CN104946033A - Sand texture paint and production method thereof - Google Patents
Sand texture paint and production method thereof Download PDFInfo
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- CN104946033A CN104946033A CN201510442263.2A CN201510442263A CN104946033A CN 104946033 A CN104946033 A CN 104946033A CN 201510442263 A CN201510442263 A CN 201510442263A CN 104946033 A CN104946033 A CN 104946033A
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Abstract
The invention discloses a sand texture paint and a production method thereof. The sand texture paint is prepared from the following components in parts by weight: 2-6 parts of a dispersing agent, 0.5-1.5 parts of a wetting agent, 0.3-1 part of an antifoaming agent, 0.3-1 part of a multifunctional additive, 6-12 parts of a film-forming additive, 12-20 parts of ethylene glycol, 1-3 parts of a rheological additive, 2-4 parts of cellulose, 20-50 parts of kaolin, 30-80 parts of titanium dioxide, 100-200 parts of an emulsion, 1-2 parts of a preservative, 1.5-4 parts of a thickening agent, 500-750 parts of texture sand, 0.3-1 part of color paste and 90-180 parts of deionized water. The sand texture paint provided by the invention is unlikely to discolor, and good in stain resistance; in addition, through choose of the components and the ratio of the components, the sand texture paint is high in viscosity, free of sand falling during construction, high in water retention, stability, constructability and weatherability, and excellent in adhesion.
Description
Technical field
The present invention relates to a kind of sand wall-like texture paint and production method thereof, belong to chemical field.
Background technology
Sand wall-like texture coating generally claims true mineral varnish or stone similar paint.Buildings through lithotome decoration is magnificent, and noble, quality is higher.But because lithotome is expensive, construction inconvenience, so develop a kind of building coating-true mineral varnish coating of artificial stone in the market, this coating direct spraying, its decorative effect has texture and the color of lithotome.Use the buildings that true mineral varnish is decorated, not only there is luxurious appearance and the flintiness of stone material, and there is elegance, noble quality, the artistic effects such as stereoscopic sensation is strong. true mineral varnish has excellent weathering resistance, colour-fast and contamination resistance, more than 10 years work-ing life was a kind of material of alternative lithotome facing.But the sandy paint that existing market uses, tackiness agent mainly pure third, phenylpropyl alcohol or vinyl acetate copolymerized and so on fluoropolymer resin or emulsion, although these coating reach certain effect in actual use, but in acid resistance, water resisting property, stain resistant, fast light weathering resistance aspect also fall flat, mainly have impact on the stable of glued membrane containing multiple water soluble emulsifier in polymkeric substance, the non-inorganic adhesive of the filler simultaneously used normally quartz sand or calcium carbonate etc. and so on, these fillers with the consistency of polymkeric substance in existing defects, cause the acid resistance of coating, water resisting property, stain resistant, the effect of fast light weathering resistance aspect is restricted.And existing sand wall-like texture paint fugitive color, contamination resistance are poor.Therefore to employ new technology and novel material to be inevitable trend to the defect making up prior art.
Summary of the invention
The technical problem to be solved in the present invention overcomes existing defect, provides a kind of sand wall-like texture paint and production method thereof.
In order to solve the problems of the technologies described above, the invention provides following technical scheme:
A kind of sand wall-like texture paint, each component following by weight part is prepared from: dispersion agent 2 ~ 6 parts, wetting agent 0.5 ~ 1.5 part, defoamer 0.3 ~ 1 part, multifunctional assistant 0.3 ~ 1 part, film coalescence aid 6 ~ 12 parts, ethylene glycol 12 ~ 20 parts, auxiliary rheological agents 1 ~ 3 part, Mierocrystalline cellulose 2 ~ 4 parts, kaolin 20 ~ 50 parts, titanium dioxide 30 ~ 80 parts, emulsion 100 ~ 200 parts, sanitas 1 ~ 2 part, thickening material 1.5 ~ 4 parts, 500 ~ 750 parts, texture sand, mill base 0.3 ~ 1 part, deionized water 90 ~ 180 parts.
, each component following by weight part is prepared from such scheme preferably: dispersion agent 3 parts, wetting agent 0.8 part, defoamer 0.5 part, multifunctional assistant 0.5 part, film coalescence aid 8 parts, ethylene glycol 15 parts, auxiliary rheological agents 2 parts, Mierocrystalline cellulose 2.5 parts, kaolin 30 parts, titanium dioxide 50 parts, emulsion 160 parts, sanitas 1.5 parts, thickening material 2 parts, 600 parts, texture sand, mill base 0.5 part, deionized water 130 parts.
