CN104609772A - Really stone paint and preparation method thereof - Google Patents
Really stone paint and preparation method thereof Download PDFInfo
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- CN104609772A CN104609772A CN201410826438.5A CN201410826438A CN104609772A CN 104609772 A CN104609772 A CN 104609772A CN 201410826438 A CN201410826438 A CN 201410826438A CN 104609772 A CN104609772 A CN 104609772A
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Abstract
The invention relates to a really stone paint and a preparation method thereof. The really stone paint is prepared from the following components in part by weight: water, hydroxyethyl celluloses, a waterborne multifunctional assistant, polyacrylic emulsion, a thickener, a coalescing agent, an antifreezing agent, a water-based defoamer, a fungicidal preservative and natural colored sand. The really stone paint prepared by the preparation method can realize the effects of good water resistance and good adhesive force under the condition of low temperature and high humidity and under the condition of low temperature and low humidity.
Description
Technical field
The present invention relates to a kind of decoration of exterior wall coating, particularly true mineral varnish of one and preparation method thereof.
Background technology
True mineral varnish is a kind of thick matter type coating, and China introduces this kind of coating about last century Mo from Japan greatly, and starts to be applied in the decorations of buildings.Buildings after true mineral varnish finishing, has the effect as natural sandstone, and decoration sense is vivid, solemnly graceful, can give effect of back to nature, thus be subject to extensively liking of people, more and more indoor and outdoor decoration for all kinds of buildings.But; the true mineral varnish of current majority is in construction application; usually can there is various problems; especially under the condition of low temperature high humidity and low temperature low humidity; often there will be coating not water-fast; meet water grow dim whiting, fade, the phenomenons such as poor adhesive force, have had a strong impact on quality and the decorative effect of true mineral varnish.
Summary of the invention
The object of the invention is to overcome weak point of the prior art, there is provided a kind of true mineral varnish and preparation method thereof, true mineral varnish prepared by the present invention can realize under the condition of low temperature high humidity and low temperature low humidity water-tolerant, effect that sticking power is good.
The present invention is achieved in that a kind of true mineral varnish, by following component and ratio of weight and number formulated:
Further prioritization scheme: described Natvosol is non-ionic water-soluble ether of cellulose, it adopts the EBS481FQ Natvosol of Akzo Nobel.
Further prioritization scheme: water-soluble multifunctional auxiliary agent adopts AMP-95 multifunctional assistant, it is mainly used for regulating potential of hydrogen.Described film coalescence aid is two kinds of any mixture in alcohol ester 12, ethylene glycol monobutyl ether, butyl and phenylcarbinol.
Further prioritization scheme: described frostproofer is that one or more in ethylene glycol, propylene glycol and glycerol mix arbitrarily.
Further prioritization scheme: described water-based defoamer is any one in non-ionic type defoamer, molecular antifoaming agent or mineral oil antifoam agent or silicone antifoam agent; It adopts the sub-F5800C defoamer in sieve ground.Fungicidal preservative adopts the fungicidal preservative of Thor Acticide HF
Further prioritization scheme: described natural colour sand is 40-80 object natural colour sand and the 80-120 object natural colour sand mixture by rational ratio combination.The value range of rational proportion is that 80-120 object natural colour sand and 40-80 object natural colour sand mix in the ratio of 1:0.3-1.0.
Further prioritization scheme: described thickening material is the non-ionic type associative thickener of polyurethanes, hydrophobic grouping modification, and it adopts ROHM AND HAAS RM8W thickening material; It and described Natvosol have extraordinary synergy, have excellent water tolerance.
