CN106074687A - A kind of Rabdosia rubescens is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof - Google Patents
A kind of Rabdosia rubescens is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof Download PDFInfo
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- CN106074687A CN106074687A CN201610611878.8A CN201610611878A CN106074687A CN 106074687 A CN106074687 A CN 106074687A CN 201610611878 A CN201610611878 A CN 201610611878A CN 106074687 A CN106074687 A CN 106074687A
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- rabdosia rubescens
- vacuum drying
- decoction pieces
- fresh
- preparation technology
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/31—Extraction of the material involving untreated material, e.g. fruit juice or sap obtained from fresh plants
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/53—Liquid-solid separation, e.g. centrifugation, sedimentation or crystallization
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Abstract
The invention discloses that a kind of Rabdosia rubescens is fresh and squeeze vacuum drying powder decoction pieces and preparation technology thereof.This technique, after Rabdosia rubescens medical material is gathered, cleans, drip washing, and takes advantage of fresh squeezing, leaching medicine juice.Medicinal residues add water stirring, filter squeezing.Concentrating under reduced pressure after the merging of gained medicine juice, vacuum drying；Concentrate condensed fluid separation volatile oil, and mix with vacuum drying thing, pack of sieving.Rabdosia rubescens powder decoction pieces prepared by this method, remains the effective ingredient in medical material to greatest extent.Decoction pieces is easy to accumulating, convenient adjustment, and quality controllable, curative effect is reliable, to ensureing that tcm clinical curative effect has great importance.The promotion and implementation of this law, will have significant social meaning and economic benefit.
Description
Technical field
The invention belongs to Chinese crude drug manufacture field, particularly relate to the processing technique of Chinese medicine Rabdosia rubescens decoction pieces.
Background technology
Chinese medicine Rabdosia rubescens is that Labiatae scented tea platymiscium is cracked rice the dry aerial parts of fork.This product has anti-inflammatory analgetic, is good for
Effect that stomach is invigorated blood circulation, can be used for the treatment of laryngopharynx swelling and pain, lump in the abdomen mass in the abdomen and snake bite and insect sting etc..
The processing mode of conventional Rabdosia rubescens decoction pieces is: extract its aerial parts in collection period, chopping, dry in the shade or dry into
Medicine；Or collated, dry after, packing storage and transport.After these Rabdosia rubescens medical materials being dried are transported to prepared slices of Chinese crude drugs factory, need
Want drip washing, section, and redry.Existing technique time and effort consuming, operation repeats, adds the production cost of decoction pieces.In this mistake
Journey not only results in water miscible a large amount of losses therein, and its abundant the most substantial amounts of loss of volatile effective component,
Thus cause the decline of medical material quanlity and the reduction of clinical efficacy.This type of prepared herbal medicine in small pieces ready for decoction, bulky, easily pollute and go mouldy,
Quality it is difficult to ensure that, be unfavorable for formula adjust and guarantee its clinical efficacy.
At present, granule pieces market also having Rabdosia rubescens medical material to make after extracting is sold.Due to granule pieces system
During Bei, extract not only time consumption and energy consumption, and because conventional water does solvent, the nonpolar effective ingredient in medical material is difficult to be extracted
Out.Additionally, due to the Rabdosia rubescens medical material extracted also is to be dried and through long-time storage, therefore, the damage of effective ingredient
It is also the biggest for losing.In order to ensure clinical effective, the steady quality of Rabdosia rubescens medical material, a kind of novel Rabdosia rubescens decoction pieces and system thereof
Standby technique is urgently developed.
Summary of the invention
The invention discloses " a kind of Rabdosia rubescens is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof ".This technique is permissible
Retain the polarity in Rabdosia rubescens medical material and nonpolar effective ingredient to greatest extent, it is to avoid medical material is in the processing of existing decoction pieces and storage
The loss of the effective ingredient caused during fortune and the decline of medical material quanlity, reduce the medical material pollution by mycete etc., to guaranteeing the winter
Steady quality and the clinical safety of LINGCAO decoction pieces effectively have great importance.