Described ethylene glycol plays antifreeze, furtherance membrane interaction; Kaolin, water-ground limestone, titanium dioxide are stopping composition and extender pigment.
In above-mentioned either a program preferably, described dispersion agent is selected from one or more in tripoly phosphate sodium STPP, Sodium hexametaphosphate 99, trisodium phosphate, triethyl hexyl phosphoric acid, sodium lauryl sulphate, methyl amyl alcohol;
Described wetting agent is selected from one or more in sulphonated oil, sulfuric acid based hydrazides class and mercaptan acetals;
Described defoamer is selected from one or more in mineral oil, organosilicon, modified paraffin defoamer;
Described multifunctional assistant is selected from one or more in amine, hydramine and organic amine;
Described film coalescence aid is selected from one or more in propandiol butyl ether, propylene glycol monomethyl ether amyl acetate, Lauryl Alcohol fat, propylene glycol phenylate;
Described auxiliary rheological agents is selected from one or more in organic clay, wilkinite, Mierocrystalline cellulose, xanthan gum, polyacrylate, Polyurethane;
Described Mierocrystalline cellulose be selected from methylcellulose gum, ethyl cellulose, hydroxy ethyl fiber one or more;
Described emulsion is selected from one or more in benzene emulsion, pure-acrylic emulsion, organosilicon crylic acid latex, elastic emulsion;
Described sanitas is selected from isothiazolinone derivatives (as: Nordes C15 etc.), benzimidazole ester class (as: Nordes C15 etc.), Dao Weixier-75,1, one or more in 2-benzisothiazole-3-ketone;
Described thickening material is selected from one or more in thick dose of inorganic thickening agent, polyacrylate and association type Polyurethane.
Described mill base is selected from organic mill base and/or inorganic mill base.
Described titanium dioxide selects unsolicited titanium dioxide, as Rutile type Titanium Dioxide etc.
In above-mentioned either a program preferably, described texture sand is circular quartz sand.
The present invention also provides the production method of described sand wall-like texture paint, comprises following steps:
(1) deionized water is injected at dispersion tank;
(2) start dispersion machine, add dispersion agent, wetting agent, defoamer, multifunctional assistant, film coalescence aid, ethylene glycol and auxiliary rheological agents successively, dispersed with stirring 10 ~ 20 minutes, rotating speed 400 ~ 600 revs/min;
(3) add Mierocrystalline cellulose, kaolin and titanium dioxide, rotating speed brings up to 1000 ~ 1500 revs/min, high speed dispersion 10 ~ 30 minutes;
(4) be decelerated to 500 ~ 700 revs/min, add emulsion, sanitas and thickening material successively, dispersion stirring 10 ~ 20 minutes;
(5) add texture sand, stirring at low speed mixes;
(6) add mill base furnishing required color and namely obtain described sand wall-like texture paint.
In above-mentioned either a program preferably, step (2) dispersed with stirring 15 minutes, rotating speed 500 revs/min.
In above-mentioned either a program preferably, step (3) rotating speed brings up to 1200 revs/min, high speed dispersion 20 minutes.
In above-mentioned either a program preferably, step (4) is decelerated to 600 revs/min, adds emulsion, sanitas and thickening material successively, dispersion stirring 15 minutes.
Beneficial effect of the present invention: sand wall-like texture paint of the present invention not fugitive color, contamination resistance is good; In addition due to the selection of instant component and proportioning, make that described sand wall-like texture paint viscosity is high, construction time can not drop, good water-retaining property, good stability, have good workability, good weatherability, has excellent sticking power.
Embodiment
Below the preferred embodiments of the present invention are described, should be appreciated that preferred embodiment described herein is only for instruction and explanation of the present invention, is not intended to limit the present invention.
The raw material used in the present invention is commercially available buying.As elastic emulsion selects the rich company of Guangdong Ahmedabad, selection of auxiliary Aksu. Nobel company, titanium dioxide selects Sichuan Long Mangtai industry company.
Embodiment 1:
A kind of sand wall-like texture paint, each component following by weight part is prepared from: dispersion agent 3 parts, wetting agent 0.8 part, defoamer 0.5 part, multifunctional assistant 0.5 part, film coalescence aid 8 parts, ethylene glycol 15 parts, auxiliary rheological agents 2 parts, Mierocrystalline cellulose 2.5 parts, kaolin 30 parts, titanium dioxide 50 parts, emulsion 160 parts, sanitas 1.5 parts, thickening material 2 parts, 600 parts, texture sand, mill base 0.5 part, deionized water 130 parts.