The preparation method of above-mentioned true mineral varnish, it comprises the step of sequentially carrying out as follows:
(a), the water of 9.35-17.65 part is added in dispersion cylinder, under 300-500rpm whipped state, add 0.2-0.4 part enter Natvosol, stir 5-10min;
(b), under the rotating speed of 300-500rpm, add 0.05-0.15 part water-soluble multifunctional auxiliary agent, then rotating speed is improved to 700-1000rpm, and 10-15min is stirred under this rotating speed, until Natvosol dissolves completely and stirs, regulate pH to 8.0-10.0;
C (), stopping add 11-15 part pure-acrylic emulsion after stirring, control rotating speed and stir 5-10min under 600-900rpm whipped state;
(d), stir after, continue under 600-900rpm whipped state, slowly add 0.1-0.3 part thickening material, 0.8-1.0 part film coalescence aid, 0.2-0.4 part frostproofer, 0.1-0.5 part water-based defoamer and 0.2-0.6 part fungicidal preservative successively, finish, after fully stirring 5-10min, obtain true mineral varnish base paste;
(e), finally the above-mentioned true mineral varnish base paste prepared is mixed with 68-74 part natural colour sand, mix rear blowing, barrelling.
True mineral varnish tool prepared by the present invention has the following advantages: the true mineral varnish adopting component of the present invention and proportioning to combine preparation overcomes under the condition of low temperature high humidity and low temperature low humidity, meet the water capacity during construction easily to whiten and grow dim, the problem of poor adhesive force, described true mineral varnish has excellent water tolerance, time of drying is controlled, has good sticking power and weathering resistance simultaneously, constructs smooth and easy, construction effect environmental protection attractive in appearance, and contamination resistance is remarkable.
The true mineral varnish of the present invention compared with prior art tool has the following advantages: adopt the non-ionic type associative thickener of hydrophobic grouping modification and non-ionic water-soluble ether of cellulose to act synergistically thickening, replace alkali swollen thickener, improve thickening efficiency, also greatly strengthen the water tolerance of true mineral varnish, contamination resistance and sticking power etc.; Adopt two kinds of true mineral varnish film formation times of the composite control of film coalescence aid again simultaneously, achieve the controlled of true mineral varnish time of drying, last and 40-80 object natural colour sand and 80-120 object natural colour sand are arranged in pairs or groups with rational proportioning, improve the water tolerance of true mineral varnish, contamination resistance and sticking power further, overcome low temperature high humidity and the construction of low temperature low humidity is easily grown dim whiting, the problem of poor adhesive force, optimizes the over-all properties of true mineral varnish greatly.
Embodiment
Below in conjunction with specific embodiment, the present invention will be described in detail.
(1) embodiment is as follows:
A kind of true mineral varnish, by following component and ratio of weight and number formulated:
A preparation method for true mineral varnish, it comprises the step of sequentially carrying out as follows:
(a), the water of 9.35-17.65 part is added in dispersion cylinder, under 300-500rpm whipped state, add 0.2-0.4 part enter Natvosol, stir 5-10min;
(b), under the rotating speed of 300-500rpm, add 0.05-0.15 part water-soluble multifunctional auxiliary agent, then rotating speed is improved to 700-1000rpm, and 10-15min is stirred under this rotating speed, until Natvosol dissolves completely and stirs, regulate pH to 8.0-10.0;
C (), stopping add 11-15 part pure-acrylic emulsion after stirring, control rotating speed and stir 5-10min under 600-900rpm whipped state;
(d), stir after, continue under 600-900rpm whipped state, slowly add 0.1-0.3 part thickening material, 0.8-1.0 part film coalescence aid, 0.2-0.4 part frostproofer, 0.1-0.5 part water-based defoamer and 0.2-0.6 part fungicidal preservative successively, finish, after fully stirring 5-10min, obtain true mineral varnish base paste;
(e), finally the above-mentioned true mineral varnish base paste prepared is mixed with 68-74 part natural colour sand, mix rear blowing, barrelling.
Natvosol described in said components adopts the EBS481FQ Natvosol of Akzo Nobel.Water-soluble multifunctional auxiliary agent adopts AMP-95 multifunctional assistant.Described water-based defoamer adopts the sub-F5800C defoamer in sieve ground.Fungicidal preservative adopts the fungicidal preservative of Thor Acticide HF.Described thickening material adopts ROHM AND HAAS RM8W thickening material.Natural colour sand is that 80-120 object natural colour sand and 40-80 object natural colour sand mix in the ratio of 1:0.3-1.0.Described often kind of component also can adopt other type product similar.
