effort consuming, operation repeats, and adds the production cost of decoction pieces.In this accumulating and the course of processing, the loss that its volatile effective component be rich in is a large amount of, thus cause the decline of medical material quanlity and the reduction of clinical efficacy.This type of prepared herbal medicine in small pieces ready for decoction, bulky, easily pollute and go mouldy, quality is difficult to ensure, is unfavorable for that formula is adjusted and guarantees its clinical efficacy.
At present, granule pieces market also having Herba Menthae medical material to make after extracting is sold.Due in granule pieces preparation process, extract not only time consumption and energy consumption, and do solvent because commonly using water, the nonpolar effective ingredient in medical material is difficult to be extracted.Or collect its volatile oil with steam distillation, due to long-time heating in process, very large to the stability influence of its aqueous soluble active constituent again.In addition, because the Herba Menthae medical material extracted also is dry also through long-time storage, therefore, in this process, the loss of effective ingredient is also very large.In order to ensure clinical effective, the steady quality of Herba Menthae medical material, a kind of novel Herba Menthae decoction pieces and preparation technology thereof urgently develop.
Summary of the invention
The present invention discloses " a kind of Herba Menthae fresh squeezing vacuum drying powder decoction pieces and preparation technology thereof ".This technique can retain polarity in Herba Menthae medical material and nonpolar effective ingredient to greatest extent, the loss of effective ingredient avoiding medical material to cause in existing decoction pieces processing and storage and transport process and the decline of medical material quanlity, reduce the pollution of medical material by mycete etc., the steady quality and clinical safety guaranteeing Herba Menthae decoction pieces is effectively had great importance.
To achieve these goals, technical scheme of the present invention is:
Gather its aerial parts collection period Herba Menthae, clean, after robbing water wash, take advantage of fresh squeezing extracting juice, medicinal residues add the water of 1 ~ 3 times amount, and stir 5 ~ 30min, filter press filter pressing, gained medicinal residues squeeze extracting juice again, merge medicine juice and filter with 80 ~ 120 eye mesh screens.By the medicinal liquid of gained, in 40 ~ 75 DEG C of concentrating under reduced pressure, gained relative density be 1.05 ~ 1.30 extractum pulverize after 4 ~ 8 hours in 40 ~ 70 DEG C of vacuum dryings.Collect the Herba Menthae condensed water of gained in concentrating under reduced pressure process, add the NaCl of 1% ~ 5% weight, be stirred to dissolve, solution is put in oil water separator, places 12 ~ 48 hours under 4 DEG C ~ 10 DEG C environment, collects top oil reservoir, and toward wherein adding the anhydrous Na of 1% ~ 5% weight
2sO
4, after jolting 5 ~ 10min clock, less than 25 DEG C room temperatures are placed 1 ~ 6 hour, filter, obtain Herba Menthae Haplocalycis volatile oil, and it mixed homogeneously with above-mentioned Herba Menthae vacuum drying powder, and cross 40 ~ 100 mesh sieves, vacuum packaging, obtains Herba Menthae fresh squeezing vacuum drying powder decoction pieces.
On the label of product packaging bags, the name of an article in printing, medicinal part, planting site, manufacturer, date of manufacture, Contents of Main Components, meridian distribution of property and flavor, function cure mainly, the information such as usage and dosage, toxic and side effects and contraindication.TLC distinguish collection of illustrative plates and/or the high-efficient liquid phase character collection of illustrative plates of Herba Menthae is enclosed, as " identity card " of product in bag.In addition, in the packaging bag of product, be printed on Quick Response Code, the information such as former plant photo, medical material photo, decoction pieces photo, character and the microscopical identification feature obtaining product can be linked by scanning.Herba Menthae fresh squeezing vacuum drying powder decoction pieces, faces before taking and adds after Chinese medicine decoction is decocted, when decreasing decoction decocting, and the trouble under after the Herba Menthae in prescription needs, significant to reservation volatile ingredient.