Described dispersion agent is tripoly phosphate sodium STPP; Described wetting agent is sulphonated oil; Described defoamer is mineral oil; Described multifunctional assistant is Monomethylamine; Described film coalescence aid is propandiol butyl ether; Described auxiliary rheological agents is wilkinite; Described Mierocrystalline cellulose is methylcellulose gum; Described emulsion is benzene emulsion; Described sanitas is Dao Weixier-75; Described thickening material is polyacrylate; Described mill base is organic mill base: iron oxide black, iron oxide yellow, iron oxide red; Described texture sand is circular quartz sand.
The production method of the sand wall-like texture paint described in the present embodiment, comprises following steps:
(1) deionized water is injected at dispersion tank;
(2) start dispersion machine, add dispersion agent, wetting agent, defoamer, multifunctional assistant, film coalescence aid, ethylene glycol and auxiliary rheological agents successively, dispersed with stirring 15 minutes, rotating speed 500 revs/min;
(3) add Mierocrystalline cellulose, kaolin and titanium dioxide, rotating speed brings up to 1200 revs/min, high speed dispersion 20 minutes;
(4) be decelerated to 600 revs/min, add emulsion, sanitas and thickening material successively, dispersion stirring 15 minutes;
(5) add texture sand, stirring at low speed mixes;
(6) add mill base furnishing required color and namely obtain described sand wall-like texture paint.
Embodiment 2:
A kind of sand wall-like texture paint, each component following by weight part is prepared from: dispersion agent 2 parts, wetting agent 0.5 part, defoamer 0.3 part, multifunctional assistant 0.3 part, film coalescence aid 6 parts, ethylene glycol 12 parts, auxiliary rheological agents 1 part, Mierocrystalline cellulose 2 parts, kaolin 20 parts, titanium dioxide 30 parts, emulsion 100 parts, sanitas 1 part, thickening material 1.5 parts, 500 parts, texture sand, mill base 0.3 part, deionized water 90 parts.
Described dispersion agent is tripoly phosphate sodium STPP; Described wetting agent is sulphonated oil; Described defoamer is mineral oil; Described multifunctional assistant is Monomethylamine; Described film coalescence aid is propandiol butyl ether; Described auxiliary rheological agents is wilkinite; Described Mierocrystalline cellulose is methylcellulose gum; Described emulsion is benzene emulsion; Described sanitas is Dao Weixier-75; Described thickening material is polyacrylate; Described mill base is organic mill base; Described texture sand is circular quartz sand.
The production method of the sand wall-like texture paint described in the present embodiment, with embodiment 1.
Embodiment 3:
A kind of sand wall-like texture paint, each component following by weight part is prepared from: dispersion agent 6 parts, wetting agent 1.5 parts, defoamer 1 part, multifunctional assistant 1 part, film coalescence aid 12 parts, ethylene glycol 20 parts, auxiliary rheological agents 3 parts, Mierocrystalline cellulose 4 parts, kaolin 50 parts, titanium dioxide 80 parts, emulsion 200 parts, sanitas 2 parts, thickening material 4 parts, 750 parts, texture sand, mill base 1 part, deionized water 180 parts.
Described dispersion agent is tripoly phosphate sodium STPP; Described wetting agent is sulphonated oil; Described defoamer is mineral oil; Described multifunctional assistant is Monomethylamine; Described film coalescence aid is propandiol butyl ether; Described auxiliary rheological agents is wilkinite; Described Mierocrystalline cellulose is methylcellulose gum; Described emulsion is benzene emulsion; Described sanitas is Dao Weixier-75; Described thickening material is polyacrylate; Described mill base is organic mill base; Described texture sand is circular quartz sand.
The production method of the sand wall-like texture paint described in the present embodiment, with embodiment 1.
The described multifunctional assistant of embodiment 1-3 can select arbitrary aminated compounds, and described mill base can select arbitrary organic mill base, all can prepare described sand wall-like texture paint.
Embodiment 4:
A kind of sand wall-like texture paint, each component following by weight part is prepared from: dispersion agent 6 parts, wetting agent 1.5 parts, defoamer 1 part, multifunctional assistant 1 part, film coalescence aid 12 parts, ethylene glycol 20 parts, auxiliary rheological agents 3 parts, Mierocrystalline cellulose 4 parts, kaolin 50 parts, titanium dioxide 80 parts, emulsion 200 parts, sanitas 2 parts, thickening material 4 parts, 750 parts, texture sand, mill base 1 part, deionized water 180 parts.