(2) embodiment is as follows:
Embodiment 1: a kind of true mineral varnish, by following component and ratio of weight and number formulated:
A preparation method for true mineral varnish, it comprises the step of sequentially carrying out as follows:
(a), the water of 17.65 parts is added in dispersion cylinder, under 500rpm whipped state, add 0.4 part enter Natvosol, stir 5min;
(b), under the rotating speed of 500rpm, add 0.15 part of water-soluble multifunctional auxiliary agent, then improve rotating speed to 1000rpm, and stir 10min under this rotating speed, until Natvosol dissolves completely and stirs, regulate pH to 8.0-10.0;
C (), stopping add 11 parts of pure-acrylic emulsions after stirring, control rotating speed and stir 5min under 900rpm whipped state;
(d), stir after, continue under 900rpm whipped state, slowly add 0.3 part of thickening material, 1.0 parts of film coalescence aid, 0.4 part of frostproofer, 0.5 part of water-based defoamer and 0.6 part of fungicidal preservative successively, finish, after fully stirring 5min, obtain true mineral varnish base paste;
(e), finally the above-mentioned true mineral varnish base paste prepared is mixed with 68 parts of natural colour sands, mix rear blowing, barrelling.
Natvosol described in said components adopts the EBS481FQ Natvosol of Akzo Nobel.Water-soluble multifunctional auxiliary agent adopts AMP-95 multifunctional assistant.Described water-based defoamer adopts the sub-F5800C defoamer in sieve ground.Fungicidal preservative adopts the fungicidal preservative of Thor Acticide HF.Described thickening material adopts ROHM AND HAAS RM8W thickening material.Natural colour sand is that 80-120 object natural colour sand and 40-80 object natural colour sand mix in the ratio of 1:1.
Embodiment 2: a kind of true mineral varnish, by following component and ratio of weight and number formulated:
A preparation method for true mineral varnish, it comprises the step of sequentially carrying out as follows:
(a), the water of 9.35 parts is added in dispersion cylinder, under 300rpm whipped state, add 0.2 part enter Natvosol, stir 10min;
(b), under the rotating speed of 300rpm, add 0.05 part of water-soluble multifunctional auxiliary agent, then improve rotating speed to 700rpm, and stir 15min under this rotating speed, until Natvosol dissolves completely and stirs, regulate pH to 8.0-10.0;
C (), stopping add 15 parts of pure-acrylic emulsions after stirring, control rotating speed and stir 10min under 600rpm whipped state;
(d), stir after, continue under 600rpm whipped state, slowly add 0.1 part of thickening material, 0.8 part of film coalescence aid, 0.2 part of frostproofer, 0.1 part of water-based defoamer and 0.2 part of fungicidal preservative successively, finish, after fully stirring 10min, obtain true mineral varnish base paste;
(e), finally the above-mentioned true mineral varnish base paste prepared is mixed with 74 parts of natural colour sands, mix rear blowing, barrelling.
Natvosol described in said components adopts the EBS481FQ Natvosol of Akzo Nobel.Water-soluble multifunctional auxiliary agent adopts AMP-95 multifunctional assistant.Described water-based defoamer adopts the sub-F5800C defoamer in sieve ground.Fungicidal preservative adopts the fungicidal preservative of Thor Acticide HF.Described thickening material adopts ROHM AND HAAS RM8W thickening material.Natural colour sand is that 80-120 object natural colour sand and 40-80 object natural colour sand mix in the ratio of 1:0.3.
Embodiment 3: a kind of true mineral varnish, by following component and ratio of weight and number formulated:
A preparation method for true mineral varnish, it comprises the step of sequentially carrying out as follows:
(a), the water of 13.5 parts is added in dispersion cylinder, under 400rpm whipped state, add 0.3 part enter Natvosol, stir 8min;
(b), under the rotating speed of 400rpm, add 0.1 part of water-soluble multifunctional auxiliary agent, then improve rotating speed to 800rpm, and stir 12min under this rotating speed, until Natvosol dissolves completely and stirs, regulate pH to 8.0-10.0;
C (), stopping add 13 parts of pure-acrylic emulsions after stirring, control rotating speed and stir 8min under 800rpm whipped state;
(d), stir after, continue under 800rpm whipped state, slowly add 0.2 part of thickening material, 0.9 part of film coalescence aid, 0.3 part of frostproofer, 0.3 part of water-based defoamer and 0.4 part of fungicidal preservative successively, finish, after fully stirring 8min, obtain true mineral varnish base paste;
(e), finally the above-mentioned true mineral varnish base paste prepared is mixed with 71 parts of natural colour sands, mix rear blowing, barrelling.