To achieve these goals, the technical scheme is that
Gather its aerial parts collection period Rabdosia rubescens, clean, after washing, be cut into the section of 1 ~ 10cm length, take advantage of fresh squeezing extracting juice, medicine
Slag adds the water of 1 ~ 5 times amount, stirs 5 ~ 30min, filter press filter pressing, and gained medicinal residues squeeze extracting juice again, merge medicine juice and use
80 ~ 200 eye mesh screens filter.The medicinal liquid that will filter, in 40 ~ 65 DEG C of concentrating under reduced pressure, obtains the extractum that relative density is 1.05 ~ 1.30
Pulverize after being vacuum dried 4 ~ 8 hours in 40 ~ 60 DEG C.Meanwhile, collect the Rabdosia rubescens condensed water of concentrating under reduced pressure gained, add 1% ~ 5%
The NaCl of weight, is stirred to dissolve.This solution is positioned in oil water separator, under 4 DEG C ~ 10 DEG C environment, stands 12 ~ 48 little
Time.Separate and collect top oil reservoir, be charged with the anhydrous Na of 1% ~ 5% weight2SO4, after shaking 5 ~ 10min clock, less than 25 DEG C
Room temperature is placed 1 ~ 6 hour, filters, obtains Rabdosia rubescens volatile oil.The Rabdosia rubescens volatile oil that this eliminates moisture was insulted with the above-mentioned winter
Grass vacuum drying powder mix homogeneously, crosses 40 ~ 100 mesh sieves, vacuum packaging, obtains Rabdosia rubescens fresh squeezing vacuum drying powder decoction pieces.
On the label of product packaging bags, the name of an article in printing, medicinal part, planting site, manufacturer, the date of manufacture, main
The information such as component content, meridian distribution of property and flavor, function cure mainly, usage and dosage, toxic and side effects and contraindication.The thin of Rabdosia rubescens is enclosed in Dai
Layer differentiates collection of illustrative plates and/or high-efficient liquid phase character collection of illustrative plates, as " identity card " of product.Additionally, in the packaging bag of product, be printed on
Quick Response Code, can link former plant photo, medical material photo, decoction pieces photo, character and the microscopical identification obtaining product by scanning
The information such as feature.
The invention have benefit that:
Fresh Rabdosia rubescens medical material clean washing after directly cutting squeezing, filtration, concentrating under reduced pressure, be vacuum dried, separate oil, mixing,
Obtained powder decoction pieces, can the most completely retain the effective ingredient in medical material.This decoction pieces volume compares to pass
System decoction pieces volume is greatly reduced, and quality is more stable, beneficially accumulating and clinical adjust, have the most significant social meaning and
Economic implications.
Detailed description of the invention
Embodiment 1
By the Rabdosia rubescens medical material of fresh collection, clean, with water wash, be cut into the section of 5cm length, take advantage of the squeezing of using fresh herb squeezer, extracting juice.
Gained medicinal residues add the drinking water of 2 times amount, stir 20min, filter press squeezing extracting juice.Gained medicinal residues squeeze medicine with squeezer again
Juice.Being merged by above-mentioned 3 medicine juice, concentrating under reduced pressure, temperature is set as 65 DEG C.When concentrating gained extractum relative density and being 1.15,
Transfer in vacuum drying oven, be dried 6 hours in 60 DEG C, obtain vacuum drying thing.It addition, the Rabdosia rubescens will collected during concentrating under reduced pressure
Condensed water, adds the NaCl of weight 5%, is stirred to dissolve.This solution is positioned in oil water separator, and in 10 DEG C of environment
Stand 24 hours, separate and collect upper strata volatile oil.The anhydrous Na of 2% weight is added in this volatile oil2SO4, shake 10min clock
After, less than 25 DEG C room temperatures are placed 6 hours, filter, obtain Rabdosia rubescens volatile oil.This volatile oil is vacuum dried thing with above-mentioned Rabdosia rubescens
Mix homogeneously, crosses 60 mesh sieves, pack, 1kg/ bag, adds packed antioxidant and desiccant, Vacuum Package, and labeling gets product.
Embodiment 2
By the Rabdosia rubescens medical material of fresh collection, clean, with water wash, be cut into the section of 10cm length, take advantage of the squeezing of using fresh herb squeezer, take
Juice.Gained medicinal residues add the drinking water of 5 times amount, stir 30min, filter press squeezing extracting juice.Gained medicinal residues squeeze with squeezer again
Take concoction.Being merged by above-mentioned 3 medicine juice, concentrating under reduced pressure, temperature is set as 60 DEG C.It is 1.10 concentrating gained extractum relative density
Time, transfer in vacuum drying oven, be dried 8 hours in 60 DEG C, obtain vacuum drying thing.It addition, the winter will collected during concentrating under reduced pressure
LINGCAO condensed water, adds the NaCl of weight 3%, is stirred to dissolve.This solution is positioned in oil water separator, and 10 DEG C of environment
Middle standing 24 hours, separates and collects upper strata volatile oil.The anhydrous Na of 5% weight is added in this volatile oil2SO4, shake 5min clock
After, less than 25 DEG C room temperatures are placed 12 hours, filter, obtain Rabdosia rubescens volatile oil.This volatile oil is vacuum dried with above-mentioned Rabdosia rubescens
Thing mix homogeneously, crosses 80 mesh sieves, pack, 1kg/ bag, adds packed antioxidant and desiccant, Vacuum Package, and labeling i.e. obtains into
Product.