Described dispersion agent is Sodium hexametaphosphate 99; Described wetting agent is mercaptan acetals; Described defoamer is organosilicon; Described multifunctional assistant is diethanolamine; Described film coalescence aid is propylene glycol monomethyl ether amyl acetate; Described auxiliary rheological agents is xanthan gum; Described Mierocrystalline cellulose is ethyl cellulose; Described emulsion is organosilicon crylic acid latex; Described sanitas is 1,2-benzisothiazole-3-ketone; Described thickening material is inorganic thickening agent; Described mill base is selected from organic mill base; Described texture sand is circular quartz sand.
The production method of the sand wall-like texture paint described in the present embodiment, comprises following steps:
(1) deionized water is injected at dispersion tank;
(2) start dispersion machine, add dispersion agent, wetting agent, defoamer, multifunctional assistant, film coalescence aid, ethylene glycol and auxiliary rheological agents successively, dispersed with stirring 10 minutes, rotating speed 400 revs/min;
(3) add Mierocrystalline cellulose, kaolin and titanium dioxide, rotating speed brings up to 1000 revs/min, high speed dispersion 10 minutes;
(4) be decelerated to 500 revs/min, add emulsion, sanitas and thickening material successively, dispersion stirring 10 minutes;
(5) add texture sand, stirring at low speed mixes;
(6) add mill base furnishing required color and namely obtain described sand wall-like texture paint.
Embodiment 5:
A kind of sand wall-like texture paint, each component following by weight part is prepared from: dispersion agent 6 parts, wetting agent 1.5 parts, defoamer 1 part, multifunctional assistant 1 part, film coalescence aid 12 parts, ethylene glycol 20 parts, auxiliary rheological agents 3 parts, Mierocrystalline cellulose 4 parts, kaolin 50 parts, titanium dioxide 80 parts, emulsion 200 parts, sanitas 2 parts, thickening material 4 parts, 750 parts, texture sand, mill base 1 part, deionized water 180 parts.
Described dispersion agent is trisodium phosphate; Described wetting agent is sulphonated oil; Described defoamer is modified paraffin defoamer; Described multifunctional assistant is TERTIARY BUTYL AMINE; Described film coalescence aid is Lauryl Alcohol fat; Described auxiliary rheological agents is polyacrylate; Described Mierocrystalline cellulose is hydroxy ethyl fiber; Described emulsion is pure-acrylic emulsion; Described sanitas is Nordes EPW; Described thickening material is thick dose of association type Polyurethane; Described mill base is selected from inorganic mill base; Described texture sand is circular quartz sand.
The production method of the sand wall-like texture paint described in the present embodiment, comprises following steps:
(1) deionized water is injected at dispersion tank;
(2) start dispersion machine, add dispersion agent, wetting agent, defoamer, multifunctional assistant, film coalescence aid, ethylene glycol and auxiliary rheological agents successively, dispersed with stirring 20 minutes, rotating speed 600 revs/min;
(3) add Mierocrystalline cellulose, kaolin and titanium dioxide, rotating speed brings up to 1500 revs/min, high speed dispersion 30 minutes;
(4) be decelerated to 500 revs/min, add emulsion, sanitas and thickening material successively, dispersion stirring 20 minutes;
(5) add texture sand, stirring at low speed mixes;
(6) add mill base furnishing required color and namely obtain described sand wall-like texture paint.
In various embodiments of the present invention, when described wetting agent is selected from sulfuric acid based hydrazides class and mercaptan acetals, existing arbitrary sulfuric acid based hydrazides class or mercaptan acetal compound can be selected as required; Described titanium dioxide can select unsolicited titanium dioxide, as Rutile type Titanium Dioxide etc.; When described defoamer is selected from modified paraffin defoamer, existing arbitrary modified paraffin defoamer compounds can be selected as required; When described thickening material is selected from inorganic thickening agent or thick dose of association type Polyurethane, existing arbitrary inorganic thickening agent or thick dose of association type Polyurethane can be selected as required; Described mill base can select existing arbitrary organic mill base or inorganic mill base two kinds as required.