Natvosol described in said components adopts the EBS481FQ Natvosol of Akzo Nobel.Water-soluble multifunctional auxiliary agent adopts AMP-95 multifunctional assistant.Described water-based defoamer adopts the sub-F5800C defoamer in sieve ground.Fungicidal preservative adopts the fungicidal preservative of Thor Acticide HF.Described thickening material adopts ROHM AND HAAS RM8W thickening material.Natural colour sand is that 80-120 object natural colour sand and 40-80 object natural colour sand mix in the ratio of 1:0.5.
Embodiment 4: a kind of true mineral varnish, by following component and ratio of weight and number formulated:
A preparation method for true mineral varnish, it comprises the step of sequentially carrying out as follows:
(a), the water of 15 parts is added in dispersion cylinder, under 350rpm whipped state, add 0.2 part enter Natvosol, stir 10min;
(b), under the rotating speed of 350rpm, add 0.1 part of water-soluble multifunctional auxiliary agent, then improve rotating speed to 900rpm, and stir 10min under this rotating speed, until Natvosol dissolves completely and stirs, regulate pH to 8.0-10.0;
C (), stopping add 12 parts of pure-acrylic emulsions after stirring, control rotating speed and stir 5min under 700rpm whipped state;
(d), stir after, continue under 700rpm whipped state, slowly add 0.1 part of thickening material, 1.0 parts of film coalescence aid, 0.4 part of frostproofer, 0.2 part of water-based defoamer and 0.5 part of fungicidal preservative successively, finish, after fully stirring 5min, obtain true mineral varnish base paste;
(e), finally the above-mentioned true mineral varnish base paste prepared is mixed with 70.5 parts of natural colour sands, mix rear blowing, barrelling.
Natvosol described in said components adopts the EBS481FQ Natvosol of Akzo Nobel.Water-soluble multifunctional auxiliary agent adopts AMP-95 multifunctional assistant.Described water-based defoamer adopts the sub-F5800C defoamer in sieve ground.Fungicidal preservative adopts the fungicidal preservative of Thor Acticide HF.Described thickening material adopts ROHM AND HAAS RM8W thickening material.Natural colour sand is that 80-120 object natural colour sand and 40-80 object natural colour sand mix in the ratio of 1:0.8.
Through the test to each embodiment, every technical performance index of the true mineral varnish of the present invention and experimental data are as follows respectively shown in table:
| Test event | Embodiment 1-4 | Existing true mineral varnish |
| State | Evenly, without caking, conglomeration | State is general |
| Initial stage water tolerance | Paint film is without whiting with without deliquescing | Paint film seriously whitens and deliquescing |
| Water tolerance | Paint film is without whiting and grow dim | Paint film whitens, and cannot recover |
| Initial dry cracking resistance | Without cracking phenomena | Cracking |
| Time of drying | Controlled, can surface drying fast | Cannot surface drying fast, need about 60min |
| Application property | Spraying is without difficulty | Spraying can a little stifled rifle |
| Drop rate | Drop rate is low | Drop is serious |
| Sticking power | Dry wet adhesion is good | Dry wet adhesion is general |
| Outward appearance | Nature attractive in appearance, without skinning, caking | Outward appearance is general |
| Opacifying power | Opacifying power is good | Opacifying power is good |
| Weathering resistance | Open air be exposed to the sun after no color differnece, fade | There is aberration open air, fades after being exposed to the sun |
| Contamination resistance | 0 grade, contamination resistance is excellent | Contamination resistance is general |
Test result from the above embodiments: true mineral varnish prepared by the present invention has excellent water tolerance, and time of drying is controlled, has good sticking power and weathering resistance simultaneously, constructs smooth and easy, construction effect environmental protection attractive in appearance, and contamination resistance is remarkable.