Usefulness of the present invention is:
Fresh mint medical material cleans directly cutting squeezing after washing, filtration, concentrating under reduced pressure, vacuum drying, separating oil, mixing, the powder decoction pieces obtained, can effective ingredient to greatest extent in complete reservation medical material.This decoction pieces volume compares to traditional decoction pieces volume and reduces widely, and volatile ingredient retains complete, and quality is more stable, is beneficial to accumulating and clinical adjustment, has very significant social meaning and economic implications.
Detailed description of the invention
Embodiment 1
By the Herba Menthae medical material of fresh collection, clean, rob water wash, take advantage of the squeezing of using fresh herb squeezer, extracting juice.Gained medicinal residues add the tap water of 2 times amount, stir 20min, filter press squeezing extracting juice.Gained medicinal residues squeeze medicine juice with squeezer again.Merged by above-mentioned 3 medicine juice, concentrating under reduced pressure, temperature is set as 65 DEG C.When concentrated gained extractum relative density is 1.15, transfers in vacuum drying oven, in 60 DEG C of dryings 6 hours, obtain vacuum drying thing.In addition, by the Herba Menthae condensed water collected during concentrating under reduced pressure, add the NaCl of weight 5%, be stirred to dissolve.This solution is positioned in oil water separator, and in 10 DEG C of environment, leaves standstill 24 hours, separated and collected upper strata volatile oil.The anhydrous Na of 2% weight is added in this volatile oil
2sO
4, after jolting 10min clock, less than 25 DEG C room temperatures place 6 hours, filter, obtain Herba Menthae Haplocalycis volatile oil.Mixed homogeneously with above-mentioned Herba Menthae vacuum drying thing by this volatile oil, cross 60 mesh sieves, pack, 1kg/ bag, add packed antioxidant and desiccant, Vacuum Package, labeling gets product.
Embodiment 2
By the Herba Menthae medical material of fresh collection, clean, with water wash, be cut into the section that 10cm is long, take advantage of the squeezing of using fresh herb squeezer, extracting juice.Gained medicinal residues add the drinking water of 3 times amount, stir 30min, filter press squeezing extracting juice.Gained medicinal residues squeeze medicine juice with squeezer again.Merged by above-mentioned 3 medicine juice, concentrating under reduced pressure, temperature is set as 60 DEG C.When concentrated gained extractum relative density is 1.10, transfers in vacuum drying oven, in 60 DEG C of dryings 8 hours, obtain vacuum drying thing.In addition, by the Herba Menthae condensed water collected during concentrating under reduced pressure, add the NaCl of weight 3%, be stirred to dissolve.This solution is positioned in oil water separator, and leaves standstill 24 hours in 10 DEG C of environment, separated and collected upper strata volatile oil.The anhydrous Na of 5% weight is added in this volatile oil
2sO
4, after jolting 5min clock, less than 25 DEG C room temperatures place 12 hours, filter, obtain Herba Menthae Haplocalycis volatile oil.Mixed homogeneously with above-mentioned Herba Menthae vacuum drying thing by this volatile oil, cross 80 mesh sieves, pack, 1kg/ bag, add packed antioxidant and desiccant, Vacuum Package, labeling gets product.
Above embodiment, is only the technological thought that this invention is described, can not limit the every technological thought proposed according to the present invention of protection scope of the present invention whereby, any change that technical scheme basis is done, all falls within the scope of protection of the invention.
Claims (3)
1. a Herba Menthae fresh squeezing vacuum drying powder decoction pieces and preparation technology thereof, it is characterized in that: gather its aerial parts collection period Herba Menthae, clean, after robbing water wash, take advantage of fresh squeezing extracting juice, medicinal residues add the water of 1 ~ 3 times amount, stir 5 ~ 30min, filter press filter pressing, gained medicinal residues squeeze extracting juice again, merge medicine juice and filter with 80 ~ 120 eye mesh screens.