Experimental example 1
Product prepared in embodiment of the present invention 1-5 is checked through Wuhan Product Quality Supervision and Inspection Institute, and with the embodiment 6 of CN104151962 for contrast, the main performance index of described sand wall-like texture paint is in table 1;
Table 1: the main performance index of sand wall-like texture paint
Last it is noted that the foregoing is only the preferred embodiments of the present invention, be not limited to the present invention, although with reference to previous embodiment to invention has been detailed description, for a person skilled in the art, it still can be modified to the technical scheme described in foregoing embodiments, or carries out equivalent replacement to wherein portion of techniques feature.Within the spirit and principles in the present invention all, any amendment done, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (8)
1. a sand wall-like texture paint, it is characterized in that: each component following by weight part is prepared from: dispersion agent 2 ~ 6 parts, wetting agent 0.5 ~ 1.5 part, defoamer 0.3 ~ 1 part, multifunctional assistant 0.3 ~ 1 part, film coalescence aid 6 ~ 12 parts, ethylene glycol 12 ~ 20 parts, auxiliary rheological agents 1 ~ 3 part, Mierocrystalline cellulose 2 ~ 4 parts, kaolin 20 ~ 50 parts, titanium dioxide 30 ~ 80 parts, emulsion 100 ~ 200 parts, sanitas 1 ~ 2 part, thickening material 1.5 ~ 4 parts, 500 ~ 750 parts, texture sand, mill base 0.3 ~ 1 part, deionized water 90 ~ 180 parts.
2. sand wall-like texture paint according to claim 1, is characterized in that: each component following by weight part is prepared from: dispersion agent 3 parts, wetting agent 0.8 part, defoamer 0.5 part, multifunctional assistant 0.5 part, film coalescence aid 8 parts, ethylene glycol 15 parts, auxiliary rheological agents 2 parts, Mierocrystalline cellulose 2.5 parts, kaolin 30 parts, titanium dioxide 50 parts, emulsion 160 parts, sanitas 1.5 parts, thickening material 2 parts, 600 parts, texture sand, mill base 0.5 part, deionized water 130 parts.
3. sand wall-like texture paint according to claim 1 and 2, is characterized in that: described dispersion agent is selected from one or more in tripoly phosphate sodium STPP, Sodium hexametaphosphate 99, trisodium phosphate, triethyl hexyl phosphoric acid, sodium lauryl sulphate, methyl amyl alcohol;
Described wetting agent is selected from one or more in sulphonated oil, sulfuric acid based hydrazides class and mercaptan acetals;
Described defoamer is selected from one or more in mineral oil, organosilicon, modified paraffin defoamer;
Described multifunctional assistant is selected from one or more in amine, hydramine and organic amine;
Described film coalescence aid is selected from one or more in propandiol butyl ether, propylene glycol monomethyl ether amyl acetate, Lauryl Alcohol fat, propylene glycol phenylate;
Described auxiliary rheological agents is selected from one or more in organic clay, wilkinite, Mierocrystalline cellulose, xanthan gum, polyacrylate, Polyurethane;
Described Mierocrystalline cellulose is selected from one or more in methylcellulose gum, ethyl cellulose, hydroxy ethyl fiber;
Described emulsion is selected from one or more in benzene emulsion, pure-acrylic emulsion, organosilicon crylic acid latex, elastic emulsion;
Described sanitas is selected from isothiazolinone derivatives, benzimidazole ester class, Dao Weixier-75,1, one or more in 2-benzisothiazole-3-ketone;
Described thickening material is selected from one or more in thick dose of inorganic thickening agent, polyacrylate and association type Polyurethane;
Described mill base is selected from organic mill base and/or inorganic mill base.
4. sand wall-like texture paint according to claim 1 and 2, is characterized in that: described texture sand is circular quartz sand.
5. the production method of sand wall-like texture paint according to any one of claim 1 to 4, comprises following steps:
(1) deionized water is injected at dispersion tank;
(2) start dispersion machine, add dispersion agent, wetting agent, defoamer, multifunctional assistant, film coalescence aid, ethylene glycol and auxiliary rheological agents successively, dispersed with stirring 10 ~ 20 minutes, rotating speed 400 ~ 600 revs/min;
(3) add Mierocrystalline cellulose, kaolin and titanium dioxide, rotating speed brings up to 1000 ~ 1500 revs/min, high speed dispersion 10 ~ 30 minutes;
(4) be decelerated to 500 ~ 700 revs/min, add emulsion, sanitas and thickening material successively, dispersion stirring 10 ~ 20 minutes;
(5) add texture sand, stirring at low speed mixes;
(6) add mill base furnishing required color and namely obtain described sand wall-like texture paint.
6. the production method of sand wall-like texture paint according to claim 5, is characterized in that: step (2) dispersed with stirring 15 minutes, rotating speed 500 revs/min.
7. the production method of the sand wall-like texture paint according to claim 5 or 6, is characterized in that: step (3) rotating speed brings up to 1200 revs/min, high speed dispersion 20 minutes.
8. the production method of the sand wall-like texture paint according to claim 5 or 6, is characterized in that: step (4) is decelerated to 600 revs/min, adds emulsion, sanitas and thickening material successively, dispersion stirring 15 minutes.
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Application publication date: 20150930 |