Above-mentioned embodiment is just explained in detail technical scheme of the present invention, and the present invention has more than and is only confined to above-described embodiment, and every any improvement according to the principle of the invention or replacement, all should within protection scope of the present invention.
Claims (8)
1. a true mineral varnish, is characterized in that, by following component and ratio of weight and number formulated:
2. true mineral varnish according to claim 1, is characterized in that: described Natvosol is non-ionic water-soluble ether of cellulose.
3. true mineral varnish according to claim 1, is characterized in that: described film coalescence aid is two kinds of any mixture in alcohol ester 12, ethylene glycol monobutyl ether, butyl and phenylcarbinol.
4. true mineral varnish according to claim 1, is characterized in that: described frostproofer is that one or more in ethylene glycol, propylene glycol and glycerol mix arbitrarily.
5. true mineral varnish according to claim 1, is characterized in that: described water-based defoamer is any one in non-ionic type defoamer, molecular antifoaming agent or mineral oil antifoam agent or silicone antifoam agent.
6. true mineral varnish according to claim 1, is characterized in that: described natural colour sand is that 80-120 object natural colour sand and 40-80 object natural colour sand mix in the ratio of 1:0.3-1.0.
7. true mineral varnish according to claim 1, is characterized in that: described thickening material is the non-ionic type associative thickener of polyurethanes, hydrophobic grouping modification.
8. a preparation method for the true mineral varnish according to any one of claim 1-7, is characterized in that: it comprises the step of sequentially carrying out as follows:
(a), the water of 9.35-17.65 part is added in dispersion cylinder, under 300-500rpm whipped state, add 0.2-0.4 part enter Natvosol, stir 5-10min;
(b), under the rotating speed of 300-500rpm, add 0.05-0.15 part water-soluble multifunctional auxiliary agent, then rotating speed is improved to 700-1000rpm, and 10-15min is stirred under this rotating speed, until Natvosol dissolves completely and stirs, regulate pH to 8.0-10.0;
C (), stopping add 11-15 part pure-acrylic emulsion after stirring, control rotating speed and stir 5-10min under 600-900rpm whipped state;
(d), stir after, continue under 600-900rpm whipped state, slowly add 0.1-0.3 part thickening material, 0.8-1.0 part film coalescence aid, 0.2-0.4 part frostproofer, 0.1-0.5 part water-based defoamer and 0.2-0.6 part fungicidal preservative successively, finish, after fully stirring 5-10min, obtain true mineral varnish base paste;
(e), finally the above-mentioned true mineral varnish base paste prepared is mixed with 68-74 part natural colour sand, mix rear blowing, barrelling.