2. a kind of Herba Menthae fresh squeezing vacuum drying powder decoction pieces according to claim 1 and preparation technology thereof, it is characterized in that: by the medicinal liquid of gained in claim 1, in 40 ~ 75 DEG C of concentrating under reduced pressure, gained relative density be 1.05 ~ 1.30 extractum pulverize after 4 ~ 8 hours in 40 ~ 70 DEG C of vacuum dryings.
3. a kind of Herba Menthae fresh squeezing vacuum drying powder decoction pieces according to claim 1 and preparation technology thereof, it is characterized in that: the Herba Menthae condensed water collecting the concentrating under reduced pressure gained in claim 2, add the NaCl of 1% ~ 5% weight, be stirred to dissolve, solution is put in oil water separator, place 12 ~ 48 hours under 4 DEG C ~ 10 DEG C environment, collect top oil reservoir, and toward wherein adding the anhydrous Na of 1% ~ 5% weight
2sO
4, after jolting 5 ~ 10min clock, less than 25 DEG C room temperatures are placed 1 ~ 6 hour, filter, obtain Herba Menthae Haplocalycis volatile oil, and itself and right are wanted the Herba Menthae vacuum drying powder in 2 to mix homogeneously, and cross 40 ~ 100 mesh sieves, vacuum packaging, obtains Herba Menthae fresh squeezing vacuum drying powder decoction pieces.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510774854.XA CN105193920A (en) | 2015-11-14 | 2015-11-14 | Freshly squeezed vacuum drying peppermint powdery decoction pieces and preparation process thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510774854.XA CN105193920A (en) | 2015-11-14 | 2015-11-14 | Freshly squeezed vacuum drying peppermint powdery decoction pieces and preparation process thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105193920A true CN105193920A (en) | 2015-12-30 |
Family
ID=54942110
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510774854.XA Pending CN105193920A (en) | 2015-11-14 | 2015-11-14 | Freshly squeezed vacuum drying peppermint powdery decoction pieces and preparation process thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105193920A (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105520987A (en) * | 2016-02-11 | 2016-04-27 | 徐自升 | Folium artemisiae argyi fresh juice vacuum-dried decoction powder and preparation process thereof |
| CN105596417A (en) * | 2016-02-11 | 2016-05-25 | 徐自升 | Freshly squeezed herba periliae vacuum-dried powder decoction pieces and preparation technology thereof |
| CN106074687A (en) * | 2016-07-31 | 2016-11-09 | 徐漫 | A kind of Rabdosia rubescens is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof |
| CN106109532A (en) * | 2016-07-23 | 2016-11-16 | 徐自升 | A kind of Flos Lonicerae is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof |
| CN107157938A (en) * | 2017-06-19 | 2017-09-15 | 徐漫 | A kind of Flos Magnoliae Liliflorae is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology |
| CN107260797A (en) * | 2017-06-18 | 2017-10-20 | 徐漫 | A kind of wrinkled giant hyssop is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology |
| CN107320527A (en) * | 2017-08-25 | 2017-11-07 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of mulberry leaf |
-
2015
- 2015-11-14 CN CN201510774854.XA patent/CN105193920A/en active Pending
Non-Patent Citations (3)
| Title |
|---|
| 傅超美等: "减压干燥", 《中药药剂学（第1版）》 * |
| 南京药学院药剂学教研组: "汁剂", 《药剂学（第1版）》 * |
| 韩维恒等: "薄荷", 《中药正别名集（第2版）》 * |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105520987A (en) * | 2016-02-11 | 2016-04-27 | 徐自升 | Folium artemisiae argyi fresh juice vacuum-dried decoction powder and preparation process thereof |
| CN105596417A (en) * | 2016-02-11 | 2016-05-25 | 徐自升 | Freshly squeezed herba periliae vacuum-dried powder decoction pieces and preparation technology thereof |
| CN106109532A (en) * | 2016-07-23 | 2016-11-16 | 徐自升 | A kind of Flos Lonicerae is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof |
| CN106074687A (en) * | 2016-07-31 | 2016-11-09 | 徐漫 | A kind of Rabdosia rubescens is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof |
| CN107260797A (en) * | 2017-06-18 | 2017-10-20 | 徐漫 | A kind of wrinkled giant hyssop is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology |
| CN107157938A (en) * | 2017-06-19 | 2017-09-15 | 徐漫 | A kind of Flos Magnoliae Liliflorae is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology |
| CN107320527A (en) * | 2017-08-25 | 2017-11-07 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of mulberry leaf |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105193920A (en) | Freshly squeezed vacuum drying peppermint powdery decoction pieces and preparation process thereof | |
| CN105213474A (en) | A kind of Herba Menthae fresh squeezing spray-dried granules decoction pieces and preparation technology thereof | |
| CN105213475A (en) | A kind of Herba Menthae fresh squeezing lyophilization powder decoction pieces and preparation technology thereof | |
| CN105213473A (en) | A kind of Herba Menthae fresh squeezing spray-dried powders decoction pieces and preparation technology thereof | |
| CN105213450A (en) | A kind of Herba Taraxaci fresh squeezing spray-dried powders decoction pieces and preparation technology thereof | |
| CN105213452A (en) | A kind of Herba Taraxaci fresh squeezing spray-dried granules decoction pieces and preparation technology thereof | |
| CN105213551A (en) | A kind of Herba Hedyotidis Diffusae fresh squeezing spray-dried granules decoction pieces and preparation technology thereof | |
| CN105213444A (en) | A kind of Herba Portulacae fresh squeezing spray-dried powders decoction pieces and preparation technology thereof | |
| CN106109559A (en) | A kind of Flos Sophorae fresh squeezing spray-dried powders decoction pieces and preparation technology thereof | |
| CN106214723A (en) | A kind of Herba Lobeliae Chinensis fresh squeezing spray-dried granules decoction pieces and preparation technology thereof | |
| CN105213453A (en) | A kind of Herba Taraxaci fresh squeezing lyophilization powder decoction pieces and preparation technology thereof | |
| CN105213460A (en) | A kind of Radix et Caulis Opuntiae Dillenii fresh squeezing spray-dried powders decoction pieces and preparation technology thereof | |
| CN105520987A (en) | Folium artemisiae argyi fresh juice vacuum-dried decoction powder and preparation process thereof | |
| CN105596417A (en) | Freshly squeezed herba periliae vacuum-dried powder decoction pieces and preparation technology thereof | |
| CN105560365A (en) | Spray-dried particle decoction piece prepared from freshly-squeezed perilla leaves and preparing technology thereof | |
| CN106074687A (en) | A kind of Rabdosia rubescens is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof | |
| CN106074686A (en) | A kind of Rabdosia rubescens fresh squeezing spray-dried granules decoction pieces and preparation technology thereof | |
| CN105596416A (en) | Freshly squeezed herba periliae freeze-dried powder decoction pieces and preparation technology thereof | |
| CN105520986A (en) | Folium artemisiae argyi fresh juice spray-dried decoction powder and preparation process thereof | |
| CN106038491A (en) | Freshly squeezed and spray-dried granular decoction pieces with verbena officinalis and process for preparing freshly squeezed and spray-dried granular decoction pieces | |
| CN105193894A (en) | Freshly squeezed vacuum drying cholla stem powdery decoction pieces and preparation process thereof | |
| CN105663199A (en) | Freshly-squeezed folium artemisiae argyi spray drying granular medicinal slices and preparation technology thereof | |
| CN106109624A (en) | A kind of Herba Potentillae Discoloris fresh squeezing spray-dried powders decoction pieces and preparation technology thereof | |
| CN106109596A (en) | A kind of Herba Plantaginis is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof | |
| CN106109723A (en) | A kind of Herba Verbenae is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20151230 |
|
| WD01 | Invention patent application deemed withdrawn after publication |