Above example, is only the technological thought that this invention is described, it is impossible to limit protection scope of the present invention whereby all
It is the technological thought proposed according to the present invention, any change done on the basis of technical scheme, each fall within present invention protection
Within the scope of.
Claims (3)
1. fresh squeezing of Rabdosia rubescens is vacuum dried powder decoction pieces and preparation technology thereof, it is characterised in that: adopt collection period Rabdosia rubescens
Collecting its aerial parts, clean, after washing, be cut into the section of 1 ~ 10cm length, take advantage of fresh squeezing extracting juice, medicinal residues add the water of 1 ~ 5 times amount, stir
Mixing 5 ~ 30min, filter press filter pressing, gained medicinal residues squeeze extracting juice again, merge medicine juice and filter with 80 ~ 200 eye mesh screens.
A kind of Rabdosia rubescens the most according to claim 1 is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof, and its feature exists
In: by the medicinal liquid of gained in claim 1,40 ~ 65 DEG C of concentrating under reduced pressure, gained relative density be the extractum of 1.05 ~ 1.30 in 40 ~
60 DEG C vacuum drying 4 ~ 8 hours after pulverize.
A kind of Rabdosia rubescens the most according to claim 1 is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof, and its feature exists
In: the Rabdosia rubescens condensed water of the concentrating under reduced pressure gained in collection claim 2, add the NaCl of 1% ~ 5% weight, stirring makes molten
Solving, solution is put in oil water separator, places 12 ~ 48 hours under 4 DEG C ~ 10 DEG C environment, collects top oil reservoir, and is charged with
The anhydrous Na of 1% ~ 5% weight2SO4, after shaking 5 ~ 10min clock, less than 25 DEG C room temperatures are placed 1 ~ 6 hour, filter, obtain Rabdosia rubescens and wave
Hair oil, and it wants with right the Rabdosia rubescens vacuum drying powder in 2 mix homogeneously, cross 40 ~ 100 mesh sieves, vacuum packaging, obtain the winter
LINGCAO is fresh squeezes vacuum drying powder decoction pieces.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610611878.8A CN106074687A (en) | 2016-07-31 | 2016-07-31 | A kind of Rabdosia rubescens is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610611878.8A CN106074687A (en) | 2016-07-31 | 2016-07-31 | A kind of Rabdosia rubescens is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof |
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| CN106074687A true CN106074687A (en) | 2016-11-09 |
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| CN201610611878.8A Pending CN106074687A (en) | 2016-07-31 | 2016-07-31 | A kind of Rabdosia rubescens is fresh squeezes vacuum drying powder decoction pieces and preparation technology thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107157938A (en) * | 2017-06-19 | 2017-09-15 | 徐漫 | A kind of Flos Magnoliae Liliflorae is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology |
| CN107260797A (en) * | 2017-06-18 | 2017-10-20 | 徐漫 | A kind of wrinkled giant hyssop is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology |
| CN107362188A (en) * | 2017-08-25 | 2017-11-21 | 徐自升 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of folium isatidis |
| CN107375396A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of fringed pink |
| CN107412301A (en) * | 2017-08-25 | 2017-12-01 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of eclipta |
| CN107485667A (en) * | 2017-08-25 | 2017-12-19 | 徐漫 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of bittersweet |
| CN107485695A (en) * | 2017-08-25 | 2017-12-19 | 徐自升 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of lophatherum gracile |
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| CN105596417A (en) * | 2016-02-11 | 2016-05-25 | 徐自升 | Freshly squeezed herba periliae vacuum-dried powder decoction pieces and preparation technology thereof |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107260797A (en) * | 2017-06-18 | 2017-10-20 | 徐漫 | A kind of wrinkled giant hyssop is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology |
| CN107157938A (en) * | 2017-06-19 | 2017-09-15 | 徐漫 | A kind of Flos Magnoliae Liliflorae is fresh to squeeze vacuum drying powder decoction pieces and its preparation technology |
| CN107362188A (en) * | 2017-08-25 | 2017-11-21 | 徐自升 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of folium isatidis |
| CN107375396A (en) * | 2017-08-25 | 2017-11-24 | 徐自升 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of fringed pink |
| CN107412301A (en) * | 2017-08-25 | 2017-12-01 | 芜湖天成普阳中药科技有限公司 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of eclipta |
| CN107485667A (en) * | 2017-08-25 | 2017-12-19 | 徐漫 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of bittersweet |
| CN107485695A (en) * | 2017-08-25 | 2017-12-19 | 徐自升 | A kind of fresh preparation technology for squeezing vacuum drying powder decoction pieces of lophatherum gracile |
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Application publication date: 20161109 |