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| CN201410826438.5A CN104609772A (en) | 2014-12-26 | 2014-12-26 | Really stone paint and preparation method thereof |
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| CN105056799A (en) * | 2015-07-28 | 2015-11-18 | 浙江三普节能建筑涂料有限公司 | Stirring apparatus for true stone paint and marbling true stone paint produced by using same |
| CN105131769A (en) * | 2015-09-10 | 2015-12-09 | 三棵树涂料股份有限公司 | Special dull finish paint for sand textured external wall coating and preparation method of special dull finish paint |
| CN105236825A (en) * | 2015-09-10 | 2016-01-13 | 三棵树涂料股份有限公司 | External wall particle type texture coating material and preparation method thereof |
| CN105254213A (en) * | 2015-09-16 | 2016-01-20 | 三棵树涂料股份有限公司 | Slow-drying brick-imitating real stone paint and preparation method thereof |
| CN105295606A (en) * | 2015-11-25 | 2016-02-03 | 亚士漆(上海)有限公司 | Lacquer for construction in low temperature and high humidity condition and preparation method thereof |
| CN106938898A (en) * | 2017-02-28 | 2017-07-11 | 河北晨阳工贸集团有限公司 | A kind of true mineral varnish suitable for airless spraying |
| CN107140874A (en) * | 2017-05-12 | 2017-09-08 | 合肥科天水性科技有限责任公司 | A kind of aqueous machine sprays true mineral varnish and preparation method thereof |
| CN107200506A (en) * | 2017-06-01 | 2017-09-26 | 信阳天意节能技术股份有限公司 | A kind of true mineral varnish and preparation method thereof |
| CN107601972A (en) * | 2017-07-31 | 2018-01-19 | 常州杰轩纺织科技有限公司 | A kind of true mineral varnish |
| CN108059389A (en) * | 2017-12-11 | 2018-05-22 | 新华盛节能科技股份有限公司 | Nano modification lacquer |
| CN108084750A (en) * | 2017-12-29 | 2018-05-29 | 平阳瑞丰新材料科技有限公司 | A kind of lacquer and its application |
| CN108409198A (en) * | 2018-03-27 | 2018-08-17 | 炫杰复合材料（上海）有限公司 | A kind of hydrophobic lacquer and preparation method thereof |
| CN110078412A (en) * | 2019-03-29 | 2019-08-02 | 河北晨阳工贸集团有限公司 | A kind of water-base resin sand lacquer and preparation method thereof |
| CN111234686A (en) * | 2020-03-10 | 2020-06-05 | 浙江华德新材料有限公司 | Self-crosslinking acrylic polyurethane dispersion stone-like paint and preparation method thereof |
| CN113150632A (en) * | 2021-03-25 | 2021-07-23 | 天津德普威涂料有限公司 | Finishing paint base material, crystal color stone finishing paint prepared from same and capable of reducing rainwater soaking whitening, and preparation methods of base material and finishing paint |
| CN113248994A (en) * | 2021-06-21 | 2021-08-13 | 锦益得节能环保科技(山东)有限公司 | Real stone paint and preparation method thereof |
| CN113604081A (en) * | 2021-09-01 | 2021-11-05 | 福建省三棵树新材料有限公司 | Low-temperature film-forming real stone paint and preparation process thereof |
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| CN105056799A (en) * | 2015-07-28 | 2015-11-18 | 浙江三普节能建筑涂料有限公司 | Stirring apparatus for true stone paint and marbling true stone paint produced by using same |
| CN105056799B (en) * | 2015-07-28 | 2017-09-01 | 浙江三普节能建筑涂料有限公司 | True mineral varnish mixing plant and the true mineral varnish of marbling produced with the equipment |
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| CN105236825A (en) * | 2015-09-10 | 2016-01-13 | 三棵树涂料股份有限公司 | External wall particle type texture coating material and preparation method thereof |
| CN105254213A (en) * | 2015-09-16 | 2016-01-20 | 三棵树涂料股份有限公司 | Slow-drying brick-imitating real stone paint and preparation method thereof |
| CN105295606A (en) * | 2015-11-25 | 2016-02-03 | 亚士漆(上海)有限公司 | Lacquer for construction in low temperature and high humidity condition and preparation method thereof |
| CN106938898A (en) * | 2017-02-28 | 2017-07-11 | 河北晨阳工贸集团有限公司 | A kind of true mineral varnish suitable for airless spraying |
| CN107140874B (en) * | 2017-05-12 | 2020-09-04 | 合肥科天水性科技有限责任公司 | Water-based machine-sprayed real stone paint and preparation method thereof |
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| CN107200506A (en) * | 2017-06-01 | 2017-09-26 | 信阳天意节能技术股份有限公司 | A kind of true mineral varnish and preparation method thereof |
| CN107601972A (en) * | 2017-07-31 | 2018-01-19 | 常州杰轩纺织科技有限公司 | A kind of true mineral varnish |
| CN108059389A (en) * | 2017-12-11 | 2018-05-22 | 新华盛节能科技股份有限公司 | Nano modification lacquer |
| CN108084750A (en) * | 2017-12-29 | 2018-05-29 | 平阳瑞丰新材料科技有限公司 | A kind of lacquer and its application |
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Application publication date: 20150513 |